Angewandte Physik
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- 3 Gefahrgutumschließungen; Energiespeicher (9)
- 3.4 Sicherheit von Lagerbehältern (7)
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- 3.3 Sicherheit von Transportbehältern (4)
- 6 Materialchemie (2)
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Optical and thermal analysis of PVB encapsulant polymer functionalized with luminescent organic dyes
(2018)
This work focused on the technology of luminescent down shift (LDS), with a primary aim to identify and investigate a methodology to introduce the luminescent organic dye into PVB polymer encapsulant as emergent material for photovoltaic application. For this goal, we propose to study the feasibility to implement the LDS functionality and to identify suitability of available luminescent to be incorporated into the host polymer encapsulant material. The first step to this direction was through a comprehensive optical study of Violet 570 (V) organic dye in ethanol solvent. The methodology and experimental conditions such as laboratory polymer preparation and luminescence dye concentration were presented. Also, the emergent polymer encapsulant sheets were characterized by using optical and thermal analysis techniques. The absorption spectrum of the prepared PVB material shifts towards longer wavelengths, with increasing organic dye concentration.
Current standards governing the design, qualification and in-service inspection of carbon fibre composite cylinders do not facilitate to optimise cylinder design. The requirements have been adapted from standards for metallic cylinders and cannot easily quantify the degradation processes in composite materials. In this article, the results of hydraulic and hydrogen pressure cycle life tests performed on composite reinforced tanks with a metal liner (type 3) and with a high density polymer liner (type 4) are shown. Moreover, the degradation measured by means of residual strength of the tanks after the cycling tests have been compared. It has been found that the most critical aging for metal based composite cylinder is the gaseous cycling while type 4 designs seem to be more sensitive to hydraulic cycling at high temperature.
Accident safe packages for the transport of spent nuclear fuel and high-level waste shall fulfil international IAEA safety requirements. Compliance is shown by consecutive mechanical and thermal testing. Additional numerical analysis are usually part of the safety evaluation. For damage protection some package designs are equipped with wood filled impact limiters encapsulated by steel sheets. The safety of these packages is established in compliance with IAEA regulations. Cumulative mechanical and fire tests are conducted to achieve safety standards and to prevent loss of containment. Mechanical reliability is proven by drop tests. Drop testing might cause significant damage of the impact limiter steel sheets and might enable sufficient oxygen supply to the impact limiter during the fire test to ignite the wood filling. The boundary conditions of the fire test are precisely described in the IAEA regulatory. During the test the impact limiter will be subjected to a 30 minute enduring fire phase. Subsequent to the fire phase any burning of the specimen has to extinguish naturally and no artificial cooling is allowed. At BAM a large-scale fire test with a real size impact limiter and a wood volume of about 3m3 was conducted to investigate the burning behaviour of wood filled impact limiters in steel sheet encapsulation. The impact limiter was equipped with extensive temperature monitoring equipment. Until today burning of such impact limiters is not sufficiently considered in transport package design and more investigation is necessary to explore the consequences of the impacting fire. The objective of the large scale test was to find out whether a self-sustaining smouldering or even a flaming fire inside the impact limiter was initiated and what impact on the cask is resulting. The amount of energy, transferred from the impact limiter into the cask is of particular importance for the safety of heavy weight packages. With the intention of heat flux quantification a new approach was made and a test bench was designed.
Micro- and nanostructuring with laser-induced periodic surface structures (LIPSS) has been demonstrated to be feasible in a wide variety of materials including metals, semiconductors and dielectrics. Suitable processing regimes for flat, curved and complex surfaces have been identified for many materials, allowing the generation of diverse applications in fields such as optics, tribology and medicine, to name a few. A common side effect when producing such structures in air environment is the formation of a thin surface oxide layer in the laser irradiated areas. Previous studies have shown that oxidation plays an important role in the tribological performance for which the structures where created, and very recently it has been shown that the laser-induced oxide graded layers may contribute to the formation of a new type of embedded low-spatial frequency LIPSS (LSFL) with annomalous orientation parallel to the laser polarization, in addition to the appearance of the well-known high-spatial frequency LIPSS (HSFL) at the surface. In this contribution, we explore this effect experimentally for chromium nitride (CrN) irradiated with femtosecond laser pulses and compare the findings to finite-difference time-domain (FDTD) simulations of the intensity distributions at different depth positions.
The authors are currently investigating the possibility to apply compaction grouting for offshore pile foundations (Jacket piles as well as monopiles) as a possible retrofitting technique for an optimised foundation concept. In this research project, we are developing a design approach aiming to predict the ideal amount and properties of a grout for a specific soil situation and desired improvement of pile bearing capacity after Installation and during service time. Both numerical and experimental tests have been carried out to investigate the injection process during which a highly viscous grout is injected into the soil under high pressure to displace and compact the surrounding soil without fracturing it. The implicit Material Point Method (MPM) based on a mixed formulation is the numerical technique chosen to deal with the expected large deformations and the arbitrary shape of the developing grout bulb. The usage of MPM prevents both the need of remeshing and the numerical instability induced by extensive mesh distortion. For validation with experimental results, we have constructed a testing chamber with one transparent sidewall. This chamber enables us to observe the injection process directly at the transparent vertical window and to measure the in-plane soil displacements and strains by means of the Digital Image Correlation (DIC) technique.
