5 Werkstofftechnik
Filtern
Erscheinungsjahr
Dokumenttyp
- Zeitschriftenartikel (416)
- Vortrag (384)
- Posterpräsentation (104)
- Beitrag zu einem Tagungsband (60)
- Forschungsdatensatz (27)
- Buchkapitel (6)
- Dissertation (4)
- Beitrag zu einem Sammelband (3)
- Sonstiges (2)
- Preprint (2)
Sprache
- Englisch (1010) (entfernen)
Schlagworte
- Additive Manufacturing (69)
- Additive manufacturing (66)
- Corrosion (56)
- Microstructure (43)
- Ontology (39)
- Glass (38)
- Creep (36)
- Transmission electron microscopy (30)
- EBSD (28)
- Fatigue (27)
- Ceramic (19)
- Sintering (19)
- Ceramics (18)
- Crack growth (18)
- CCS (17)
- Residual stress (17)
- Crystallization (16)
- Degradation (16)
- Steel (16)
- High entropy alloys (14)
- 316L (13)
- Oxidation (13)
- High temperature corrosion (12)
- Nanoparticles (12)
- Scanning electron microscopy (12)
- Aging (11)
- CALPHAD (11)
- CCUS (11)
- Carbon steel (11)
- Crystal plasticity (11)
- FAIR (11)
- Mechanical properties (11)
- Ti-6Al-4V (11)
- 3D printing (10)
- CO2 (10)
- Coarsening (10)
- Electron microscopy (10)
- High entropy alloy (10)
- Metallic glass (10)
- Neutron diffraction (10)
- Alloy 2618A (9)
- Diffraction (9)
- Digitalization (9)
- EN AW-2618A (9)
- Glass fiber reinforced polymers (9)
- Impurities (9)
- Laser powder bed fusion (9)
- SEM (9)
- Slurry (9)
- Water speciation (9)
- X-ray diffraction (9)
- AGIL (8)
- Alumina (8)
- Aluminium (8)
- DCB (8)
- Fatigue crack growth (8)
- Fractography (8)
- Geothermal (8)
- High-temperature corrosion (8)
- Hydrogen (8)
- Machine Learning (8)
- Martensitic steel (8)
- Nickel-base superalloys (8)
- Thermoelectrics (8)
- AISI 316L (7)
- Aluminium alloy (7)
- Anisotropy (7)
- Data Interoperability (7)
- Heat treatment (7)
- Laser Powder Bed Fusion (7)
- Layerwise slurry deposition (7)
- Mechanical testing (7)
- Metallic glasses (7)
- Residual Stress (7)
- Robotic melting (7)
- S-phase (7)
- Semantic Interoperability (7)
- Simulation (7)
- Soda-lime silicate glass (7)
- Sulfidation (7)
- TEM (7)
- Viscosity (7)
- Water content (7)
- Bioactive glass (6)
- CO2 quality (6)
- Computed Tomography (6)
- Environmental stress cracking (6)
- Environmental stress cracking (ESC) (6)
- Foaming (6)
- LTCC (6)
- Lattice parameters (6)
- Low Cycle Fatigue (6)
- Nanoindentation (6)
- Particle size (6)
- Plasticity (6)
- Powder (6)
- Selective laser melting (6)
- Semantic Web Technologies (6)
- Supercritical/dense phase CO2 (6)
- Thermomechanical fatigue (6)
- Vickers (6)
- Wind turbine blades (6)
- CCU (5)
- Carbon capture (5)
- Carbon steels (5)
- Creep behavior (5)
- Damage (5)
- Data mapping (5)
- Dislocation (5)
- Droplet corrosion (5)
- Electron backscatter diffraction (5)
- FAIR data (5)
- FAIR data management (5)
- Fe-Al alloys (5)
- Fracture (5)
- High alloyed steel (5)
- High-density polyethylene (5)
- In situ (5)
- Inconel 686 (5)
- Intermetallics (5)
- Iron aluminides (5)
- Knowledge Representation (5)
- Knowledge graph and ontologies (5)
- LCF (5)
- Low cycle fatigue (5)
- Microstructure evolution (5)
- Modeling (5)
- Non-destructive testing (5)
- P92 (5)
- PMD Core Ontology (5)
- Phase-field simulation (5)
- Pipeline (5)
- Pipeline network (5)
- Plastic deformation (5)
- Plattform MaterialDigital (5)
- Polymer (5)
- Polymer matrix composites (5)
- Reference data (5)
- Sandwich (5)
- Shear modulus (5)
- Single crystal (5)
- Stress relaxation (5)
- Structure (5)
- Superalloy (5)
- Superaustenite steel (5)
- Tensile testing (5)
- Texture (5)
- ToF-SIMS (5)
- Transmission electron microscopy (TEM) (5)
- VSSA (5)
- Vickers indentation (5)
- X-ray refraction (5)
- Young's modulus (5)
- 3D-printing (4)
- AISI 304L (4)
- Additive Fertigung (4)
- Alkali ions (4)
- Alkali zinc borate glasses (4)
- Aluminum alloys (4)
- Binder Jetting (4)
- Biodiesel (4)
- Brinell hardness (4)
- Calcination (4)
- Calcium cobaltite (4)
- Carbon capture storage (4)
- Carbon dioxide (4)
- Characterization (4)
- Coating (4)
- Composite (4)
- Compositionally complex alloys (4)
- Computed tomography (4)
- Concrete (4)
- Crack healing (4)
- Crack propagation (4)
- Crack tip opening displacement (4)
- Crystal orientation (4)
- Deuterium (4)
- Diesel (4)
- Diffusion (4)
- EXAFS (4)
- Elastic modulus (4)
- Electron Backscatter Diffraction (4)
- Finite element analysis (4)
- Fracture toughness (4)
- Full Notch Creep Test (4)
- Full notch creep test (FNCT) (4)
- GD-OES (4)
- Glas (4)
- Grain boundaries (4)
- HIP (4)
- High Cycle Fatigue (4)
- High temperature (4)
- High-entropy alloy (4)
- High-entropy alloys (4)
- IN718 (4)
- In-space manufacturing (4)
- Inconel 718 (4)
- Internal friction (4)
- Joined nickel-based alloys (4)
- Kikuchi patterns (4)
- Martensite (4)
- Mechanical behavior (4)
- Microgravity (4)
- Microplastics (4)
- Microstrucrue Design (4)
- Microstructural characterization (4)
- Microstructure Design (4)
- Molecular dynamics (4)
- NTE (4)
- Orientation (4)
- PE-HD (4)
- Pattern matching (4)
- Pitting (4)
- Polyaniline (4)
- Precipitation (4)
- Raman spectroscopy (4)
- Recommendations (4)
- Research Data Management (4)
- Roughness (4)
- SIMS (4)
- Sample preparation (4)
- Scale-bridging (4)
- Scarf repairs (4)
- Self-healing (4)
- Spectroscopy (4)
- Spray drying (4)
- Steels (4)
- Surface energy (4)
- Tensile Test Ontology (4)
- Tensile test (4)
- Ultrasound (4)
- Virtual experiments (4)
- Welding (4)
- Whole-chain CCS scenario (4)
- Workflow (4)
- Zirconia (4)
- 3D-Printing (3)
- Ab-initio (3)
- Advanced ceramics (3)
- Aluminium Alloy (3)
- Aluminum alloy (3)
- Binder jetting (3)
- Bioceramics (3)
- Carbon Fiber Reinforced Plastics (3)
- Carbon fibres (3)
- Cement (3)
- Ceramic multilayer (3)
- Ceramic spring (3)
- Chemically complex alloy (3)
- Composites (3)
- Corrosion Fatigue (3)
- Corrosion fatigue (3)
- Coulomb explosion (3)
- Crack Propagation (3)
- Crack evolution (3)
- Creep data (3)
- Creep-fatigue (3)
- Dark-field transmission electron microscopy (3)
- Dark-field transmission electron microscopy (DFTEM) (3)
- Data Space (3)
- Defects (3)
- Deformation (3)
- Density-based Thermodynamics (3)
- Destabilization (3)
- Dielectric breakdown (3)
- Dielectric strength (3)
- Diffraction Enhanced Imaging (3)
- Digital image correlation (3)
- Digtial Representation (3)
- Diopside (3)
- Dynamics (3)
- Elastic constants (3)
- Electron-beam-induced modification (3)
- Electronic Lab Notebook (3)
- Environmental Stress Cracking (3)
- FIB (3)
- Ferritic-martensitic steels (3)
- Fracture Toughness (3)
- Fracture mechanics (3)
- Fracture surface (3)
- Fracture surface analysis (3)
- Full-Notch Creep Test (FNCT) (3)
- GFRP (3)
- General Materials Science (3)
- Glass ceramic (3)
- Glass powder (3)
- Glass transition (3)
- Glass-ceramic (3)
- Glass-ceramics (3)
- Gold nanoparticles (3)
- Grain boundary (3)
- Grain boundary engineering (3)
- Hardness (3)
- High Entropy Alloy (3)
- High temperature mechanical properties (3)
- ISRU (3)
- In situ tensile test (3)
- Interfacial strength (3)
- Interoperability (3)
- Iron (3)
- Iron oxide nanoparticles (3)
- Kikuchi diffraction (3)
- Kikuchi pattern (3)
- Knowledge graph (3)
- Laser (3)
- Laser ablation in liquid (3)
- Laser beam melting (3)
- Laser cladding (3)
- Laser scanning microscopy (LSM) (3)
- Lattice misfit (3)
- Layerwise Slurry Deposition (3)
- Li-ion battery (3)
- Lightweight materials (3)
- Lithium Ion Batteries (3)
- Mechanical Engineering (3)
- Mechanics of Materials (3)
- Metadata schema (3)
- Microhardness (3)
- Multilayer (3)
- NMR spectroscopy (3)
- Nano-powder (3)
- Nanomaterials (3)
- Neutron Diffraction (3)
- Nickel-based superalloys (3)
- Ontologies (3)
- Oxide Glasses (3)
- PBF-LB/M/316L (3)
- PMD (3)
- Permeability (3)
- Phase transformations (3)
- Phase-field (3)
- Polyethylene (3)
- Porosity (3)
- Pressure-assisted sintering (3)
- Recycling (3)
- Referenzdaten (3)
- Relaxation (3)
- Reproducibility (3)
- Residual Stresses (3)
- Residual stresses (3)
- Rotor blade (3)
- SLM (3)
- Scintillators (3)
- Selective Laser Melting (3)
- Semantic Data (3)
- Shape-memory alloys (3)
- Shear bands (3)
- SiO2 (3)
- Silicate Glasses (3)
- Silicon Carbide (3)
- Single-crystals (3)
- Slow crack growth (SCG) (3)
- Sol-gel (3)
- Sol-gel coating (3)
- Solid-state (3)
- Solubility (3)
- Stress intensity factor (3)
- Sulfiding (3)
- Superalloys (3)
- Surface crystallization (3)
- Syngle Crystal alloy (3)
- TDEP (3)
- Temperature (3)
- Tempered Martensite Ferritic Steels (3)
- Tempered martensite-ferritic steel (3)
- Tensile Test (3)
- Tensile data (3)
- Thermal expansion (3)
- Thermo-Mechanical Fatigue (3)
- Thermomechanics (3)
- Titanium (3)
- Titanium oxide (3)
- Topography (3)
- Transport (3)
- UV-irradiation (3)
- Utilization (3)
- Vickers hardness (3)
- Viscoplasticity (3)
- Wind turbine blade shells (3)
- XANES (3)
- XRD (3)
- µ-gravity (3)
- μ-gravity (3)
- AM (2)
- Adiabatic calorimeter (2)
- Ageing (2)
- Agglomerates (2)
- Aggressive environment (2)
- Air-coupled ultrasonic testing (2)
- Airborne ultrasonic testing (2)
