Chemie und Prozesstechnik
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A software toolbox is introduced that addresses several needs common to computed tomography (CT). Built for the WIPANO CTSimU project to serve as the reference implementation for its image processing and evaluation tasks, it provides a Python 3 interface that is adaptable to many conceivable applications. Foremost, the toolbox features a pipeline architecture for sequential 2D image processing tasks, such as flat field corrections and image binning, and enables the user to create their own processing modules. Beyond that, it provides means to measure line profiles and image quality assessment algorithms to calculate modulation transfer functions (MTF) or to determine the interpolated basic spatial resolution (iSRb) using a duplex wire image. It can also be used to calculate projection matrices for the reconstruction of scans with arbitrary industrial CT geometries and trajectories. The CTSimU project defined a framework of projection- and volume-based test scenarios for the qualification of radiographic simulation software towards its use in dimensional metrology. The toolbox implements the necessary evaluation routines and generates reports for all projection-based tests.
CS particles show unique properties by merging individual characteristics of the core and the shell materials. An alteration particularly in their surface roughness affects the final performance of the particles in the targeted application. Quantitative evaluation of the roughness of CS microparticles is, however, a challenging task employing microscopic techniques being scarce and showing large differences in terms of methodology and results.
In our previous work, we have reported a systematic study with a reliable analysis tool, which evaluates profile roughness quantitatively, for individual core-shell microparticles using electron microscopy (EM) images of both types, Scanning Electron Microscopy (SEM) and transmission mode SEM (or TSEM). The SEM images contain two-dimensional (2D) information, therefore, provide profile roughness data only from the projection in the horizontal plane (in other words, from the “belly”) of a spherical particle. The present study offers a practical procedure to give access to more information by tilting the sample holder and hence allowing images of a single particle to be recorded at different orientations under the same view angle. From the analysis of these images, extended information on surface roughness of the particle can be extracted. Thus, instead of obtaining 2D information from a single SEM image, three-dimensional (3D) information is obtained from 2D projections recorded at different particle orientations.