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Differential Scanning Calorimetry (DSC) may be used to avoid testing for explosive and self-reactive properties according to the legal regulations of chemicals substances and dangerous goods.
Demonstrated measured exothermic decomposition energy value significantly affected by numerous factors - choice of sample vessel, sample mass, baseline shape, peak shape, heating rate.
This is a short review on ongoing work and interests in Division 2.6 of BAM with a focus on transport regulations and related testing. The behaviour of primer caps in different packaging configurations is addressed and the new apparatus for the "Minimum Burning Pressure" test is presented. Further topics regarding classification are touched with the aim to attract comments and stimulate cooperation internationally.
The safety characteristics of flammable gases and liquids are required when identifying potentially explosive mixtures and taking appropriate actions concerning explosion protection. Examples are given in this review of the safe handling and evaluation of hazards during the processing, storage, transport, and disposal of flammable liquids and gases. The CHEMSAFE database is presented as a reliable source of safety characteristic data, and ist new open-access version is introduced. CHEMSAFE currently contains assessed properties for about 3000 flammable liquids, gases and mixtures. The lack of a broad experimental foundation in the extensive field of non-atmospheric conditions shows the need for further investigation and standardization. This review summarizes experimental evidence and estimation methods for safety characteristic data under non-atmospheric conditions pointing out current limitations. Suggestions for pre-normative research on safety data under nonatmospheric conditions are given.
Polymerizing Substances
(2017)
Polymerizing substances are classified in different classes of the UN Recommendations on the Transport of Dangerous Goods. Based on incidents a new division 4.1 for polymerizing substances, which are not meet the criteria of the Classes 1-8, was implemented in the regulations. In the lecture, the criteria and the determination of the SAPT (self-accelerating polymerization temperature are discussed.