- Al2O3 (2)
- Alloy design (2)
- Aluminosilicate glasses (2)
- Analysis (2)
- Annealing (2)
- Aquifer (2)
- Atom probe tomography (2)
- Austenitic stainless steel (2)
- Austenitic steel 316L (2)
- Automation (2)
- Bacteria (2)
- Bi-material structure (2)
- Biaxial strength (2)
- Bio Ceramics (2)
- Bioactive Glass (2)
- Bioactivity (2)
- Biofilm (2)
- Bond energy (2)
- Bone regeneration (2)
- Brittle fracture (2)
- Bulk metallic glasses (2)
- CO2-storage (2)
- Capture (2)
- Carbon (2)
- Carbon Fibre (2)
- Carbon capture and storage (2)
- Carbon storage (2)
- Casting (2)
- CeO2 (2)
- Ceria (2)
- Chemo-mechanical coupling (2)
- Chromium oxide (2)
- Coatings (2)
- Condensate (2)
- Condensation (2)
- Continnum damage model (2)
- Copper (2)
- Copper alloys (2)
- Corrosion resistance (2)
- CrCoNi (2)
- CrMnFeCoNi (2)
- Crack propagation analysis (2)
- Creep-Fatigue (2)
- Crevice corrosion (2)
- Crop protection products (2)
- Cross linking (2)
- Cure process (2)
- Cyclic softening (2)
- Data Management (2)
- Data Structures (2)
- Data analysis (2)
- Data management (2)
- Dataset (2)
- Debinding (2)
- Density-based Phase-Field Modelling (2)
- Density-based model (2)
- Densty-based Thermodynamics (2)
- Dental (2)
- Depth-profiling (2)
- Dielectric properties (2)
- Diffraction Elastic Constants (2)
- Diffraction contrast (2)
- Diffusion coefficient (2)
- Digital material representation (2)
- Digital representation (2)
- Digitization (2)
- Diopsid (2)
- Directional grain growth (2)
- Dislocations (2)
- Dispersion process (2)
- Distribution function (2)
- Ductile iron (2)
- Dynamic mechanical analysis (DMA) (2)
- EDX (2)
- EDXRD (2)
- Early oxidation (2)
- Elastic microstructure (2)
- Elasticity (2)
- Electron beam induced modification (2)
- Electron beam-induced fragmentation (2)
- Electron diffraction (2)
- Electron energy (2)
- Energy distribution (2)
- Environmentally assisted cracking (2)
- Epoxy (2)
- FAIR Data Management (2)
- Fatigue damage (2)
- Fatigue of sandwich shell structures (2)
- Fatigue performance (2)
- Fatigue testing (2)
- FeCr- alloys (2)
- Ferroelectret (2)
- Fiber reinforced polymer (2)
- Flowability (2)
- Fluoride phosphate glasses (2)
- Fracture Surface Analysis (2)
- Fracture surface energy (2)
- Fungi (2)
- Gender gap (2)
- Gitterkonstanten (2)
- Glass Digital (2)
- Glass composition (2)
- Glass matrix composite (2)
- Gold (2)
- Granules (2)
- HEA (2)
- Hard machining (2)
- Heat Treatment (2)
- High Alloyed Steel (2)
- High Entropy Alloys (2)
- High Temperature Corrosion (2)
- High Temperature Testing (2)
- Hot pressing (2)
- Hot stage microscopy (2)
- Hydrogen permeation (2)
- IR (2)
- Imaging techniques (2)
- In-situ (2)
- Inconel 625 (2)
- Infrared spectroscopy (2)
- Infrastructure (2)
- Injection (2)
- Interfacial shear strength (2)
- Interphase (2)
- Inverted classroom (2)
- Ionic porosity (2)
- Kikuchi (2)
- Knowledge Graph (2)
- LPBF (2)
- LSD-print (2)
- Laminography (2)
- Laser Powder Bed fusion (2)
- Lattice distortion (2)
- Layerwise (2)
- Lead borate glasses (2)
- Liquid-metal embrittlement (2)
- Long-term behavior (2)
- Long-term storage (2)
- Lorenz transmission electron microscopy (2)
- Lunar habitat (2)
- Lunar regolith (2)
- Lunar regolith simulant (2)
- MEA (2)
- MOUSE (2)
- Manganese oxide (2)
- Manufacturing (2)
- Mars (2)
- Martensitic transformation (2)
- Mass transport (2)
- Material degradation (2)
- Material digital (2)
- MaterialDigital (2)
- Materials Modelling (2)
- Materials science (2)
- Medium Entropy Alloys (2)
- Melt pool boundary (2)
- Metal seal (2)
- Micro-shrinkages (2)
- Micromechanical model (2)
- Microstructural analysis (2)
- Microstructural evolution (2)
- Microstructure analysis (2)
- Microstructure and texture (2)
- Microstructure-property-correlation (2)
- Mikrostruktur (2)
- Mixed Ca-K-Na phosphates (2)
- Mixed gas atmosphere (2)
- Mobility (2)
- Monte-Carlo Simulation (2)
- Multifunctional nanoparticles (2)
- Multilayer technology (2)
- NDT (2)
- NFDI (2)
- NMR (2)
- Na and K rhenanites (2)
- Nano powder (2)
- Nanostructure quantification (2)
- Native oxide (2)
- Nickel alloys (2)
- Nickel-base alloy (2)
- Nickel-based alloys (2)
- Niobium alloying (2)
- Notches (2)
- Nucleation (2)
- Ontologie (2)
- Ontology development (2)
- Orientation precision (2)
- Oriented surface crystallization (2)
- Ostwald ripening (2)
- Oxidation behavior (2)
- Oxyfuel (2)
- PMDco (2)
- Particle morphology (2)
- Paving (2)
- Persistent luminescence (2)
- Phase change material (2)
- Phase diagram (2)
- Phase separation (2)
- Phase transformation (2)
- Phase-Field Simulation (2)
- Phase-Field Simulations (2)
- Phasenidentifikation (2)
- Photon counting detector (2)
- Plattform Material Digital (2)
- Polyethylene, PE-HD (2)
- Polymer Matrix Composites (2)
- Porcelain (2)
- Pores (2)
- Preceramic polymer (2)
- Pressure assisted sintering (2)
- Process monitoring (2)
- Protective coating (2)
- Push-out Test (2)
- Quasicrystal (2)
- Rapid solidification (2)
- Ratio refinement (2)
- Reaction sintering (2)
- Reaction-sintering (2)
- Reference Data (2)
- Reference material (2)
- Refractory high entropy alloys (2)
- Ressidual stress (2)
- Review (2)
- Round robin (2)
- S-Phase (2)
- S355 steel sheet (2)
- SAXS (2)
- Safety assessment (2)
- Salt eutectics (2)
- Scanning transmission electron microscopy (STEM) (2)
- Semantic Representation (2)
- Semantic web (2)
- Short-range order (2)
- Sibayak (2)
- Silicon carbide (2)
- Silicon nanowires (2)
- Silver diffusion (2)
- Silver metallization paste (2)
- Silver nanoparticle (2)
- Silver-glass-metallization-paste (2)
- Simulation of concrete (2)
- Single-Crystal (2)
- Sintering additives (2)
- Slow crack growth (2)
- Small-angle scattering (2)
- Soda-lime-silica glass (2)
- Solar sintering (2)
- Sorption (2)
- Space (2)
- Spring constant (2)
- Stainless steel (2)
- Standard (2)
- Standardization (2)
- Starch (2)
- Starch nanoparticle (2)
- Storage (2)
- Strength (2)
- Stress corrosion cracking (2)
- Sulphidation (2)
- Superconducting magnet (2)
- Supercritical CO2 (2)
- Surface (2)
- Surface Energy (2)
- Surface nucleation (2)
- Surface treatments (2)
- Synchrotron Tomography (2)
- Synchrotron radiation (2)
- Synthetic air (2)
- TED-GC-MS (2)
- Tensile Properties (2)
- Tensile properties (2)
- Thermal Spray (2)
- Thermal energy storage (2)
- Thermodynamics (2)
- Thermoelectric (2)
- Thermoelectric oxide (2)
- Thermoelectric oxides (2)
- Thermoelectric properties (2)
- Thermography (2)
- Thermogravimetry (2)
- Thermoplastic (2)
- Thermoset polymers (2)
- Toughness (2)
- Transmission electron microscope (TEM) (2)
- Transparent ceramics (2)
- Two Photon Polymerization (2)
- Under cyclic loading (2)
- Upconversion (2)
- Utilization, and storage (CCUS) technology (2)
- Viscous sintering (2)
- Volume specific surface area (2)
- Wall thickness (2)
- Water-based (2)
- Weibull Distribution (2)
- Weibull distribution (2)
- Wetting (2)
- Wind energy (2)
- Wind turbine (2)
- Wood protection (2)
- Workshop (2)
- X-Ray Diffraction (2)
- X-ray absorption spectroscopy (2)
- X-ray computed tomography (CT) (2)
- X-ray laminography (2)
- Zero-g (2)
- corrosion (2)
- 12%Cr steel (1)
- 150 Years (1)
- 2PP (1)
- 316L stainless steel (1)
- 3D (1)
- 3D Reconstruction (1)
- 3D etching (1)
- 3D glass structure model (1)
- 3D imaging (1)
- 3D materialography (1)
- 3D-finite element modeling (1)
- 4-Dimensional scanning transmission (1)
- 5G (1)
- 9-12% Cr ferritic-martensitic steels (1)
- 9-12%Cr steel (1)
- AFM (1)
- ATZ (1)
- Abrasion (1)
- Accelerated integration scheme (1)
- Accelerated temporal integration (1)
- Accessible (1)
- Acid-leaching (1)
- Acids (1)
- Acoustic emission (1)
- Active thermography (1)
- Additive manufactured Ni-base superalloys (1)
- Adiabatic shear bands (1)
- Adolf Martens (1)
- Advanced high strength steels (1)
- Advanced manufacturing (1)
- Advanced wastewater treatment (1)
- Aerospace (1)
- Aggressive environement (1)
- Aggressive environments (1)
- Aggressive gases (1)
- Aging mechanisms (1)
- Al alloys (1)
- Al-Cu alloy (1)
- Al-Cu binary alloy system (1)
- Al-Cu-Li alloys (1)
- Al-Cu-Li-alloy (1)
- Al-Li alloys (1)
- Al2CuMg (1)
- Alcium alkali phosphate (1)
- Alkali aluminosilicate glasses (1)
- Alkali and alkaline earth silicate and borate glass (1)
- Alkali zinc borate glass (1)
- Alkali-activated materials (1)
- Alloy (1)
- Alloy 2818A (1)
- Alloy Safety (1)
- Alloy microstructure (1)
- Alloys (1)
- Alloys' Safety (1)
- Alpha-tricalcium phosphate (1)
- Alumina coatings (1)
- Alumina toughened zirconia (1)
- Aluminium alloys (1)
- Aluminum (1)
- Aluminum Alloy Aging (1)
- Amorphization (1)
- Amorphous silica (1)
- Analytical scanning electron microscopy (1)
- Analytical services (1)
- Angle measurement (1)
- Anhydrite (1)
- Approximant (1)
- Aquifer fluid (1)
- Artefact (1)
- Artificial weathering (1)
- Assemblies of gold nanoparticles (1)
- Atacama Desert (1)
- Atmospheric Plasma Spraying (1)
- Atmospheric plasma spraying (1)