The results already reveal the interrelation of soil and grout properties for a successful usage of this common ground improvement technique.
The new crack luminescence method offers the possibility of making fatigue surface cracks in metallic materials more visible during inspections through a special coating system. This coating system consists of two layers, whereby the first layer has fluorescent properties and emits visible light as soon as it is irradiated by UV light. The top layer is black and is designed to prevent the fluorescent layer from emitting if no crack develops in the underlying material. The technique proved particularly useful in a wide variety of fatigue tests of steel components under laboratory conditions. Moreover, it has the potential to be used in various industrial applications. To enable industrial deployment and integration into maintenance strategies, a concept study is developed in this contribution, resulting in a qualification framework that can serve as a foundation for determining the reliability of the crack luminescence system in terms of a probability of detection curve. Within this study, factors causing measurement variability and uncertainty are being determined and their influences assessed. Due to the extension of the system by a moving computer vision system for automated crack detection using artificial intelligence, additional long-term effects associated with structural health monitoring systems need to be incorporated into an extended probability of detection study as part of the technical justification. Finally, important aspects and findings related to design of experiments are discussed, and a framework for reliability assessment of a new optical crack monitoring method is presented, emphasizing the influence of various uncertainty parameters, including long-term effects such as system ageing.
Several ultrasonic approaches for material determination are formulated in terms of an (nonlinear) inverse problem, e.g. immersion technique (Castaings et al. (2000)) or plate-waveguide techniques (Marzani et al. (2012)). In this contribution we focus on cylindrical waveguides for ultrasonic material determination and especially on the sensitivity of recorded transmission signals to the material properties. We utilize composite scaled sensitivities to determine the information content that can be achieved by the setup to certain parameters and discuss the limitations of the approach.
The Bundesanstalt für Materialforschung und –Prüfung (BAM) runs an investigation program on the long-term behavior of multi-component metal seals. Such seals are used in a wide area of applications including transport and storage casks for spent nuclear fuel and high level radioactive waste.
The seal function is mainly based on the compression of the inner helical spring, which generates the necessary seal force to keep the sealing surfaces in close contact. This in turn leads to a plastic deformation of the outer jacket of the seal, comprised of highly ductile aluminum or silver that adapts to the sealing surfaces of cask body and bolted lid, thus providing high Level leak tightness. In Germany, those casks are licensed for Interim storage periods of up to 40 years or more if extended Interim storage would become necessary before a final repository is available. Thus, the sealing performance has to be evaluated, including factors like elevated temperature due to decay heat or mechanical loads due to transport under normal as well as accident conditions. Long-term investigations at BAM have been running over the last nine years to identify and evaluate the seal performance by measuring the remaining seal force, the useable resilience and the leakage rate after various time intervals at temperatures ranging from room temperature up
to 150 °C. It was found that the seal force and useable resilience decrease with time and temperature, caused by creep deformation of the outer jacket. In order to obtain an analytical description for the seal behavior and to achieve more information on the material behavior under application conditions a comprehensive investigation program with Focus on aluminum as outer jacket material was launched. The program includes material investigations such as compression and tension creep tests with representative basic materials. An additional test setup allows for the continuous measurement of the remaining seal force at temperatures of up to 150 °C. Furthermore, seal segments are compressed and stored in heating chambers, thus producing segments at different stages of the aging process. The segments are investigated regarding the development of the contact area width, jacket thickness and microstructural changes. This data will be used to develop material models and an analytical description of the time and temperature dependent long-term sealing behavior. This paper explains the current status of gained test results and modelling approaches and closes with an outlook to the future Project plans.
Online condition monitoring of submarine power cables helps to avert failures and damages produced by mechanical impacts. We report, to our knowledge for the first time, on investigations regarding the feasibility of distributed fiber optic acoustic sensors based on C-OTDR, with the sensor fibres being embedded in the cable, to detect vibrations due to mechanical disturbances along the cable. We present first results of sensing experiments where acoustic signals are transmitted through water to simulate the corresponding submarine conditions. Furthermore, we show results evaluating the usefulness of fibre commonly embedded in existing power cable designs for our sensing purposes.
A permanent-magnet synchronous motor (PMSM) servo drive for lightweight robotic platforms that have a high torque demand at low rotational speeds has been developed. First, a current-independent torque controller is derived and cascaded with a speed and position controller, while merely an encoder is used as a sensor device in combination with a speed estimator. Finally, the speed estimator output is compared to gyroscope measurements and the overall functioning is verified on a real system.
