Ingenieurwissenschaften und zugeordnete Tätigkeiten
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The microstructure has a great influence on short fatigue crack growth in metallic materials. Laser-based Powder Bed Fusion AlSi10Mg alloys exhibit in the as-built condition a fine fibrous Si structure and a supersaturated solid solution of Si in the α-Al matrix, which is significantly modified by heat treatments starting already at temperatures under 260 °C. This study focuses on the influence of post-process heat treatments on the microstructural evolution and the resulting fatigue crack growth resistance. As compared to the as-built condition, two heat treatments at 265 °C/1 h and at 300 °C/2 h are found to be beneficial to the fatigue crack growth resistance of the investigated material.
Oxide thermoelectric semiconducting materials like p-type calcium cobaltite Ca3Co4O9 are investigated as oxidation- and temperature-resistant thermoelectric materials for thermoelectric generators (TEGs). To realize TEGs in planar film technology, the powder aerosol deposition (PAD) method is emerging recently. PAD is a method to obtain dense ceramic films directly from the synthesized starting powders without a subsequent high temperature step.
In the present work, Ca3Co4O9 (CCO) powders are processed by PAD to ceramic films at room temperature. The thermoelectric properties of the films (film thickness 10 – 20 µm) are characterized from room temperature to 900°C. Additionally, the layer morphology and texture of the films will be investigated.
As result, the Seebeck coefficient of the CCO-PAD film is comparable to pressed and sintered CCO-bulk materials during the 1st heating cycle to 900°C. The morphology of the films after the thermal treatment shows strong aligned crystallites resulting in a strong texture of the films. The electrical conductivity increases strongly during the 1st heating cycle to 900°C and stays almost constant afterwards. Compared to CCO-bulks, the films provide higher electrical conductivity which could be explained by the oriented crystal growth in-plane direction of the film.
The relationship between thermoelectric properties and layer morphology as a function of thermal annealing parameters will be further investigated.
The present research focuses on the weldability of PBF-LB/M lattice structure parts of Inconel 718 by means of laser beam welding. The integration of complex and lightweight AM structures into assemblies employing conventional joining methods is challenging. During the welding process, dissipation of the laser heat input through thin-walled structures of these lightweight structures is strongly limited, resulting in heat accumulation, atypical cooling rates, and affecting weld geometry, quality of the joint and microstructure. PBF-LB/M parts have been manufactured in three characteristic build directions. They were all stress relieved, then a group of them were submitted to an additional solution annealing and the second group to a two-step aging treatment. Afterwards, these parts were welded to identical PBF-LB/M parts and to wrought ones in butt position. To gain insight into the welding temperature field and to explain segregation mechanisms, grain growth and asymmetries, thermocouples have been attached on the surface’s regions and struts nearby. Joining a lattice structure with a full material wrought sample results in clear asymmetric welds due to dissimilar heat dissipation on both sides of the seam. Selected pre-weld heat treatments have a crucial influence on the quality of the seam on the AM part.