- Atomic packing factor (1)
- Atomistic Simulation (1)
- Atomistic simulations (1)
- Atomization (1)
- Austenite-to-martensite phase transformation (1)
- Austenitic alloys (1)
- Austenitic cast iron (1)
- Austenitic steel (1)
- Austenitischer Stahl (1)
- Automatable digital approach (1)
- Automated Bragg angle determination (1)
- Automated analysis (1)
- Automated finite element analysis (1)
- Automated image analysis (1)
- Automatische Finite Element Simulation (1)
- Avalanches (1)
- BTEX (1)
- BTS (1)
- Bacterial attachment (1)
- Batch reactions (1)
- Behmite (1)
- Bimodal distribution (1)
- Binders/binding (1)
- Bio Ceramic (1)
- Bio active ceramic (1)
- Bio-ceramic engineering (1)
- Bioactive (1)
- Bioactive bone grafting material (1)
- Bioactive glass scaffold (1)
- Bioceramic (1)
- Biogeochemical cycling (1)
- Biogeochemistry (1)
- Biomineralisation (1)
- Biopolymer (1)
- Bioresorbable (1)
- Biosensor (1)
- Biphasic calcium phosphate (1)
- Bitter technique (1)
- Blended learning (1)
- Blähen (1)
- Bone marrow-derived mesenchymal stem cell (1)
- Borate (1)
- Borate glasses (1)
- Borosilicate glass (1)
- Bragg angles (1)
- Brass (1)
- Bravais lattice (1)
- Bravais lattices (1)
- Brazing (1)
- Breakdown strength (1)
- Brittle / ductile fracture behavior (1)
- Brown-rot fungi (1)
- Brownian motion (1)
- Bubble formation (1)
- Burst (1)
- Burst test (1)
- C. lap-shear (1)
- CALPHAD database analysis (1)
- CALPHAD databases analysis (1)
- CCUS, supercritical/dense phase CO2, carbon steels, martensitic steel, superaustenite steel, droplet corrosion (1)
- CFRP (1)
- CKAN (1)
- CLS (1)
- CO2 Corrosion (1)
- CO2 corrosion (1)
- CO2 pipeline transport (1)
- CO2 separation membranes (1)
- CO2-corrosion (1)
- Cabon capture and storage (1)
- Calcium Cobaltite (1)
- Calcium alkali orthophosphate materials (1)
- Calcium manganate (1)
- Calcium sulfates (1)
- Calculated intrinsic fracture toughness (1)
- Calibration (1)
- Cantor alloy (1)
- Carbide phase NbC (1)
- Carbidic austempered ductile iron (1)
- Carbon steels (1)
- Carbon Capture (1)
- Carbon Capture, Utilization and Storage (CCUS) (1)
- Carbon Fibers (1)
- Carbon capture, utilization and storage technology (1)
- Carbon fibre-reinforced-plastics (1)
- Carbon nanotubes (1)
- Casing (1)
- Catalogue of services (1)
- Cavitation (1)
- Ccs (1)
- CdTe quantum dots (1)
- Cellular substructure (1)
- Cellulose (1)
- Cement-based materials (1)
- Centrifugal casting (1)
- Ceramic layers (1)
- Ceramic multilayers (1)
- Ceramic nano particles (1)
- Ceramic springs (1)
- Ceramics 3D printing (1)
- Cerium oxide (1)
- Certification Standard 22 (1)
- Certified Referencematerial (1)
- Chalcogenides (1)
- Characterisation (1)
- Charpy test (1)
- Chemically Complex Alloy (1)
- Chemically complex alloys (1)
- Chemically complex materials (1)
- Chemometrics (1)
- Chromatography (1)
- Chromia (1)
- Chrystal orientation (1)
- Circular Economy (1)
- Clay ISRU (1)
- Co-axial monitoring (1)
- Co-firing (1)
- Co-segregation (1)
- Co-firings (1)
- Co2-Storage (1)
- Cobald based alloy (1)
- Coefficient of thermal expansion (1)
- Coherent x-ray scattering (1)
- Complex borides (1)
- Complex concentrated alloy (CCA) (1)
- Complex loading (1)
- Component assessment (1)
- Composite materials (1)
- Composite pressure vessels (1)
- Composite recycling (1)
- Composite structures (1)
- Composite testing (1)
- Compositionally complex alloy (1)
- Concrete 3D-printing (1)
- Condensed Matter Physics (1)
- Confined catalyst (1)
- Confocal laser scanning microscopy (LSM) (1)
- Coniophora puteana (1)
- Contact angle (1)
- Contact fatigue (1)
- Contact mechanics (1)
- Contamination (1)
- Cooling rate (1)
- Cooling simulations (1)
- Coordinate measurement machine (1)
- Copper vacancies (1)
- Corrosion and storage (CCUS) technology (1)
- Corrosion costs (1)
- Corrosion mechanism (1)
- Corrosion pits (1)
- Corrosion protection (1)
- Cow stress (1)
- Cr2O3 (1)
- CrN/NbN (1)
- Crack arrest (1)
- Crack growth in air (1)
- Crack initiation (1)
- Crack opening displacement (1)
- Cracks (1)
- Craze-crack mechanism (1)
- Craze–crack mechanism (1)
- Creation-relaxation algorithm (1)
- Creep anisotropy (1)
- Creep behaviour (1)
- Creep mechanisms (1)
- Creep strength (1)
- Creep under thermal cycling (1)
- Creep, Creep Rupture, and Stress Rupture (1)
- Creep-fatigue interaction (1)
- Critical energy release rate (1)
- Crop protection formulations (1)
- Cross-sectioning (1)
- Crosslinking (1)
- Cryogenic (1)
- Cryogenic cycling (1)
- Crystal Defects (1)
- Crystal Orientation (1)
- Crystal Plasticity Modelling (1)
- Crystal Texture (1)
- Crystal growth (1)
- Crystal growth velocity (1)
- Crystal lattice (1)
- Crystal lattice period (1)
- Crystal morphology (1)
- Crystalline defects (1)
- Crystallographic texture (1)
- Cubical Iron Oxide (1)
- Cubical shape (1)
- Cupriavidus metallidurans (1)
- Cuttlefish (1)
- Cycle jump (1)
- Cyclic R-Curve (1)
- Cyclic loading (1)
- Cyclic oxidation (1)
- Cyclic steam oxidation (1)
- Cytocompatibility (1)
- D. aging (1)
- D. creep D. viscoelasticity (1)
- DCB geometry (1)
- DED-L (1)
- DLS (1)
- Damage Behavior (1)
- Damage Tolerance (1)
- Damage behavior (1)
- Damage evolution (1)
- Damage mechanisms (1)
- Data Exchange (1)
- Data Fusion (1)
- Data Integration (1)
- Data Mapping (1)
- Data format (1)
- Data fusion (1)
- Data infrastructures (1)
- Data linking (1)
- Data pipeline (1)
- Data pipeline concept (1)
- Data processing (1)
- Data schema (1)
- Data space (1)
- Data storage (1)
- Data structure (1)
- Debonding (1)
- Deep Learning (1)
- Deep learning (1)
- Defect detection (1)
- Defect population (1)
- Defects engineering (1)
- Defects phase diagram (1)
- Defects thermodynamics (1)
- Deformation behavior (1)
- Deformation mechanisms (1)
- Degradation signatures (1)
- Demonstrators (1)
- Dense phase (1)
- Density (1)
- Density-based Model (1)
- Density-based phase-field modelling (1)
- Dental ceramics (1)
- Dentine (1)
- Deposition microstructure (1)
- Design of experiment (1)
- Desorption (1)
- Die casting (1)
- Dielectric Spectroscopy (1)
- Dielectric breakdown strength (1)
- Dielectric characterization (1)
- Diesel Fuel (1)
- Differential scanning calorimetry (1)
- Differential scanning calorimetry (DSC) (1)
- Diffusivity (1)
- Digital Image Correlation (1)
- Digital Transformation (1)
- Digital Twin (1)
- Digital representations (1)
- Digital workflow (1)
- Digital workflows (1)
- Digitalizations (1)
- Dimensional mismatch of crystalline lattice periods (misfit) (1)
- Discrete element method (1)
- Dislocation avalanches (1)
- Dislocation substructure (1)
- Disordered Assemblies (1)
- Disordered assemblies (1)
- Disorientation (1)
- Dissimilar metal weld (1)
- Dissolved water (1)
- Distributed fiber optic sensing (1)
- Distributed fiber optic sensors (1)
- Distributed fibre optic sensors (1)
- Diversity (1)
- Domain Ontology Development (1)
- Double notched creep specimen (1)
- Driving physical mechanism (1)
- Droplet (1)
- Dry preparation (1)
- Drying stress (1)
- Drywood termite (1)
- Dual-energy (1)
- Dual-material nickel-based alloys (1)
- Dwell periods (1)
- Dwell times (1)
- Dwell-Fatigue (1)
- Dynamic mechanical analysis (1)
- Dynamic recrystallization (1)
- Dynamisch Mechanische Analyse (1)
- EAC-1A (1)
- EASA (1)
- EC4SafeNano (1)
- EELS in STEM (1)
- EFTEM (1)
- EIS (1)
- EN AW 2618A (1)
- EN AW 2618A a (1)
- EPR (1)
- Early stages (1)
- Early sulfidation (1)
- Education (1)
- Efficiency (1)
- Elastic energy (1)
- Elastic properties (1)
- Elctronic Lab Notebook (1)
- Electric conductivity (1)
- Electric field distribution (1)
- Electric field strength (1)
- Electrical insulation (1)
- Electrical insulators (1)
- Electrical resistance (1)
- Electrochemical characterisation (1)
- Electrochemical deposition (1)
- Electrochemical dressing (1)
- Electrochemical impedance spectroscopy (1)
- Electromicroscopy (1)
- Electron Microscopy (1)
- Electron back-scattered diffraction (1)
- Electron backscattered diffraction (1)
- Electron backscattered diffraction (EBSD) (1)
- Electron beam-induced charging (1)
- Electron microscopy, transmission (1)
- Electronic (1)
- Electropolishing (1)
- Enamel (1)
- End of life (1)
- Endothelial progenitor cell (1)
- Endurance Limit (1)
- Environment (1)
- Environmental Stress Cracking (ESC) (1)
- Epitaxial films (1)
- Epoxy Resin (1)
- Epoxy resin (1)
- Equilibrium relaxation (1)
- Etching (1)
- European Centre (1)
- Eutectic (1)
- Expanding cavity model (1)
- Experimental and numerical techniques (1)
- Explosive welding (1)
- Exposed metal sites (1)
- FAIR Data (1)
- FAIR data. (1)
- FAIR principles (1)
- FAIR research data management (1)
- FCH JU (1)
- FIB Tomography (1)
- FNCT (1)
- FSDC (1)
- FT-IR (1)
- Fabrication (1)
- Fabrication method (1)
- Faceting (1)
- Facilitated activation (1)
- Failure mechanisms (1)
- Failure rate (1)
- Failure test (1)
- Fatigue Crack Growth (1)
- Fatigue Life Evaluation (1)
- Fatigue Testing (1)