Elastomers show a high versatility which makes them ideal materials for sealing applications in various fields. Especially under changing application conditions the high recovery potential of this class of material is beneficial to compensate temperature or pressure fluctuation, and geometrical changes resulting from mechanical loads in e.g. accident conditions. Out of these reasons elastomers are also used in containers for low and intermediate level radioactive waste and for spent fuel transportation casks. In casks designed for low and intermediate level waste elastomer seals can act as primary seal responsible for the containment function whereas in spent fuel storage and transportation casks (dual purpose casks (DPC)) elastomer seals are used as auxiliary seals to allow leakage rate measurements of metal barrier seals. An inherent prerequisite for this kind of application is the Long time-scale of operation without or with limited possibility of seal replacement. In Germany an interim storage license for DPC`s is typically issued for 40 years, a timeframe which might increase in the future due to challenges of the final repository siting procedure. For low and intermediate level waste, also long time periods are required before final disposal can be achieved. Therefore, the performance of elastomer seals over extended time periods is, as for other applications, of high importance.
A typical approach to ensure long-term functionality is to perform accelerated aging tests to calculate an estimated lifetime by assuming e.g. Arrhenius like equations for the timetemperature relationship. This approach requires a suitable end of life criterion considering the application of interest. This often can represent a challenge on its own.
As BAM is involved in most of the cask licensing procedures and especially responsible for the evaluation of cask-related long-term safety issues we initiated several test programs for investigating the behavior of elastomer seals. Experiments concerning the low temperature performance down to -40 °C and the influence of gamma irradiation have been started first.
Currently the thermal aging behavior of elastomer seals, which is the topic of this contribution, is examined. For our aging investigations we use a broad approach to first determine the property changes in different elastomer materials due to thermo-oxidative aging at elevated temperatures and secondly, we test how the typical methods of lifetime extrapolation can be applied to these results. This Approach enables us to detect and exclude undesired side effects which very often influence lifetime estimations. In this contribution, our recent results are extended. The results show that lifetime estimation based on single material properties can be misleading and therefore a combination of several methods is recommended.
CONRAD-2 is an imaging instrument using low-energy (cold) neutrons. The instrument is installed at the end of a curved neutron guide which avoids the direct line of sight towards the reactor core. This ensures a very low background of high-energy neutrons and. photons at the sample position. The cold neutron beam provides a wavelength range which is suitable for phase-and diffraction-contrast imaging such as grating interferometry and Bragg edge mapping. The instrument is well suited for high resolution imaging due to the high efficiency of the very thin scintillators that can be used for the detection of cold neutrons. An instrument upgrade was performed recently as a part of an upgrade program for the cold neutron instrumentation at HZB. The parameters of the instrument as well as some research highlights will be presented.
The shaft bearing capacity often plays a dominant role for the overall structural behaviour of axially loaded piles in offshore deep foundations. Under cyclic loading, a narrow zone of soil at the pile-soil interface is subject to cyclic shearing solicitations. Thereby, the soil may densify and lead to a decrease of confining stress around the pile due to microphenomena such as particle crushing, migration and rearrangement. This reduction of radial stress has a direct impact on the shaft capacity, potentially leading in extreme cases to pile failure. An adequate interface model is needed in order to model this behaviour numerically. Different authors have proposed models that take typical Interface phenomena in account such as densification, grain breakage, normal pressure effect and roughness. However, as the models become more complex, a great number of material parameters need to be defined and calibrated. This paper proposes the adoption and transformation of an existing soil bulk model (Pastor- Zienkiewicz) into an interface model. To calibrate the new interface model, the results of an experimental campaign with the ring shear device under cyclic loading conditions are here presented. The constitutive model shows a good capability to reproduce typical features of sand behaviour such as cyclic compaction and dilatancy, which in saturated partially-drained conditions may lead to liquefaction and cyclic mobility phenomena.
We introduce the optical frequency domain reflectometry (OFDR) technique based on intensity modulation frequency sweep measurement for distributed disturbance measurement in optical fibres. By evaluating interferometric Rayleigh scattering changes along the fibre, strain and temperature changes are detected with 100 nε sensitivity and 10 mK resolution. The vibration frequencies for low frequencies and up to the kHz-range can be obtained from power change Evaluation in the spatial domain. This novel OFDR approach is a low-cost alternative for distributed disturbance measurement up to distances of several kilometres.
Investigation of the internal impact during a 9 m drop test of an accident-safe waste package
(2021)
The safety assessment of packages for the transport of radioactive material follows the IAEA regulations and guidance. The specified regulatory tests cover severe accidents and demonstrate the package containment system integrity.
Special attention must be drawn to the behaviour of the content which could move inside the package due to unpreventable gaps caused by the loading procedure and the structure of the content. A possible internal impact of the content which occurs during the drop tests onto the lid system is investigated. The IAEA regulations SSR-6 and the Guidance SSG-26, revised recently, consider input from Germany and France related to the significance of internal gaps.
In the context of a waste package design assessment, a model was equipped with a representative content to conduct a drop test with an internal impact. The weight and kinetic impact of this content covered all possible real contents. The objective of the test was to maximize the load onto the lid system and to prove the mechanical integrity by complying with the required leak tightness. The test was conducted
conservatively at a package temperature lower than -40 °C at the BAM Test Site Technical Safety.
