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New interpretation approaches for seizure load tests on the translatory oscillation tribometer (SRV)
(2016)
When looking in detail at analyses of the tribological load-carrying capacity of high-performance lubricants, it becomes apparent that the stop of the machine of an exclusive evaluation of the development of the coefficient of friction cannot provide any sufficient criteria for determining the occurrence of adhesive failure. This is due on the one hand to the increasing complexity of lubricant formulae and sophisticated additive packages, and on the other hand to the increasing frictional power capacity of modern drive and control concepts in the design of tribometers. For this reason, it is urgently needed to examine the adhesive processes and their detection in more detail with the help of appropriate tribological values and criteria. The evolution of the friction can be coupled with the stroke, contact resistant and/or noise emission. Besides from new criteria for adhesive failure, which were compiled by the work group for the relevant ISO, DIN and ASTM standards, this contribution discusses the inclusion of additional parameters. Among other things, it provides guidance on what evidence the continuous recording of the original coefficient of friction and position signals, the electrical contact resistance, temperature, noise emission, frictional power input of the machine and further derived parameters help to identify adhesive failures or events.
Purity statements of high purity materials serving as primary standards by GDMS.
Primary standards are materials known for their total purity and therefore appropriate to realise the link with the International System of Units (SI). The realisation and dissemination of primary standards is of fundamental importance for comparability of measurement results through traceability in all fields of chemical analysis.
To serve as a primary standard for element determination the total purity of a high purity material needs to be measured. In order to achieve a sufficiently small uncertainty (i.e. < 0.01%) this involves determining all possible impurity contributions and to subtract their sum from the ideal purity of 100%.
GD-MS has the potential to reduce the effort for purity determination, as a fast sensitive multi-element analysis without extensive sample preparation. Similar to other solid sampling techniques, glow discharge
requires calibration link the measured signal and the content of the impurities in the matrix.
The use of the concept Relative Sensitivity Factors (RSFs) provides good approximations especially for high purity materials. However, it only works with a wide uncertainty of the results.
The preparation of synthetic pressed powder samples by different modifications of liquid and powder doping used for the determination of both metallic and none-metallic impurities are described. Efficient determination of metallic impurities by GD-MS via differential and absolute measurements with a significantly reduced target uncertainty of 20 % for absolute measurements using liquid doped pressed powder calibration could be achieved. The determination of impurities has been evaluated by independent analytical methods such as HR-ICP-MS, ETAAS; CGHE and combustion analysis
Etwa 25% aller weltweit produzierten Nahrungsmittel sind mit Schimmelpilzgiften (Mykotoxinen) kontaminiert. Dies birgt nicht nur gesundheitliche Risiken sondern verursacht auch hohe wirtschaftliche Verluste. Daher werden in der EU seit Jahren Anstrengungen unternommen, die Mykotoxin-Analytik voranzutreiben und Grenzwerte zu etablieren. Im Vortrag werden aktuelle Trends der Mykotoxin-Analytik und entsprechende Bedarfe präsentiert. Neben einer verbesserten Verfügbarkeit rückführbarer nativer und isotopenmarkierter Standards treten verstärkt maskierte Mykotoxine in den Fokus.
Tribological profile of hydraulic oils by using SRV. The determination of a set of critical, tribological by using different SRV-based test methods. The SRV-based concept of tribological profile generates the wear volumes on two triboelements (specimen), the extreme pressure properties and friction under different contact pressures.
Thus, the benchmark and validation of hydraulic oils bear on a wider range of tribological properties.
The RR2016 extends with six hydraulic oils to other base oil types including biodegradable fluids, which were all tested according to ASTM D7043 in order to consolidate the correlation between SRV and V104C.
Actions from the meeting in April 2016: 1. Four SAC test methods are in place and were revised: SH/T 0721 (Grease, coefficient of friction and wear), SH/T 0784 (Grease, pass load/O.K. load), SH/T 0847 (Oil, coefficient of friction and wear) and SH/T 0882 released by 11-2014 (Oil, pass load/O.K. load). 2. New test method to evaluate anti-fretting properties of greases based was approved by SAC TC280 and will be released. 3. SAC TC280 accepted the project “Simulation of synchronizer by using SRV”. Draft text to be submitted by 03-2017. Discussions on a parallel ASTM test method. 4. A procedure for “Wear Volume” is under development for SAC TC280.