- Fatigue crack propagation (1)
- Fatigue crack propagation stages (1)
- Fatigue fracture (1)
- Fatigue of sandwich structures (1)
- Fe-Mn steels (1)
- Feldspar (1)
- Fem (1)
- Female noble prize winners (1)
- Femtosecond laser (1)
- Ferritic Alloys (1)
- Ferritic steels (1)
- Ferritic–martensitic steel (1)
- Ferrous phosphate hydrate (1)
- Fiber (1)
- Fiber reinforced polymers (1)
- Fiber-matrix interface (1)
- Fiber/matrix bond (1)
- Fibre reinforced plastic (1)
- Fibre/matrix bond (1)
- Fibre/matrix bonding (1)
- Film depositition (1)
- Filters (1)
- Fine Powder (1)
- Finite element method (1)
- Finite elmenet simulation (1)
- Finite-Elemente-Methode (1)
- Finland (1)
- Firing (1)
- First derivative (1)
- First year students (1)
- Flipped classroom (1)
- Flow Coefficient (1)
- Fluorescence spectroscopy (1)
- Fluoride nanoparticles (1)
- Fluorolytic sol−gel (1)
- Focussed ion beam growth (1)
- Force-distance diagram (1)
- Four-point bending test (1)
- Fourier series (1)
- Fourier transform infrared spectroscopy (1)
- Fractional diffusion (1)
- Fracture Mechanics (1)
- Fracture behavior (1)
- Fracture surfaces (1)
- Fragility (1)
- Freeze Drying (1)
- Freeze casting (1)
- Fresnoit (1)
- Fresnoite (1)
- Friction (1)
- Friction Stir Welding (1)
- Friction stir processing (1)
- Frozen state photopolymerization (1)
- Fuel sorption (1)
- Full Notch Creep Test (FNCT) (1)
- Full notch creep test (1)
- Full-Notch Creep Test (1)
- Full-notch creep test (1)
- Fullerite (1)
- Functional fatigue (1)
- Fused Filament Fabrication (1)
- GMR (1)
- GMR sensors (1)
- Gallium (1)
- Gas flow assisted powder deposition (1)
- Gas permeation (1)
- Gas storage (1)
- Gasabgabe (1)
- Gasgehalt (1)
- Gd3+ (1)
- Gefüge (Werkstoffkunde) (1)
- General Chemistry (1)
- General Computer Science (1)
- General Engineering (1)
- Geometrical factors (1)
- Geopolymers (1)
- Glass Ceramic (1)
- Glass Fibres (1)
- Glass capillaries (1)
- Glass crystallization stress (1)
- Glass fiber reinforced polymer (1)
- Glass fiber-epoxy composites (1)
- Glass fibre (1)
- Glass fibre reinforced plastics (1)
- Glass forming (1)
- Glass forming melts (1)
- Glass liner (1)
- Glass manufacturing (1)
- Glass melt (1)
- Glass melting (1)
- Glass scintillator (1)
- Glass screening device (1)
- Glass structure (1)
- Glass transformation temperature (1)
- Glass-ceramics definition (1)
- Glasses (1)
- Glassy solids (1)
- Global stability criterion (1)
- Gnomonic projections (1)
- Gold Nanoparticle Synthesis (1)
- Gold microparticles (1)
- Gold nanoparticle synthesis (1)
- Grade S960QL steel (1)
- Gradient-enhanced damage (1)
- Gradient-enhanced fatigue model (1)
- Grain Boundary (1)
- Grain Boundary Corrosion (1)
- Grain Boundary Phase Diagram (1)
- Grain Boundary Segregation (1)
- Grain Boundary Spinodal (1)
- Grain boundary oxidation (1)
- Grain boundary phase diagram (1)
- Grain boundary precipitates (1)
- Grain boundary structure (1)
- Grain boundary thermodynamics (1)
- Grain growth (1)
- Grain structure (1)
- Graphic design (1)
- Graphite (1)
- Growth kinetics (1)
- Growth rate (1)
- Gypsum (1)
- HV-Insulation (1)
- Hackmanite (1)
- Hardness test (1)
- Hausner ratio (1)
- Heat Treatments (1)
- Heat accumulation (1)
- Heat transfer (1)
- Heat-resistant nickel alloys (1)
- Heißgasextraktion (1)
- Hertzian cracks (1)
- Hierarchical microstructure (1)
- Hierarchical microstructure Premartensite (1)
- Hierarchical porosities (1)
- High - temperature (1)
- High - temperature corrosion (1)
- High Voltage Insulation (1)
- High alloyed steels (1)
- High cycle fatigue (1)
- High density polyethylene (1)
- High energy radiation (1)
- High entropy superalloys (1)
- High interstitial austenitic steel (1)
- High pressure (1)
- High pressure gas storage (1)
- High temperature nickel-based eutectic alloys (1)
- High temperature oxidation (1)
- High temperatures (1)
- High-Entropy Alloys (1)
- High-Entropy Materials (1)
- High-Temperature Corrosion (1)
- High-Temperature Materials (1)
- High-density polyethylene (PE-HD) (1)
- High-strength steel (1)
- High-temperature fatigue crack growth (1)
- High-temperature oxidation (1)
- High-temperature properties (1)
- High-voltage testing (1)
- High‐temperature corrosion (1)
- Hipims (1)
- Hochentropie-Legierung (1)
- Hochentropielegierung (1)
- Homogenization (1)
- Honing (1)
- Honing Stone (1)
- Horizon 2020 (1)
- Host-guest hybrid materials (1)
- Hot Press (1)
- Hot isostatic pressing (1)
- Hot isostatic pressing (HIP) (1)
- Hybrid Manufacturing (1)
- Hybrid additive manufacturing (1)
- Hydrogel (1)
- Hydrogen diffusivity (1)
- Hydrogen gas (1)
- Hydrogen permeability (1)
- Hydrogen sensor (1)
- Hydrogen sensors (1)
- Hydrogen storage (1)
- Hydrogen storage tank (1)
- Hydrothermal Ageging (1)
- Hydrous glass (1)
- Hygrothermal (1)
- Hyper-arid (1)
- IASCC (1)
- IN 718 (1)
- IN738LC (1)
- IR spectroscopy (1)
- Imaging (1)
- Impact damage (1)
- Impact wear (1)
- Implant failures (1)
- Implants (1)
- In situ diffraction (1)
- In situ synthesis (1)
- In situ thermal-annealing experiment (1)
- In-Situ Testing (1)
- In-situ ED-XRD (1)
- In-situ Process Monitoring (1)
- In-situ SEM micro shear deformation (1)
- In-situ composites (1)
- In-situ diffraction (1)
- In-situ process monitoring (1)
- In-situ tomography (1)
- In-vivo (1)
- In718 (1)
- Incipient plasticity (1)
- Inclusion cluster (1)
- Inclusion size (1)
- Inconel 686 coating (1)
- Incremental lifetime models (1)
- Indentation (1)
- Indentation fracture toughness (1)
- Indentation hardness (1)
- Industrial and Manufacturing Engineering (1)
- Infrared nano AFM (1)
- Initial attachment (1)
- Inkjet (1)
- Inter layer time (1)
- Interdiffusion (1)
- Interface (1)
- Interface Strength (1)
- Interfacial Spinodal (1)
- Interfacial Strength (1)
- Interfacial anisotropy (1)
- Interfacial free energy (1)
- Interlaboratory comparability (1)
- Intermetallic (1)
- Intermittent microplasticity (1)
- Intermodulation AFM (1)
- Internal Sulfidation (1)
- Internal Surfaces (1)
- Internal oxidation (1)
- Internal stresses (1)
- Interoperable (1)
- Intrinsic stress (1)
- Invar (1)
- Inverse ostwald ripening (1)
- Investment casting (1)
- Ion beam erosion Sectioning (1)
- Iron meteorite (1)
- Iron oxide (1)
- Irradiation (1)
- Irregular topography (1)
- JMAK model (1)
- Joints/joining (1)
- KCl (1)
- KI (1)
- Kernel average misorientation (1)
- Keywords: Poly(ether ether ketone) (1)
- Kidney injury (1)
- Kikuchi bands (1)
- Knowledge Graphs (1)
- Knowledge graphs (1)
- Knowledge representation (1)
- Kriechen (1)
- Kristallisation (1)
- L-PBF (1)
- LIBS (1)
- LMD (1)
- LSD print (1)
- LTCC multilayer (1)
- Laboratory X-ray diffraction (1)
- Laser Beam Melting (1)
- Laser Cladding (1)
- Laser Poeder Bed Fusion (1)
- Laser Powder Bed Fusion (LPBF) (1)
- Laser Scanning Microscopy (1)
- Laser Scanning Microscopy (LSM) (1)
- Laser beam melting (LBM) (1)
- Laser curing (1)
- Laser induced slipcasting (1)
- Laser light scattering (1)
- Laser powder-based directed energy deposition (1)
- Laser-induced slip casting (1)
- Lateral flow (1)
- Lattice distortions (1)
- Lattice parameter determination (1)
- Lattice point density (1)
- Lattice rotation (1)
- Lattice structures (1)
- Lattices (1)
- Laves phase (1)
- Layer depostion (1)
- Layered manganese oxide (1)
- Layering misalignment (1)
- Lecture films (1)
- Lecture videos (1)
- Legierung mit komplexer Zusammensetzung (1)
- Life cycle (1)
- Lifetime prediction (1)
- Light (1)
- Light curing (1)
- Lightweighting (1)
- Limestone Filler (1)
- Lindemann criterion (1)
- Linear elastic fracture mechanics (1)
- Linked open data (1)
- Liquid Metal Embrittlement (1)
- Liquid metal embrittlement (1)
- Liquid phase sintering (1)
- Lithium-ion batteries (1)
- Lithography-based technologies (1)
- Local landscape evolution (1)
- Localized Surface Plasmon Resonances (1)
- Localized plasmons (1)
- Log-normal distribution (1)
- Long-term aging (1)
- Long-term calculation (1)
- Low Cycle Fatigue (LCF) (1)
- Low carbon steel (1)
- Low expansion (1)
- Low strain (1)
- Low-Cycle Fatigue (LCF) (1)
- Low-Cycle-Fatigue (1)
- Low-cycle fatigue (1)
- Low-cycle fatigue. (1)
- Low-cycle-fatigue behaviour (1)
- Low-loading (1)
- MGS-1 regolith simulant (1)
- MOF-74 (1)
- Machine learning (1)
- Magmatic and hydrothermal processes (1)
- Magnetic domain distribution (1)
- Magnetic shape memory (1)
- Magnetic stray field (1)
- Magnetic stray fields (1)
- Magnetomechanical effect (1)
- Martensitic steel (1)
- Martensitic steels (1)
- Martensitic structure (1)
- Master curve (1)
- Mat-o-lab (1)
- Material Digital (1)
- Material Life Cycle (1)
- Material characterization (1)
- Material defects (1)
- Material failure (1)
- Material modeling (1)
- Material oxidation (1)
- Materials Chemistry (1)
- Materials Data Space (1)
- Materials Science (1)
- Materials Testing (1)
- Materials and Processes Data Reusability (1)
- Materials informatics (1)
- Materials science and engineering (1)
- Materials testing (1)
- Matrix residual stress (1)