This paper gives an overview of efforts to address internal gaps and their consequences, and the BAM efforts with the implementation of this topic into IAEA regulations and guidance material. The paper then focuses on the conduction of a drop test and investigation of internal component impact.
Packages for intermediate level waste (ILW) often contain residual water besides the actual waste. The water either exists as obvious free water or it may be bound physically or chemically, e.g. as pore water. A water driven gas generation could occur by vaporisation and by radiolysis. Steam as the result of vaporisation causes an increasing pressure inside a package and can affect corrosion. Vaporisation and condensation processes itself change the thermal behavior of the content especially during strongly unsteady thermal situations like accident fire situations. Radiolysis changes the chemical composition of the content which could cause an unexpected interaction, e.g. hydrogen embrittlement. Besides the pressure build-up the radiolysis of water generates hydrogen and oxygen, which can be highly flammable respectively explosive. The gas generation caused by vaporisation and radiolysis must be taken into account during the design and the safety assessment of a package. Pressure build-up, a changed thermal behavior and content chemistry, and especially the risk of accumulation of combustible gases exceeding the limiting concentration for flammability has to be considered in the safety assessment. Approaches to ensure the transportability of stored packages due to radiolysis will be discussed.
Typical transport packages used in Germany are equipped with wooden impact limiting devices. In this paper we give an overview of the latest status regarding the development of a finite element material model for the crush of spruce wood. Although the crush of wood – mainly in longitudinal direction – is a phenomenon governed by macroscopic fracture and failure of wood fibres we smear fracture and failure mechanisms over the continuous voume. In first step we altered an existing LS-DYNA material model for foams, which considers an ellipse shaped yield surface written in terms of the first two stress invariants. The evolution of the yield surface in the existing model depends on the volumetric strain only. For the use with spruce wood, we modified the existing material model to consider the deviatoric strain for the evolution of the yield surface as well. This is in accordance with the results of crush tests with spruce wood specimens, where the crushing deformation was rather deviatoric for uniaxial stress states and rather volumetric for multiaxial stress states We rate the basic idea of this approach to be reasonable, though other problems exist regarding the shape of the yield surface and the assumption of isotropic material properties. Therefore we developed a new transversal isotropic material model with two main directions, which considers different yield curves according to the multiaxiality of the stress state via a multi-surface yield criterion and a non-associated flow rule. The results show the ability to reproduce the basic strength characteristics of spruce wood. Nevertheless, problems with regularization etc. show that additional investigations are necessary.
A 400 m² soil test field with gas injection system was built up, which enables an experimental validation of linear gas sensors for specific applications and gases in an application-relevant scale. Several injection and soil watering experiments with carbon dioxide (CO2) at different days with varying boundary conditions were performed indicating the potential of the method for, e.g., rapid leakage detection with respect to Carbon Capture and Storage (CCS) issues.
Pipe steels suitable for carbon capture and storage technology (CCS) require resistance against the corrosive environment of a potential CCS-site, e.g. heat, pressure, salinity of the aquifer, CO2-partial pressure. Samples of different mild and high alloyed stainless injection-pipe steels partially heat treated: 42CrMo4, X20Cr13, X46Cr13, X35CrMo4 as well as X5CrNiCuNb16-4 were kept at T=60 °C and ambient pressure as well as p=100 bar for 700 h - 8000 h in a CO2-saturated synthetic aquifer environment similar to possible geological on-shore CCS-sites in the northern German Basin. Main corrosion products are FeCO3 and FeOOH. Corrosion rates obtained at 100 bar are generally much lower than those measured at ambient pressure. Highest surface corrosion rates are 0.8 mm/year for 42CrMo4 and lowest 0.01 mm/year for X5CrNiCuNb16-4 in the vapour phase at ambient pressure. At 100 bar the highest corrosion rates are 0.01 mm/year for 42CrMo4, X20Cr13 (liquid phase), X46Cr13 and less than 0.01 mm/year for X35CrMo4 and X5CrNiCuNb16-4 after 8000 h of exposure with no regard to atmosphere. Martensitic microstructure offers good corrosion resistance.
This paper scopes the specialties of a hazard identification study for large and extra-large unmanned undersea vehicles (UUVs). A generic node/function structure is derived from different large and extra-large UUV designs, partially own vehicle designs from research projects, and partially from commercial vehicles. For each node, a short overview of its components and the proper function or operations is defined. A set of guide words is used to prompt a hazard discussion for each node, which identifies unwanted functions, resulting in potential hazards and unmitigated consequences. Related to the SafeMASS-Report from DNV, this work concentrates on selected topics of the bridge-related function on voyage, control & monitoring, and abnormal situations. For unmanned vehicles without any person on board, these three topics become more important for underwater vehicles with very limited connectivity or temporary disruptions of communication whereby an operator in a remote-control center could only be provided with rough vehicle or mission states. Therefore, vehicle control, whether in hard- or software, must handle most tasks belonging to the considered functions automatically or autonomously. Hence, the most appropriate reactions of the system to unwanted system
behavior must be implemented. This HAZID study could, on the one hand, be used as background for such an implementation, and on the other hand, it is used to verify the implemented actions on the risks and hazards.
