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Analyzing the impact of individual alloying elements on weld microstructure: In situ chemical composition measurement during TIG welding of Duplex Stainless Steels microstructure

  • Various industrial applications require the joining of DSS components. Tungsten Inert Gas (TIG) welding is particularly well-suited for this purpose due to the ability to achieve highly reproducible automated welds. However, during solidification of the weld pool, critical phase ratios of ferrite (α) and austenite (γ) may occur, leading to solidification cracking, increased corrosion susceptibility, lower ductility and critical strength values. Hence, in order to achieve the desired material characteristics, it is crucial to accurately predict the α/γ phase ratio within the weld. Conventionally, the WRC-1992 diagram is employed for this purpose. In our study, we used Laser-Induced Breakdown Spectroscopy (LIBS) to track alterations in the chemical composition of the weld metal on the surface throughout the welding process. One significant benefit of this method is its capability to provide precise and real-time measurements of chemical compositions during welding, both temporally andVarious industrial applications require the joining of DSS components. Tungsten Inert Gas (TIG) welding is particularly well-suited for this purpose due to the ability to achieve highly reproducible automated welds. However, during solidification of the weld pool, critical phase ratios of ferrite (α) and austenite (γ) may occur, leading to solidification cracking, increased corrosion susceptibility, lower ductility and critical strength values. Hence, in order to achieve the desired material characteristics, it is crucial to accurately predict the α/γ phase ratio within the weld. Conventionally, the WRC-1992 diagram is employed for this purpose. In our study, we used Laser-Induced Breakdown Spectroscopy (LIBS) to track alterations in the chemical composition of the weld metal on the surface throughout the welding process. One significant benefit of this method is its capability to provide precise and real-time measurements of chemical compositions during welding, both temporally and spatially. In previous investigations, we could develop routines to quantify the measurement of chemical compositions within the weld metal and the Heat-Affected Zone (HAZ). The conducted research focuses on examining the alterations in chemical concentrations of specific alloying elements, namely Cu and Mn as γ-forming elements, and Nb and Cr as α-forming elements, during welding. These changes are measured in real-time using Laser-Induced Breakdown Spectroscopy (LIBS). To achieve this, both the ferrite number, determined through magnetic-inductive techniques, and the weld microstructure are analyzed. Through image-analytical methods, a correlation is established between the microstructure and the LIBS data obtained.zeige mehrzeige weniger

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Metadaten
Autor*innen:Lukas QuackatzORCiD
Koautor*innen:Axel Griesche, Thomas Kannengießer, Kai Treutler, Volker Wesling
Dokumenttyp:Vortrag
Veröffentlichungsform:Präsentation
Sprache:Englisch
Jahr der Erstveröffentlichung:2023
Organisationseinheit der BAM:9 Komponentensicherheit
9 Komponentensicherheit / 9.4 Integrität von Schweißverbindungen
DDC-Klassifikation:Technik, Medizin, angewandte Wissenschaften / Ingenieurwissenschaften / Ingenieurwissenschaften und zugeordnete Tätigkeiten
Freie Schlagwörter:Duplex stainless steel; In situ measurement; LIBS; TIG welding
Themenfelder/Aktivitätsfelder der BAM:Material
Material / Degradation von Werkstoffen
Veranstaltung:AJP 2023
Veranstaltungsort:Braga, Portugal
Beginndatum der Veranstaltung:19.10.2023
Enddatum der Veranstaltung:20.10.2023
Verfügbarkeit des Dokuments:Datei im Netzwerk der BAM verfügbar ("Closed Access")
Datum der Freischaltung:26.10.2023
Referierte Publikation:Nein
Eingeladener Vortrag:Nein
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