- Mean atomic number (1)
- Mean-field modelling (1)
- Mechanical Behavior (1)
- Mechanical and thermal testing (1)
- Mechanical anisotropy (1)
- Mechanical deformation (1)
- Mechanistic Modelling (1)
- Medium entopy alloy (1)
- Medium entropy alloy (1)
- Medium entropy alloys (1)
- Medium-entropy alloy (1)
- Mehrskalenmodell (1)
- Melting (1)
- Meta material (1)
- Metadata (1)
- Metal Dusting (1)
- Metal Magnetic Memory (1)
- Metal additive manufacturing (1)
- Metal and alloys (1)
- Metal magnetic memory (1)
- Metal powder characterization (1)
- Metallic Glass (1)
- Metallic components (1)
- Metallic materials (1)
- Metallic silver precipitates (1)
- Metallography (1)
- Metals and Alloys (1)
- Metformin (1)
- Methodology (1)
- Metrology (1)
- Micro computed tomography (1)
- Micro-cracking (1)
- Microbiologically influenced corrosion (1)
- Microcrystals (1)
- Micromanipulation (1)
- Microplastic stress (1)
- Microplasticity (1)
- Microsegregation (1)
- Microspine (1)
- Microstructur (1)
- Microstructural changes of a Fe Si alloy (1)
- Microstructural orientation (1)
- Microstructure Characterization (1)
- Microstructure Evolution (1)
- Microstructure characterisation (1)
- Microstructure design (1)
- Microstructure modification (1)
- Microstructure, γ/γ' misfit (1)
- Microwave technology (1)
- Microwave-assisted synthesis (1)
- Mid-Level Ontology for MSE (1)
- Mikroplastik (1)
- Milling (1)
- Miniature specimens (1)
- Mis-match (1)
- Misfitting precipitate (1)
- Misorientation (1)
- Mixed conductors (1)
- Mixed-linkers (1)
- Mn-oxides (1)
- Mn3O4 (1)
- Model (1)
- Moisture (1)
- Molecular Dynamics (1)
- Molten salt (1)
- Monte-Carlo-Analysis (1)
- Moon (1)
- Mortar (1)
- Mortel (1)
- Multi-principal element alloys (1)
- Multiaxial deformation (1)
- Multilayer ceramic technology (1)
- Multilayers (1)
- Multilayertechnik (1)
- Multiple cracks (1)
- NFDI-MatWerk (1)
- NGS (1)
- NIST (1)
- Nano CRM (1)
- Nano metal fluorides (1)
- Nano particle (1)
- Nano screening (1)
- Nano-assemblies (1)
- Nano-ceramic-additive-manufacturing photoresin (1)
- Nano-composite (1)
- Nano-landscape (1)
- Nano-powder characterization (1)
- Nano-safety (1)
- Nano-scratch test (1)
- NanoCAM (1)
- Nanocomposites (1)
- Nanocrystalline alloys (1)
- Nanocrystalline structure (1)
- Nanoelectromechanical systems (NEMS) (1)
- Nanomaterial screening (1)
- Nanoparticle structure (1)
- Nanoparticle synthesis (1)
- Nanoparticles synthesis (1)
- Nanoplattform (1)
- Nanopowder (1)
- Nanoribbons (1)
- Nanoscale multilayers (1)
- Nanostructure (1)
- Natural (1)
- Natural silver wires (1)
- Nb3Sn (1)
- Near Infrared Spectroscopy (1)
- Negative charged microparticle (1)
- Net zero (1)
- Networking (1)
- New standards (1)
- Ni-Mn-Ga (1)
- Ni-Resist (1)
- NiMaGa (1)
- NiTi (1)
- Nickel based coatings (1)
- Nickel-base superalloy (1)
- Nimonic 75 (1)
- Nitride (1)
- Noble metal nanoparticles (1)
- Non-desired foaming (1)
- Non-destructive Materials (1)
- Non-metallic inclusions (1)
- Non-serrated inhomogeneous flow (1)
- Nondestructive testing (1)
- Normung (1)
- Notch (1)
- Nucleation mode (1)
- Nucleation tendency (1)
- Number density (1)
- Nydrogen melting (1)
- Online Process Monitoring (1)
- Online quality control (1)
- Online teaching (1)
- Ooxidation (1)
- Optic (1)
- Optical and Magnetic Materials (1)
- Optical backscatter reflectometry (1)
- Optical centrifugation (1)
- Optical criterion (1)
- Optical criterion of brittleness (1)
- Optical fibre (1)
- Optical properties (1)
- Optical properties of glasses and ceramics (1)
- Optical spectroscopy (1)
- Optical tweezers (1)
- Ordered/disordered structures (1)
- Ordering (1)
- Orientation refinement (1)
- Orientation relationship (1)
- Orientation-dependent microstructure (1)
- Orowan Mechanism (1)
- Osteogenesis (1)
- Overaging (1)
- Oxidation protection (1)
- Oxide (1)
- Oxide coatings (1)
- Oxide glass (1)
- Oxide scale (1)
- Oxides (1)
- Oxidglas (1)
- Oxyfluoride (1)
- Oxygen evolution reaction (1)
- P92 steels (1)
- PA6.6 (1)
- PE-HD Sorption (1)
- PLS-DA (1)
- PPA (1)
- PV modules (1)
- Packaging (1)
- Parabolic flight (1)
- Parametric modeling (1)
- Particle Size Distribution (1)
- Particle-bed binder jetting (1)
- Passive components and circuits (1)
- Permittivity reduction (1)
- Persistent luminescent (1)
- Phase Diagram (1)
- Phase Diagrams (1)
- Phase Separation (1)
- Phase analysis (1)
- Phase field crystal (1)
- Phase field method (1)
- Phase field model (1)
- Phase field simulation (1)
- Phase stability (1)
- Phase-field Simulation (1)
- Phase-field model (1)
- Phase-field modelling (1)
- Phosphate (1)
- Phosphors (1)
- Photocatalysis (1)
- Photochromism (1)
- Photocleavable organosilanes (1)
- Photodynamic therapy (1)
- Photopolymer composites (1)
- Phototrophs (1)
- Photovoltaic modules (1)
- Physical aging (1)
- Physical properties (1)
- Physically based material model (1)
- Physics-informed Neural Network (1)
- Phytolith (1)
- Pipelines (1)
- Pitting corrosion (1)
- Planetary surface (1)
- Plasma imaging (1)
- Plasma nanocoatings (1)
- Plasma spray (1)
- Plasmon enhancement (1)
- Plasmonic (1)
- Platform Material Digital (1)
- Platform Material Digital (PMD) (1)
- Platform MaterialDigital (1)
- Platform MaterialDigital (PMD) (1)
- Platinum-group-metals (1)
- Pole figures (1)
- Polyethylen (1)
- Polymer Matrix Composite (1)
- Polymer analysis/characterization (1)
- Polymer composite (1)
- Polymer-Ceramic-Composite (1)
- Polymer-ceramic mixtures (1)
- Polymer-matrix composites (PMC) (1)
- Polymeric Materials (1)
- Polymer–matrix composites (1)
- Polyolefins (1)
- Polypropylene (1)
- Polystyrene (1)
- Polyurethane (1)
- Pore (1)
- Porosification (1)
- Porous materials (1)
- Portable sensor (1)
- Portfolio (1)
- Positron annihilation spectroscopy (1)
- Powder bed additive manufacturing (1)
- Powder bed density (1)
- Powder deposition (1)
- Powder diffraction (1)
- Powder flow (1)
- Powder processing (1)
- Powder rheology (1)
- Powder-based processes (1)
- Powdered activated carbon (1)
- Power factor (1)
- Power law (1)
- Power plant (1)
- Precipitate shape (1)
- Precipitation Analysis (1)
- Precipitation hardening (1)
- Preparation (1)
- Preventive strategies (1)
- Primary phases (1)
- Principal Stress (1)
- Principal stress (1)
- Principal stress components (1)
- Printing (1)
- Process (1)
- Process Monitoring (1)
- Process development (1)
- Processing window (1)
- Production scatter (1)
- Proficiency test (1)
- Projection center (1)
- Projekt AGIL - Alterung additiv gefertigter metallischer Materialien und Komponenten (1)
- Properties (1)
- Property simulation (1)
- Pseudosymmetry (1)
- Pull-out composite materials (1)
- Pultruded fiber rods (1)
- Quality assurance (1)
- Quantitative Precipitation Analysis (1)
- Quantitative image analysis (1)
- Quantum dots (1)
- Radiation-matter interaction (1)
- Radii distribution (1)
- Radon transform (1)
- Rafting (1)
- Raman (1)
- Reaction Sintering (1)
- Real time growth control (1)
- Real-time deformation (1)
- Real-time qPCR (1)
- Reference Dataset (1)
- Reference Material (1)
- Reference material BCR-425 (1)
- Reference nanomaterials (1)
- Reference nanoparticles (1)
- Refractory alloy (1)
- Refractory chemically complex alloy (1)
- Refractory chemically complex alloys (1)
- Refractory superalloys (1)
- Regolith (1)
- Reheating (1)
- Rejuvenation (1)
- Relaxation fatigue (1)
- Relaxation metallic glasses (1)
- Relaxation tests (1)
- Relaxationsphänomene (1)
- Reliable characterization (1)
- Repair of sandwich shell structures (1)
- Repair patch (1)
- Residual strains (1)
- Residual stress analysis (1)
- Resistance (1)
- Resistance spot welding (1)
- Resistance stress (1)
- Resonance testing (1)
- Reusability (1)
- Reusable data (1)
- Rheology (1)
- Rhodonia placenta (1)
- Rissausbreitung (1)
- Risswachstum (1)
- Robot-assisted galss melting (1)
- Roboter (1)
- Robotic glass melting (1)
- Robotische Glasschmelzanlage (1)
- Round Robin (1)
- SDC (1)
- SEM micrography (1)
- SEM wood characterization (1)
- SHM (1)
- SO2 (1)
- STEM (1)
- Safety (1)
- Sailplane Development Panel (1)
- Sall-angle scattering (1)
- Salt melt (1)
- Samarium doped ceria (1)
- Sample holder (1)
- Sand blasting (1)
- Sandwich structures (1)
- Scaffold (1)
- Scaffold geometry (1)
- Scaffolds (1)
- Scale-dependent behavior (1)
- Scan strategies (1)
- Scanning Electron Microscopy (1)
- Scanning Electron Microscopy (SEM) (1)
- Scanning acoustic microscopy (SAM) (1)
- Scanning electron microscope (1)
- Scanning electron microscopy (SEM) (1)
- Scarf joint (1)
- Scarf joint repair (1)
- Scarf joint repairs (1)
- Scavenging effect of iron (1)
- SchwarzP cells (1)
- Scratches (1)
- Screen printing (1)
- Screening method (1)
- Segregation (1)
- Segregation Engineering (1)
- Segregation engineering (1)
- Selective laser melting (SLM) (1)
- Self-Assembly (1)
- Self-consistent dipole model (1)
- Self-organization (1)
- Semantic Data Integration (1)
- Semantic Interioerability (1)