We report on the successful application of distributed acoustic sensing (DAS) to the detection of partial discharge (PD). A detection limit of about 1 nC discharge magnitude was achieved for PD in a real-scale model of a high voltage termination. Dedicated ultrasonic fibre-optic transducers were interrogated using coherent optical time-domain Rayleigh backscatter reflectometry (C-OTDR). Random quadrature demodulation was employed for retrieving relevant acoustic information from the raw C-OTDR backscatter traces. To our knowledge, our results are a first-time demonstration that quasi-distributed fibre-optic acoustic sensing is a candidate technology for the acoustic partial discharge monitoring of power cable joints and terminations.
The containment systems of transport casks for spent fuel and high radioactive waste usually include bolted lids with metallic or elastomeric seals.
The mechanical and thermal loadings associated with the routine, normal and accident conditions of transport can have a significant effect on the leak tightness of such containment system.
Scaled cask models are often used for providing the required mechanical and thermal tests series. Leak tests have been conducted on those models.
It is also common practice to use scaled component tests to investigate the influence of deformations or displacements of the lids and the seals on the standard leakage rate as well as to study the temperature and time depending alteration of the seals.
In this paper questions of the transferability of scaled test results to the full size design of the containment system will be discussed.
To increase the competitiveness of jacket substructures compared to monopiles a changeover from an individual towards a serial jacket production based on automated manufactured tubular joints com-bined with standardized pipes has to be achieved. Therefore, this paper addresses fatigue tests of automatical-ly welded tubular X-joints focusing on the location of the technical fatigue crack. For this X-joint, the detect-ed location of the technical crack is then compared to numerical investigations predicting the most fatigue prone notch considering the structural stress approach as well as the notch stress approach. Additionally, the fatigue prone hot spot according to both approaches is compared for a typical offshore jacket double-K-joint to emphasize the significance of the presented outcomes for the existing offshore structures. Besides, the welding process of the automated manufactured tubular X-joints is presented.
The shock absorbing material damping concrete is for the foundation in dry interim storage facilities for radioactive waste in Germany. In case of a potential cask drop damping concrete minimizes the mechanical loads to the cask. In course of safety analyzes this accident scenario is considered by numerical simulations using the finite element method. To get reliable results of numerical simulations a suitable material model is needed to take the characteristics of damping concrete into account. Due to the lack of sufficient material knowledge a research project was started to characterize the material’s behavior under different load conditions. This paper presents the test program to analyze the material behavior of damping concrete which is characterized by large volume change and
strain rate hardening dependence. The determined Parameters were used to adapt an existing material model of the FE-code ABAQUS®. This model has to handle the mechanical damage behavior of damping concrete which occurs under compression and shear loads during a potential cask drop. To verify the material model numerical simulations are compared with dynamic penetration tests, which were conducted with specimens assembled similar to the real application of the damping concrete footings. The transferability of the material
model to a real accident scenario was verified by a drop test with a full-scale cask on a damping concrete footing.
Polyurethane foam used as impact limiter material undergoes high plastic deformations, whereat the resulting stress-strain relations strongly depend on loading speed and temperature. This paper discusses the efforts necessary to develop a reliable numerical foam simulation model focussing on generation and implementation of temperature- dependent yield curves
Light concentration opens up the path to enhanced material efficiency of solar cells via increased conversion efficiency and decreased material requirement. For true material saving, a fabrication method allowing local growth of high quality absorber material is essential. We present two scalable fs-laser based approaches for bottom-up growth of Cu(In,Ga)Se2 micro islands utilizing either site-controlled assembly of In(,Ga) droplets on laser-patterned substrates during physical vapor deposition, or laser-induced forward transfer of (Cu,In,Ga) layers for local precursor arrangement. The Cu(In,Ga)Se2 absorbers formed after selenization can deliver working solar devices showing efficiency enhancement under light concentration.
Identifying optimal inspection and repair strategies for offshore jacket structures is a challenging task. We pre-sent an approach, which is based on recent developments in the field of risk-based operation and maintenance planning at the structural system level. The approach utilizes heuristics to define inspection and repair strate-gies at the system level and to reduce the search space of possible strategies. For each defined strategy, the expected service life cost of inspection, repair and failure is evaluated based on simulated inspection and re-pair histories. Subset simulation is applied to compute the conditional repair and failure probabilities required for this analysis. It also forms the basis for simulating inspection and repair histories. The strategy that mini-mizes the expected service life cost is the optimal one in the set of pre-selected strategies. The underlying condition and performance model accounts for the stochastic dependence among the deterioration states of the different structural elements and the structural redundancy. The approach is demonstrated in a case study considering a jacket-type frame. In this study, we essentially vary the inspection interval, the minimum num-ber of inspected components and the target reliability, and identify the combination that minimizes the ex-pected total service life cost.