„Cliff“-testing by using SRV
The identification in engine or gear tests of the induction time or off-set point („cliff“), after which wear and friction increased.
“Cliff” testing as auxiliary method supports the interpretation of engine tests, as it enhances the values of expensive engine tests, because it enables correlations between friction & wear, either from engine or in SRV tests, with additive depletion, oxidation, viscometrics and dispersancy/detergency.
Oil samples taken in discrete intervals and “Cliff” tested monitors the evolution of tribological and functional properties versus engine running time. “Cliff” testing by using SRV is a purposeful tool in order to secure and accelerate metallurgical developments and the development of lubricant formulations.
Over the last couple of years a lot of effort was put into the development of internationally recognized standards for fireworks. The work is globally organized within the ISO/TC 264 “Fireworks”. This technical committee consists of five working groups (WGs), set up for the development of criteria for safety requirements, test methods and labelling of fireworks articles:
WG1: Terminology
WG2: Safety requirements and labelling
WG3: Categories and types
WG4: Test methods
WG5: Fireworks display
The Bundesanstalt für Materialforschung und -prüfung (BAM) was from the beginning part of the entire standardization activities and participated actively with experts in all WGs, project leadership and provided the chairman for the ISO/TC 264-WG2 “Safety requirements and labelling”. This paper aims at giving an overview about the meetings, the philosophy behind the chosen standardization approaches and selected information on safety requirements, test methods and labelling aspects.
Additive Manufacturing provides an important enabling technology for the digital transformation of the economy. As an emerging technology it has seen a remarkable development over the last three decades. Nevertheless, it is far from a broad adoption with several barriers to overcome yet. One of the major challenges is the lack of standards. The critical role of standardization for innovation is generally recognized, still the topic too often has been neglected in strategic roadmapping exercises for emerging technologies. Too little is known about the complex dynamics and interrelations of standardization and innovation. The anticipation of standardization needs and the timely and efficient implementation of standards is challenging. This paper aims at contributing to a better understanding of the role that standards play in the multi-dimensional system of innovation. It analyzes the trajectories of innovation in Additive Manufacturing in a systematic and holistic way, focusing on standardization activities with regard to coordination, stakeholders involved, the timing and types of standards developed. Putting standardization in context of the multi-dimensional innovation system of Additive Manufacturing the research shows where standards can support the diffusion of an emerging technology.
Additive Manufacturing provides an important enabling technology for the digital transformation of the economy. As an emerging technology it has seen a remarkable development over the last three decades. Nevertheless, it is far from a broad adoption with several barriers to overcome yet. One of the major challenges is the lack of standards. The critical role of standardization for innovation is generally recognized, still the topic too often has been neglected in strategic roadmapping exercises for emerging technologies. Too little is known about the complex dynamics and interrelations of standardization and innovation. The anticipation of standardization needs and the timely and efficient implementation of standards is challenging. This paper aims at contributing to a better understanding of the role that standards play in the multi-dimensional system of innovation. It analyzes the trajectories of innovation in Additive Manufacturing in a systematic and holistic way, focusing on standardization activities with regard to coordination, stakeholders involved, the timing and types of standards developed. Putting standardization in context of the multi-dimensional innovation system of Additive Manufacturing the research shows where standards can support the diffusion of an emerging technology.
Standardization for the Industrial Internet of Things: Engagement by China, Germany and the USA
(2018)
Standardization is a major challenge for a successful digital transformation of manufacturing. Industry and governments have put this topic on their agenda and stakeholders worldwide are engaged in various Standard Development Organizations, consortia and fora, seeking to shape the standards for the Industrial Internet of Things (IIoT). This paper for the first time analyzes how well participants from the USA, China and Germany are actually represented and engaged in standards development for the IIoT. Using quantitative metrics, the study specifically investigates standardization activities for Wireless Sensor Networks at the Internet Engineering Taskforce (IETF). The results are divergent: Measuring the authorships of IETF Internet-Drafts, China’s successful catch-up in international standardization is confirmed, having even outperformed the USA. When it comes to the authorship of the actual standards at IETF, China could not assert its top position. Here, US authors are leading, followed by German participants. The paper discusses different engagement patterns in depth and analyzes the national economic, institutional and political backgrounds that influence them.