- Semantic Web (1)
- Semantic Web technologies (1)
- Semantic data integration (1)
- Semantic interoperability (1)
- Semantic structuring (1)
- Sensing (1)
- Sensor (1)
- Sewage treatment plant (1)
- Shadowgraphy (1)
- Shape memory alloy (1)
- Shape memory alloys (1)
- Shear (1)
- Shear load (1)
- Shear strain (1)
- Shear testing (1)
- Shear thinning (1)
- Shear-band cavitation (1)
- Shear-band structure (1)
- Short range order (1)
- Short-beam strength (1)
- Silicate glass (1)
- Silicate glass-ceramics (1)
- Silicatglas (1)
- Silicoborate glasses (1)
- Silicon release (1)
- Silver (1)
- Silver cluster (1)
- Silver glass paste (1)
- Silver precipitates (1)
- Silver-glass metallization paste (1)
- Simulation workflow (1)
- Single crystal Ni-Base superalloys (1)
- Single crystal superalloys (1)
- Single fiber pull-out test (1)
- Sinter additive (1)
- Sinter retardation (1)
- Sintering additive (1)
- Sintering atmosphere (1)
- Sintern (1)
- Sinus floor augmentation (1)
- Size (1)
- Size and size distribution (1)
- Size distribution (1)
- Size effect (1)
- Sliding simulation (1)
- Slip localization (1)
- Slip-rolling (1)
- Slurry optimization (1)
- Small angle x-ray scattering (1)
- Small-Angle X-ray Scattering (1)
- Small-scale (1)
- Smart materials (1)
- Smectite (1)
- Soda lime silicate glass (1)
- Soda-lime-silica (1)
- Sodium ion batteries (1)
- Sodium zinc borate glass (1)
- Sodiumborosilicate glasses (1)
- Softening temperature (1)
- Soil (1)
- Soil sample (1)
- Solar panels (1)
- Solid oxide fuell cell (1)
- Solid solution strengthening (1)
- Solid-State-Synthesis (1)
- Solid-state-synthesis (1)
- Space exploration (1)
- Spar cap design (1)
- Spark plasma sintering (1)
- Specimen geometry (1)
- Spinodal Decomposition (1)
- Spinodal decomposition (1)
- Split Hopkinson bar (1)
- Split-vacancy defect complexes (1)
- Spring constant (1)
- Stable crack growth (1)
- Standardisation (1)
- Statistics (1)
- Steam oxidation resistance (1)
- Steel P92 (1)
- Steel alloy (1)
- Stereoscopy (1)
- Strain (1)
- Strain difference (1)
- Strain energy (1)
- Strain rate dependence (1)
- Stress distribution (1)
- Stress intensity (1)
- Stress-corrosion (1)
- Stress-strain behavior (1)
- Stress-strain-behavior (1)
- Structural composites (1)
- Structural defects (1)
- Structural dynamics (1)
- Structural health monitoring (1)
- Structural health monitoring (SHM) (1)
- Structural steel (1)
- Structure property correlations (1)
- Structure-property correlation (1)
- Structured Data (1)
- Structured heating (1)
- Subcritical crack growth (1)
- Subsurface defects (1)
- Superalloy single crystals (1)
- Superaustenite steel (1)
- Supercritical/dense phase CO 2 (1)
- Superelasticity (1)
- Superlattice extrinsic stacking faults (1)
- Superlegierung (1)
- Supersaturation (1)
- Support configurations (1)
- Support vector machines (1)
- Surface Nucleation (1)
- Surface elasticity (1)
- Surface modification (1)
- Surface roughness (1)
- Surface stress (1)
- Surface-induced Melting (1)
- Swept wavelength interferometry (1)
- Swept wavelength interferometry (SWI) (1)
- Symmetric dwell periods (1)
- Synchrotron CT (1)
- Synchrotron X-ray diffraction (1)
- Synchrotron micro-tomography (1)
- Synchrotron radiations (1)
- Synchrotron tomography (1)
- Synthesis (1)
- T1 precipitate (1)
- TAHYA (1)
- TED (1)
- TIG-welding (1)
- TMF (1)
- TMF experiments (1)
- Tape casting (1)
- Tb3+ (1)
- Technical Ceramics (1)
- Temperature dependence (1)
- Temperature driven process (1)
- Tempered martensite ferritic steel (1)
- Tempered martensite ferritic steels (1)
- Tensile strength (1)
- Tensile stress relaxation (1)
- Tensile stress relaxation testing (1)
- Tensile tests (1)
- Termites (1)
- Test Improvement (1)
- Tetragonal distortion (1)
- Tetragonality (1)
- Texturation (1)
- Theranostics (1)
- Thermal Cycling (1)
- Thermal cycling (1)
- Thermal degradation (1)
- Thermal desorption mass spectrometry (1)
- Thermal stress (1)
- Thermo mechanical fatigue (1)
- Thermo-mechanical fatigue (1)
- Thermo-mechanical loading (1)
- Thermo-mechanical-loading (1)
- Thermo-mechanics (1)
- Thermo-optical measurement (1)
- Thermoanalysis (1)
- Thermoanalytical Methods (1)
- Thermobimetal (1)
- Thermodynamic analysis (1)
- Thermodynamic stability (1)
- Thermodynamische Stabilität (1)
- Thermoelectric generator (1)
- Thermoelectric generator design (1)
- Thermogravimetric analysis (1)
- Thermomechanical Fatigue (TMF) (1)
- Thermomechanische Ermüdung (1)
- Thermoplastic forming (1)
- Thermoplastic matrix (1)
- Thermoplastic prepreg (1)
- Thermoset composition (1)
- Thermosetting resin (1)
- Thesaurus (1)
- Thickening (1)
- Thin films (1)
- Thin tribofilm (1)
- Thiol-ene click chemistry (1)
- Three-dimensional Bone tissue engineering (1)
- Three-dimensional tomographies (1)
- Tomography (1)
- Tools (1)
- Tooth wear (1)
- Transducers (1)
- Transformer (1)
- Transmission Electron Microscopy (1)
- Transmission Kikuchi diffraction (1)
- Transmittance (1)
- Transparency (1)
- Transparent (1)
- Transparent ceramic (1)
- Tribology (1)
- Tricalcium Phosphate (1)
- Triply Periodical Minimal Surface (1)
- Tungsten carbide (1)
- Tungsten-Rhenium (1)
- Turbine disk (1)
- Twinning (1)
- Two-photon adsorption (1)
- Two-photon polymerization (1)
- Two-photon-polymerization (1)
- Ultrasonic assited machining (1)
- Unidirectional composites (1)
- Upconversion nanoparticles (1)
- Upconverting nanoparticles (1)
- VCSEL (1)
- VM12 SHC (1)
- Vacancies (1)
- Vacuum hot extraction (1)
- Very high cycle fatigue (1)
- Vickers Hardness (1)
- Vickers identation (1)
- Viscoelastic model (1)
- Viscose sintering (1)
- Visual ontology development (1)
- Visualization (1)
- Vivianite (1)
- Vocabulary providers (1)
- Volatiles from thermosets (1)
- Volume Fraction (1)
- Volume changes (1)
- Volume fraction (1)
- WAXS (1)
- Wasser (1)
- Waste water (1)
- Water (1)
- Water Diffusion (1)
- Water droplet erosion resistance (1)
- Water in glass (1)
- Welding processing influences (1)
- Wet chemical etching (1)
- Wet dispersion (1)
- White light emitters (1)
- Wind turbine blade shell structures (1)
- Withstand voltage tests (1)
- Women in science (1)
- Work of adhesion (1)
- X-ray Diffraction (1)
- X-ray diffraction analysis (1)
- X-ray imaging (1)
- X-ray refractography (1)
- X-ray scattering (1)
- X-ray tomographic (1)
- X-ray tomography (1)
- X-ray-diffraction (1)
- XPCS (1)
- Xolography (1)
- Young`s modulus (1)
- Young´s Modulus (1)
- Young´s modulus (1)
- Young’s Modulus (1)
- Yttria stabilized zirconia (1)
- Zinc oxide (1)
- Zirconia-toughened alumina (1)
- Zirconia: yttria stabilized (1)
- ZnO (1)
- aerosol deposition method (ADM) (1)
- alumina (1)
- arbidic austempered ductile iron (1)
- arbon capture (1)
- battery aging mechanism (1)
- bioactive (1)
- biomaterials (1)
- bone (1)
- calcium cobaltite (1)
- carbon steel (1)
- ceramic (1)
- ceramics (1)
- condensate (1)
- current collector corrosion (1)
- dental (1)
- depth profiles (1)
- electrochemical characterization (1)
- electron microscopy (1)
- high entropy alloys (1)
- high pressure (1)
- hydrogen storage (1)
- impurities (1)
- in-situ synthesis (1)
- infrared spectroscopy (1)
- laser cladding (1)
- microstructural changes (1)
- microstructure analysis (1)
- multi scale testing (1)
- negative crystal growth (1)
- oxidation (1)
- phosphate glasses (1)
- pitting corrosion (1)
- scanning electron microscopy (1)
- selective laser melting (1)
- sulfidation (1)
- thermoelectric oxide (1)
- thermoelectrics (1)
- utilization, and storage (CCUS) technology (1)
- volume resistivity (1)
- water speciation (1)
- γ/γ' matrix (1)
- γ″ phase (1)
- θ′ phase (1)
- θ′-(Al2Cu) precipitate phase (1)
Organisationseinheit der BAM
- 5 Werkstofftechnik (1010)
- 5.1 Mikrostruktur Design und Degradation (307)
- 5.2 Metallische Hochtemperaturwerkstoffe (237)
- 5.4 Multimateriale Fertigungsprozesse (191)
- 5.6 Glas (139)
- 5.5 Materialmodellierung (106)
- 5.3 Polymere Verbundwerkstoffe (101)
- 8 Zerstörungsfreie Prüfung (93)
- 9 Komponentensicherheit (86)
- 7 Bauwerkssicherheit (83)
Paper des Monats
- ja (11)
The control of stress development in cast ceramics during drying is usually one of critical steps in ceramic processes, which is important also for additive manufacturing technologies using a suspension as feedstock. This work introduces a method based on the cantilever deflection method, to simultaneously quantify the kinetics of solvent evaporation, the shrinkage and the intensity of in-plane stresses developed during drying. Particular attention is given here to the experimental limits of the method and to the optimization of the experimental conditions to suitably measure the intensity of in-planar stress in the coating. The optimized method is applied to
four alumina slurries for the water-based additive manufacturing technology LSD-print. Four stages of drying are identified and discussed in relation with the granulometry and morphology of the alumina ceramic particles.