Current trend suggests that global energy consumption will increase in the future. This growing energy demand and advancement of technology lead to explore all potential offshore fossil and non-fossil energy sources, necessitating erection of exploration and production structures, rigs, platforms and towers, which are susceptible to adverse environmental conditions along with their maintenances. Cylindrical grouted joints provide suitable connections between steel substructure and foundation in these offshore platforms and wind structures especially monopiles for ease of installation. However, these are composite connections with exterior sleeve, interior pile and infill grout. The capacity of these connections is affected by number of factors. The literature over last four decades by numerous researchers has shown the development of these connections with increasingly higher capacities and influences on these capacities due to various factors. This paper provides a comprehensive review on the factors affecting the connection capacity along with technical challenges for the future. Critical aspects and shortcomings of the current connection systems and potential solutions may be sought after for these issues are also discussed.
Superplasticizer and Shrinkage Reducing Admixture Dosages for Microfine Cement in Grout Systems
(2019)
Grouts have numerous applications including crack repair as maintenance in construction industries. Microfine cements are intensively used for high strength mortar and grout products. They are ideal for injection grouting in structural repair. Such grouts should have suitable rheological properties to be injectable, especially those used in repair and rehabilitation. The use of superplasticizers (SP) in these products is thus becoming increasingly crucial to achieve favorable workability and viscosity properties. A difficulty in such grouts is the plastic shrinkage due to finer particles used. It is thus necessary to determine optimum SP and shrinkage reducing admixture (SRA) dosages for a microfine cement based grout. In this study, a saturation dosage was decided from two Polycarboxylate ether (PCE) based SPs in relation to neat cement using slump flow and rheological parameters. A range of grout mixtures was formulated containing micro silica (MS) and fly ash (FA), and tested for suitable rheological and mechanical parameters. Based on the results, a grout mixture with MS and FA was selected to determine optimum SRA content. According to the results, a SP dosage of 3% by weight of neat cement is sufficient to achieve saturation. The grout material including MS and FA can produce comparable properties to neat cement grout. MS is found to improve compressive strength within the range considered, whereas a higher FA content provides favourable rheological properties. Finally, a SRA dosage of 4%, which could reduce the shrinkage by about 43% after 28d days, is determined for the grout system.
In this paper, we present the first results regarding the on-line monitoring of gamma-ray exposure effects on a commercial multi-mode perfluorinated polymer optical fiber (PF-POF), type GigaPOF-50SR from Chromis Fiberoptics. Our focus was to evaluate on-line the radiation induced attenuation (RIA) over a wide spectral range (320 nm – 1700 nm), in order to assess the fiber’s radiation hardness and its possible use in radiation detection. An Ocean Optics QE65000 high sensitivity spectrometer and a StellarNet near-IR spectrometer were used to cover the spectral ranges 200 nm – 1μm and 900 nm – 1.6 μm, respectively. Electron paramagnetic resonance was used to monitor the recovery of the irradiation induced centers at room temperature. The study indicated that the optical fiber can be used as radiation monitor at low dose rates by measuring the attenuation in the UV, while higher dose rates irradiation can be observed by RIA monitoring at specific wavelengths in the visible spectral range.
Sensitivity of two commercial perfluorinated (PF) polymer optical fibers (POFs) to gamma radiation was measured, compared and exploited for dosimetry purposes. Fiber radiation induced attenuation (RIA) was found to be highly wavelength dependent and pronounced towards the UV part of the spectrum. PF-POFs were shown to be highly radiation sensitive and RIA-based on-line radiation monitoring with sensitivity as high as 135 dBm-1/kGy was demonstrated at 460 nm with co-extruded PF-POF. In addition, thanks to low inherent attenuation in the near-infrared region, possibility of distributed radiation detection with PF-POFs was demonstrated for the first time, utilizing optical time domain reflectometry.
The sensitivity of low-loss perfluorinated polymer optical fiber (PF-POF) to gamma radiation is investigated for on-line radiation monitoring purposes. The radiation-induced attenuation (RIA) of a commercial PF-POF based on Cytop material is measured in the visible spectral region. The fiber RIA shows strong wavelength dependence with rapid increase towards the blue side of the spectrum. The wide range of radiation sensitivities is available via careful selection of appropriate monitoring wavelength. The accessible sensitivities span from 1.6 ± 0.2 dBm-1/kGy measured at 750 nm to 18.3 ± 0.7 dBm-1/kGy measured at 420 nm. The fairly high radiation sensitivity as well as its wide tunability makes the fiber a promising candidate for a broad range of applications.