The current lack of quantitative knowledge on processing-microstructure–property relationships is one of the major bottlenecks in today’s rapidly expanding field of additive manufacturing. This is centrally rooted in the nature of the processing, leading to complex microstructural features. Experimentally-guided modeling can offer reliable solutions for the safe application of additively manufactured materials. In this work, we combine a set of systematic experiments and modeling to address creep anisotropy and its correlation with microstructural characteristics in laser-based powder bed fusion (PBF-LB/M) additively manufactured Inconel-738LC (IN738LC). Three sample orientations (with the tensile axis parallel, perpendicular, and 45° tilted, relative to the building direction) are crept at 850 °C, accompanied by electron backscatter secondary diffraction (EBSD), scanning electron microscopy (SEM) and transmission electron microscopy (TEM) investigations. A crystal plasticity (CP) model for Ni-base superalloys, capable of modeling different types of slip systems, is developed and combined with various polycrystalline representative volume elements (RVEs) built on the experimental measurements. Besides our experiments, we verify our modeling framework on electron beam powder bed fusion (PBF-EB/M) additively manufactured Inconel-738LC. The results of our simulations show that while the crystallographic texture alone cannot explain the observed creep anisotropy, the superlattice extrinsic stacking faults (SESF) and related microtwinning slip systems play major roles as active deformation mechanisms. We confirm this using TEM investigations, revealing evidence of SESFs in crept specimens. We also show that the elongated grain morphology can result in higher creep rates, especially in the specimens with a tilted tensile axis.
A widespread recovery of waste heat requires a cost‐effective production of thermoelectric generators. Thermoelectric oxides are predestined for use at high temperatures. For manufacturing reasons, a multilayer generator design will be easily scalable and cost‐effective. To evaluate the potential of ceramic multilayer technology for that purpose, a multilayer of the promising thermoelectric oxides calcium cobaltite (Ca3Co4O9), calcium manganate (CMO, CaMnO3), and glass–ceramic insulation layers is fabricated. Cracks and reaction layers at the interfaces are observed in the microstructure. The compositions of these reaction layers are identified by energy‐dispersive X‐ray spectroscopy and X‐ray diffraction. Mechanical and thermal properties of all layers are compiled from literature or determined by purposeful sample preparation and testing. Based on this data set, the internal stresses in the multilayer after co‐firing are calculated numerically. It is shown that tensile stresses in the range of 50 MPa occur in the CMO layers. The reaction layers have only a minor influence on the level of these residual stresses. Herein, it is proven that the material system is basically suitable for multilayer generator production, but that the co‐firing process and the layer structure must be adapted to improve densification and reduce the tensile stresses in the CMO.
The present work addresses powder bed binder jetting additive manufacturing by selective magnesium phosphate cement activation. Despite the potential of this technology to aid the digitalization of the construction industry, the effect of processing parameters on the mechanical performance of printed materials has not yet been studied to generate a guideline for the further development of the technology. Statistical methodologies were used to screen the effect of four printing process parameters (printing speed, layer thickness, raster angle, and build direction on flexural and compressive strength). As the exploited technology works with constant fluid pressure, the physical interpretation of the effect of each factor can be considered taking into account the interactions between the binder materials in the powder bed. Analysis of variance (ANOVA) indicated that printing speed and layer thickness significantly affect mechanical performances. Furthermore, the layout of samples for the printing process is preferable to be parallel the printhead movement. An anisotropic behavior was observed, and the samples subjected to compressive forces parallel to the layer plane possessed lower strength values. This effect can be interpreted as a result of a weak area of low density in between layers, leading to a pronounced delamination under compression. Even though the strength of the printed material is not suitable for a structural concrete, it can be marginally improved by design of experiment and optimized for non-structural applications, such as for porous artificial stone. Design of experiment coupled with ANOVA methods can be used in the future to support the development of novel material mixtures, thus expanding the fields of application of this novel additive manufacturing technology.
An interlaboratory study, involving eigth international laboratories and coordinated by COMTES FHT (Czech Republic), was conducted to validate tensile measurements obtained using miniature specimens on additively manufactured (AM) components and artifacts. In addition to AM 316L stainless steel (316L SS), a wrought highstrength steel (34CrNiMo6V, equivalent to AISI 4340) was also used. Based on the results, a precision statement in accordance with ASTM E691 standard practice was developed, intended for inclusion in a proposed annex to the ASTM E8/E8M tension testing method. The primary outcomes of the study highlighted the agreement between yield and tensile strength measured from miniature and standard-sized tensile specimens. Furthermore, most tensile properties exhibited similar standard deviations, offering users insight into the efficacy of miniature specimen applications.
Advancements in bulk metallic glass thermoplastic forming unleash the potential to fabricate microscale metallic features with unparalleled precision and durability, i.e. microspine gripping structures for mobility platforms on planetary or in-space robots. Four designs of grippers were fabricated and rigorously tested. Coefficient of friction on four test surfaces were measured and compared to SiC paper and Velcro. The hardness and elasticity of the bulk metallic glasses make them a game-changer in the field, offering a superior alternative to conventional nonmetallic grippers.
Relation of craze to crack length during slow crack growth phenomena in high‐density polyethylene
(2024)
The craze‐crack mechanism occurring in high‐density polyethylene (HDPE) causing slow crack growth and environmental stress cracking is investigated in detail with respect to the relation of crack length and the related craze zone. This is essential for the understanding of the resulting features of the formed fracture surface and their interpretation in the context of the transition from crack propagation to ductile shear deformation. It turns out that an already formed craze zone does not inevitably result in formation of a propagating crack, but could also undergo ductile failure. For the examination, the full notch creep test (FNCT) was employed with a subsequent advanced fracture surface analysis that was performed using various imaging techniques: light microscopy, laser scanning microscopy, scanning electron microscopy, and X‐ray micro computed tomography scan. FNCT specimens were progressively damaged for increasing durations under standard test conditions applying Arkopal, the standard surfactant solution, and biodiesel as test media were used to analyze the stepwise growth of cracks and crazes. From considerations based on well‐established fracture mechanics approaches, a theoretical correlation between the length of the actual crack and the length of the preceding craze zone was established that could be evidenced and affirmed by FNCT fracture surface analysis. Moreover, the yield strength of a HDPE material exposed to a certain medium as detected by a classic tensile test was found to be the crucial value of true stress to induce the transition from crack propagation due to the craze‐crack mechanism to shear deformation during FNCT measurements.
Highlights
- Progress of crack formation in high‐density polyethylene is analyzed by different imaging techniques
- Determined growth rates depend on distinction between craze zone and crack
- The ratio of the present crack to the anteceding craze zone is validated theoretically
- The transition from crack propagation to ductile shear deformation is identified
- An already formed craze zone may still fail by ductile mechanisms
Self-healing polymers have been developed to improve durability and reduce costs associated with maintenance during service. The addition of thermoplastics to thermosets to produce mendable polymers appears as a promising selfhealing technique. In this study, poly (ethylene-co-methacrylic acid) (EMAA) was added to epoxy resin and the effects of EMAA addition on epoxy properties were evaluated. Specimens with two different contents of thermoplastic and particles sizes were manufactured. A two-level full factorial experimental design was used to evaluate the effect of particle size and particle content on properties of epoxy modified with addition of EMAA. Tensile tests and dynamic mechanical analysis (DMA) were used and the evaluated responses were tensile strength, modulus of elasticity, and glass transition temperature (Tg). X-ray computed tomography (XCT) was used to investigate particle size and concentration after manufacturing. It was found that the particle concentration has greater effects on stress–strain behavior of epoxy while Tg was not significantly affected by neither of the analyzed entrance variables.
AbstractTwo‐photon polymerization (2PP) additive manufacturing (AM) utilizes feedstocks of ceramic nanoparticles of a few nanometers in diameter, enabling the fabrication of highly accurate technical ceramic design with structural details as small as 500 nm. The performance of these materials is expected to differ from conventional AM ceramics, as nanoparticles and three‐dimensional printing at high resolution introduce new microstructural aspects. This study applies 2PP‐AM of yttria‐stabilized zirconia to investigate the mechanical response behavior under compressive load, probing the influence of smallest structural units induced by the line packing during the printing process, design of sintered microblocks, and sintering temperature and thereby microstructure. We find a dissipative mechanical response enhanced by sintering at lower temperatures than conventional. The pursued 2PP‐AM approach yields a microstructured material with an increased number of grain boundaries that proposedly play a major role in facilitating energy dissipation within the here printed ceramic material. This microplastic response is further triggered by the filigree structures induced by hollow line packing at the order of the critical defect size of ceramics. Together, these unique aspects made accessible by the 2PP‐AM approach contribute to a heterogeneous nano‐ and microstructure, and hint toward opportunities for tailoring the mechanical response in future ceramic applications.
Photon-based additive manufacturing technologies such as SLA, DLP, LCM, moreover volumetric two-photon-polymerization, Xolography and holographic technologies promise the highest accuracy and dimensional freedom. But to transfer the light through the feedstock it needs sufficient transparency at the used light wavelength. Ceramic particles used for powder processing routes act as scattering sites and therefore hinder the light transmission, unless…
The particle size and particle size distribution are chosen small and narrow enough. Particles which are smaller than roughly 1/10th of the light wavelength, mostly nanoparticles around 5nm size, decrease scattering vastly. This turns resins even with homogeneously distributed ceramic weight fraction of up to 80% transparent again. Feedstocks could be prepared for the highly accurate two-photon-polymerization gaining the smallest yttria stabilized zirconia structures with a resolution of 500nm and unique mechanical properties. The same feedstocks could be applied to DLP and LCM as layer-by-layer AM-technologies for bigger parts. Hybridizing both technologies lead to ceramic parts with microscopic accuracy at macroscopic dimensions. The feedstock was even applied to the volumetric Xolography with the highest transparency requirement so far and to versatile and flexible holographic AM.
Highly filled nano-particle containing transparent ceramic feedstocks open the way for technical ceramics in high precision manufacturing where the performance and durability and accessibility are increased and created by the unique ceramic properties such as mechanical strength, chemical and thermal resistance and biocompatibility
In order to be able to manipulate ceramic powder compacts and ceramic suspensions (slurries) in their volume with light, a minimum transparency of the materials is required. Compared to polymers and metals, ceramic materials are characterized by the fact that they have a wide electronic band gap and therefore a wide optical window of transparency. The optical window generally ranges from less than 0.3 µm to 5 µm wavelength. Therefore, to focus light into the volume of a ceramic powder compact, its light scattering properties need to be tailored. In this study, we present the physical background and material development strategies for the application of two-photon polymerization (2PP), Xolography and selective volumetric sintering for the additive manufacturing of structures in the volume of ceramic slips and green compacts.