Up to now, the inspection of wind turbines with industrial climbers has been considered ”state of the art”. However, ever-larger wind turbines and advancing digitization make modern and automated inspection methods indispensable. Passive thermography can serve as such a digital and atomized method while it is well known for its applications in the inspection of buildings or electrical circuits. However, its application relies on thermal gradients in the inspected object such that a temperature contrast exists between damaged and sound areas. This also holds for unheated structures like rotor blades of wind turbines which show no intrinsic temperature gradient and can hardly be heated. Under certain weather conditions with sufficient solar loading and diurnal temperature variations, passive thermography is suitable for the in-service inspection of rotor blades. However, for a reliable use of passive thermography on ”thermal passive” components, the incorporation of these environmental conditions in the planning and evaluation of thermal inspections is crucial. Additionally, the complex inner structure of wind turbine blades in comparison to other objects and buildings require a specific method referencing the individual rotor blades to each other. This allows the distinction between the thermal response of design-specific structural features and damages or irregularities between the three blades. We show thermal signatures of damage in rotor blades and contrast them with structural characteristics by comparing the three blades. In addition to measurements in industrial environments, laboratory measurements are shown and compared to simulations. The long-term goal is to simulate the influence of different weather parameters and thus gain a better understanding of measurements in the field. The results shown here can be seen as one step towards industrial application.
Accelerated electrical and mechanical ageing tests of high temperature low sag (HTLS) conductors
(2017)
As part of the Best Paths project, work package 6 of the DEMO #4 combines the R&D tasks for repowering of transmission overhead line corridors. The aim of the presented research work is the electrical and mechanical investigation of high temperature low sag conductors (HTLS) and their respective accessories. In contrast to the conventional ACSR (aluminum conductor steel reinforced) conductors, new material combinations of HTLS technologies result in a better sagging behavior combined with an operation at higher temperatures. Because of missing operational experience, the ageing behavior of HTLS conductor technologies shall be analyzed regarding the operating parameters such as electrical, thermal and mechanical load.
Numerical approach to determine the correct puncture bar length for the IAEA puncture bar drop test
(2018)
Among other mechanical tests the 1 meter drop onto a steel puncture bar shall be considered for accident safe packages for the transport of radioactive material. According with the IAEA regulations “the bar shall be of solid mild steel of circular section, 15.0 ± 0.5 cm in diameter and 20 cm long, unless a longer bar would cause greater damage…”. The most damaging puncture bar length can be estimated by iterative processes in numerical simulations. On the one hand, a sufficient puncture bar length has to guarantee that shock absorbers or other attachments do not prevent or reduce the local load application to the package, on the other hand, a longer and thus less stiff bar causes a smaller maximum contact force. The contrary influence of increasing puncture bar length and increasing effective drop height shall be taken into account if a shock absorber is directly placed in the target area. The paper presents a numerical approach to identify the bar length that causes maximum damage to the package. Using the example of two typical package masses the sensitivity of contact forces and puncture bar deformations to the initial length are calculated and assessed with regard to the international IAEA package safety requirements.
Testing and numerical simulation of elastomeric seals under consideration of time dependent effects
(2016)
Due to delays in the siting procedure to establish a deep geological repository for spent nuclear fuel and high level waste and in construction of the already licensed Konrad repository for low and intermediate level waste, extended periods of interim storage will become more relevant in Germany. BAM is involved in most of the cask licensing procedures and is responsible for the evaluation of cask-related long-term safety issues. Elastomeric seals are widely used as barrier seals for containers for low and intermediate level radioactive waste. In addition they are also used as auxiliary seals in spent fuel storage and transportation casks (dual purpose casks (DPC)).
To address the complex requirements resulting from the described applications, BAM has initiated several test programs for investigating the behavior of elastomeric seals. These include experiments concerning the hyperelastic and viscoelastic behavior at different temperatures and strain rates, the low temperature performance down to -40°C, the influence of gamma irradiation and the aging behavior.
The first part of the paper gives an overview of these tests, their relevant results and their possible impact on BAM’s work as a consultant in the framework of approval and licensing procedures.
The second part presents an approach of the development of a finite element model using the finite element code ABAQUS®. The long-term goal is to simulate the complex elastomeric behavior in a complete lid closure system under specific operation and accident conditions.
Due to delays in the siting procedure to establish a deep geological repository for spent nuclear fuel and high level radioactive waste as well as in construction of the already licensed Konrad repository for low and intermediate level radioactive waste, extended periods of interim storage become more relevant in Germany. BAM is involved in most of the cask licensing procedures and especially responsible for the evaluation of cask-related long-term safety issues.
The long-term performance of elastomer seals for lid systems of transport and storage casks, whether used as auxiliary seals in spent fuel casks or as primary seals for low and intermediate level waste packages, is an important issue in this context. The polymeric structure of these seals causes a complex mechanical behavior with time-dependent sealing force reduction.
The results of a comprehensive purpose-designed test program consisting of basic compression and tension tests as well as relaxation tests on unaged specimens of representative types of elastomers (fluorocarbon rubber (FKM) and ethylene propylene diene rubber (EPDM)) at different temperatures and strain rates are presented. They were used to identify the constitutive behavior and to obtain parameters for finite element material models provided by the computer code ABAQUS®. After estimating the influence of uncertainties such as Poisson’s ratio and friction coefficient by sensitivity analyses, the chosen parameters had to prove their suitability for the finite element simulation of the specimen tests themselves.
Based on this preliminary work the simulation of a specific laboratory test configuration containing a typical elastomer seal with circular cross section is presented. The chosen finite element material model and the implemented parameters had to show that they are able to represent not only the specimen behavior under predominantly uniaxial load but also the more complex stress states in real components. Deviations between the measured and calculated results are pointed out and discussed.
For the consideration of long-term effects in the simulation of elastomer behavior, test results of aged specimens are needed. First information about a new test program, started recently and planned to provide these data, are given.
The excellent mechanical properties of elastomer seals at a wide range of temperatures as well as their high versatility and recovery potential under several load conditions make these materials well suitable for the application in containers designed for transport and disposal of negligible heat generating radioactive waste. While a seal exchange at defined intervals is typical in many conventional applications, it is impossible or at least hard to perform when principles of minimization of radiation exposure have to be considered which prohibit an avoidable cask handling. An extensive knowledge of the change of the elastomer properties during aging and the availability of reliable end-of-lifetime criteria to guarantee the safe enclosure of the radioactive material for the required time are mandatory. As BAM is involved in most of the national cask licensing procedures and in the evaluation of cask-related long-term safety issues, great efforts have already been made and are still ongoing to scientifically support this task.
Among other representative types of elastomers, specimen made from ethylene propylene diene rubber (EPDM) were tested before, during and after aging to capture the with respect to application most important of their complex mechanical properties.
Exemplary results of these investigations were used to calibrate material models implemented in the commercial finite element software ABAQUS/Standard®. The finite element model already presented in previous works uses a sequential temperature displacement coupling. The calculated compression stress relaxation (CSR) and compression set (CS) values do satisfactorily match the experimental results.
In many investigations performed at BAM both values (CSR and CS) were identified as key indicators of elastomer’s long-term performance.
However, the possibility to correlate these equivalent indicators with performance values such as tightness and leakage rate, measurable in the mounted state, is an important goal of our future work. In the presented study the ABAQUS® feature of “pressure penetration” is introduced in the suggested finite element model for this purpose. It provides the possibility to simulate the penetration of a gas into a possible gap between flange and O-ring causing an opening of a leakage path. Three dimensional and axis-symmetric finite element models were generated to represent flat and grooved flanges of different dimensions.
The sensitivity of the feature to several input parameters is investigated and the observed behavior of the O-ring is correlated with the results of performed leakage tests.
Elastomer seals are used in many industrial applications due to their excellent mechanical properties at a wide range of temperatures. Their high versatility and recovery potential under several load conditions make them well suitable for the application in containers designed for transport, storage and/or disposal of radioactive materials. In containers for low and intermediate level radioactive waste, elastomer seals are used as barrier seals, and as auxiliary seals in storage and transportation casks (dual purpose casks) for heat generating radioactive waste, such as spent fuel and high-level waste. While a seal exchange at defined intervals is typical in many conventional applications, it is impossible or at least hard to perform when principles of minimization of radiation exposure have to be considered and prohibit an unnecessary cask handling. An extensive knowledge of the change of the elastomer’s properties during aging and the availability of reliable end-of-lifetime criteria to guarantee the permanent safe enclosure of the radioactive material is mandatory. As BAM is involved in most of the national cask licensing procedures and in the evaluation of cask-related long-term safety issues, great efforts have been already made and are still planned to scientifically support this task.
Compression stress relaxation and compression set were identified as key indicators of elastomer long-term performance and quantitatively investigated in comprehensive test programs. Among other representative types of elastomers, specimens made from ethylene propylene diene rubber (EPDM) were tested before, during and after aging to capture the most important of their complex mechanical properties.
In the presented study, exemplary results were used to simulate the compression stress relaxation and the compression set of elastomer O-rings during aging. Regarding the influence of temperature, the time-temperature superposition principle is applied in the relaxation analysis of elastomer O-rings. The proposed model is implemented in the commercial finite element software ABAQUS/Standard® [1] with a sequential temperature displacement coupling. Numerical results match the experimental compression stress relaxation measurements well. The prediction of compression set values after long-term aging shows a relatively good agreement with the experimental results. Nevertheless, all input parameters derived from the specimen tests, additional assumptions concerning boundary conditions and modeling strategy are discussed with regard to the identified slight discrepancies.
The possibility to extend the finite element model to represent the O-ring seal’s ability to recover after a (fast) partial release is taken into account.
Influence of impact angle and real target properties on drop test results of cubic containers
(2017)
Drop test scenarios with cubic containers without impact limiters at interim storage sites or in a final repository have been investigated by numerical simulations. An ideally flat drop is impossible to conduct as a free fall of a container even under laboratory conditions. Dynamic stresses and strains inside the container structure are sensitive to the impact angle. Even very small impact angles cause remarkable changes in the experimental or numerical results when a flat bottom or wall of a container hits a flat target. For drop tests with transport packages the International Atomic Energy Agency (IAEA) regulations define an essentially unyielding target. In contrast, potential accident scenarios for storage containers are derived from site-specific safety analyses or acceptance criteria in Germany. Each interim storage site or repository has a yielding or so-called real target with individual structural and material properties. The real target acts as a kind of impact limiter. A more conservative container design is required if the impact limiting effect of the target is not considered.