Nickel-based alloys have been widely used for gas turbine blades owing to their excellent mechanical properties and corrosion resistance at high temperatures. The operating temperatures of modern gas turbines have been increased in pursuit of increased thermal efficiency. Turbine blades are exposed to these high temperatures combined with mechanical stresses, resulting in material damage through creep, fatigue, and other mechanisms. These turbine blades must be regularly inspected and replaced as needed, to prevent the loss of efficiency, breakdown, and catastrophic failure. Repair of the damaged turbine blades is often a more practical and cost-effective option than replacement, as replacement is associated with high costs and loss of material resources. To this end, state-of-the-art repair technologies including different additive manufacturing and brazing processes are considered to ensure efficient repair and optimum properties of repaired components.
In any repaired part, materials property-mismatches and/or inner defects may facilitate the crack initiation and propagation and thus reduce the number of load cycles to failure. Therefore, a fundamental understanding of the fatigue crack growth and fracture mechanisms in joining zones is required to enable the prediction of the remaining life of repaired components and to further improve and adapt the repair technologies.
Fatigue crack growth experiments have been conducted on SEN (Single Edge Notch) specimens joined via brazing, and pre-sintered Preform (PSP) and multi-materials (casted/printed) specimens layered via additive manufacturing (AM). The experiments were performed at 950 °C and various stress ratios. The crack growth was measured using DCPD (Direct Current Potential Drop) method. The stress intensity factors for joined SEN specimens were calculated using the finite element method and then used to derive the fatigue crack growth curves. Metallographic and fractographic analyses were conducted to get insight into the fracture mechanism.
Results show that the experimental technique for fatigue crack growth was successfully adapted and applied for testing joined specimens. Furthermore, the initial tests indicate that the investigated braze filler material provides a lower resistance to crack growth, and bonding defects cause a crack to deviate to the interface of the base material and joining zone. In AM-sandwich specimens, the crack growth rates are significantly reduced when the crack reaches the interface of printed material and casted material. The obtained crack growth data can be used to calibrate a crack growth model, which will further be utilized to predict the remaining life of repaired components.
High Temperature Fatigue Crack Growth in Nickel-Based Alloys Refurbished by Additive Manufacturing
(2024)
Hybrid additive manufacturing plays a crucial role in the restoration of gas turbine blades, where, e.g., the damaged blade tip is reconstructed by the additive manufacturing process on the existing blade made of a parent nickel-based alloy. However, inherent process-related defects in additively manufactured material, along with the interface created between the additively manufactured and the cast base material, impact the fatigue crack growth behavior in bi-material components. This study investigates the fatigue crack growth behavior in bi-material specimens of nickel-based alloys, specifically, additively manufactured STAL15 and cast alloy 247DS. The tests were conducted at 950 °C with stress ratios of 0.1 and −1. Metallographic and fractographic investigations were carried out to understand crack growth mechanisms. The results revealed significant retardation in crack growth at the interface. This study highlights the potential contributions of residual stresses and microstructural differences to the observed crack growth retardation phenomenon, along with the conclusion from an earlier study on the effect of yield strength mismatch on crack growth behavior at a perpendicular interface in bi-material specimens.
This study introduces an innovative method for efficiently determining the creep properties of high-temperature materials through high-throughput testing, employing digital image correlation [1,2]. The focus is on the AlCoCrFeNiTi alloy [3-5], synthesized by directional solidification, known for its exceptional strength and unique properties. Experimental investigations, including compression, and bending creep tests, were conducted at 750°C.
Capitalizing on the inhomogeneous stress and strain distribution within a cantilever subjected to bending, we leverage this characteristic to extract multiple creep curves from a single test. Stresses at key points were determined using existing analytical solutions [5,6]. Uniaxial tests spanning 300 to 500 MPa initial stress were complemented by bending tests designed to induce similar stress levels. A detailed comparison between bending and uniaxial creep is presented, including the results of verification studies on additional alloys.
This methodology not only expedites testing but also minimizes material usage, energy consumption, and manual labour. This research showcases a reliable and time-efficient approach to exploring the creep behavior of high-temperature materials. The technique is particularly advantageous for characterizing precious alloys with limited dimensions. Microstructural heterogeneity may exist in specimens tested under bending load, however, it can still be correlated to the mechanical properties with modern high-resolution characterization methods. Stress and resulting strain can be directly compared in a single specimen, ensuring uniform manufacturing, and heating history. This method eliminates the possible errors due to testing with different rigs, which could impair the accuracy of studies based on individual tests.
Up to now, oriented surface crystallization phenomena are discussed controversially, and related studies are restricted to few glasses. For silicate glasses we found a good correlation between the calculated surface energy of crystal faces and oriented surface nucleation. Surface energies were estimated assuming that crystal surfaces resemble minimum energy crack paths along the given crystal plane. This concept was successfully applied at the Institute of Physics of Rennes in calculating fracture surface energies of glasses. Several oriented nucleation phenomena can be herby explained assuming that high energy crystal surfaces tend to be wetted by the melt. This would minimize the total interfacial energy of the nucleus. Furthermore, we will discuss the evolution of the microstructure and its effect on the preferred crystal orientation.
Compared to mechanisms like solid solution strengthening, the stacking fault energy (SFE) should be considered as a further factor that influences the material properties. The effect of SFE of alloys or individual elements on strength and resistance can vary considerably. In the high-temperature regime above 700 ◦C, there are still significant gaps in the knowledge about the effect of the SFE on the mechanical properties of single-phase alloys. The effect of SFE on creep resistance of two face-entered cubic equiatomic medium and high entropy alloys, CrCoNi and CrMnFeCoNi, respectively, is evaluated to fill parts of these gaps. Using the Bridgman solidification process, the alloys were produced as single crystals and crept under vacuum at 700 ◦C up to 1100 ◦C. This work shows a significant impact of the lower SFE of CrCoNi on the creep behavior compared to the results of previous investigations of CrMnFeCoNi. The creep resistance of the former is higher over the complete temperature range. At very high temperatures, the strengthening effect of the stacking faults is significantly present. The formation of tetragonal stacking faults and extended dislocation nodes can be identified as the reason for this effect.
Modern dry pressing of ceramic powders using spray‐dried granulates cannot avoid the occurrence of defects related to persisting inter‐ and intra‐granulate interstitial voids. These constitute the parent defect size population limiting the application of polycrystalline ceramics in high‐stress conditions. The mitigation of such defects could widen the range of application in technical and biomedical engineering, reduce the safety range for design, and extend the lifetime of components. Herein, the Weibull size‐effect on strength in size‐partitioned Yttria‐stabilized zirconias (YSZ) feedstocks is used to explore the viability of changing the density distribution of granulate sizes as an effective strategy to obtain a denser particle packing that could reduce the size distribution of strength‐limiting pressing defects. In a direct assessment of critical defect size using multiscale strength testing with a dataset of ≈1300 values, the success of such an approach in increasing the strength reliability for small volume components is demonstrated, along with its ultimate failure in altering the defect size distribution in sintered YSZ ceramics across several length scales. Finally, it is shown that granule morphology (spherical or dimpled) fails to affect the defect density and size distribution in YSZ ceramics.
The digitalization of materials science and engineering (MSE) is currently leading to remarkable advancements in materials research, design, and optimization, fueled by computer‐driven simulations, artificial intelligence, and machine learning. While these developments promise to accelerate materials innovation, challenges in quality assurance, data interoperability, and data management have to be addressed. In response, the adoption of semantic web technologies has emerged as a powerful solution in MSE. Ontologies provide structured and machine‐actionable knowledge representations that enable data integration, harmonization, and improved research collaboration. This study focuses on the tensile test ontology (TTO), which semantically represents the mechanical tensile test method and is developed within the project Plattform MaterialDigital (PMD) in connection with the PMD Core Ontology. Based on ISO 6892‐1, the test standard‐compliant TTO offers a structured vocabulary for tensile test data, ensuring data interoperability, transparency, and reproducibility. By categorizing measurement data and metadata, it facilitates comprehensive data analysis, interpretation, and systematic search in databases. The path from developing an ontology in accordance with an associated test standard, converting selected tensile test data into the interoperable resource description framework format, up to connecting the ontology and data is presented. Such a semantic connection using a data mapping procedure leads to an enhanced ability of querying. The TTO provides a valuable resource for materials researchers and engineers, promoting data and metadata standardization and sharing. Its usage ensures the generation of finable, accessible, interoperable, and reusable data while maintaining both human and machine actionability.
This is the stable version of the full-notch creep test ontology (OntoFNCT) that ontologically represents the full-notch creep test. OntoFNCT has been developed in accordance with the corresponding test standard ISO 16770:2019-09 Plastics - Determination of environmental stress cracking (ESC) of polyethylene - Full-notch creep test (FNCT).
The OntoFNCT provides conceptualizations that are supposed to be valid for the description of full-notch creep tests and associated data in accordance with the corresponding test standard. By using OntoFNCT for storing full-notch creep test data, all data will be well structured and based on a common vocabulary agreed on by an expert group (generation of FAIR data) which is meant to lead to enhanced data interoperability. This comprises several data categories such as primary data, secondary data and metadata. Data will be human and machine readable. The usage of OntoFNCT facilitates data retrieval and downstream usage. Due to a close connection to the mid-level PMD core ontology (PMDco), the interoperability of full-notch creep test data is enhanced and querying in combination with other aspects and data within the broad field of materials science and engineering (MSE) is facilitated.
The class structure of OntoFNCT forms a comprehensible and semantic layer for unified storage of data generated in a full-notch creep test including the possibility to record data from analysis and re-evaluation. Furthermore, extensive metadata allows to assess data quality and reliability. Following the open world assumption, object properties are deliberately low restrictive and sparse.
Extended X-ray absorption fine structure (EXAFS) conducted on an equiatomic MoNbTaW bcc medium-entropy alloy that was annealed at 2273 K reveals unexpectedly small 1st and 2nd shell element-specific lattice distortions. An experimental size-mismatch parameter, δexp, is determined to be ca. 50% lower than the corresponding calculated value. Around W, short-range order (SRO) preferring 4d elements in the 1st and 2nd shells persists. A Nb-W ordering is found, which is reminiscent of ordering emerging at lower temperatures in the B2(Mo,W;Ta,Nb)- and B32(Nb,W)-phases. With high-temperature ordering preferences in fcc also foreshadowing low-temperature phase, these findings suggest a general feature of high-temperature SRO.
Processing and cytocompatibility of Cu-doped and undoped fluoride-containing bioactive glasses
(2024)
Sintered or additive-manufactured bioactive glass (BG) scaffolds are highly interesting for bone replacement applications. However, crystallization often limits the high-temperature processability of bioactive glasses (BGs). Thus, the BG composition must combine high bioactivity and processability. In this study, three BGs with nominal molar (%) compositions 54.6SiO2-1.7P2O3-22.1CaO-6.0Na2O-7.9K2O-7.7MgO (13–93), 44.8SiO2-2.5P2O3-36.5CaO-6.6Na2O-6.6K2O-3.0CaF2 (F3) and 44.8SiO2-2.5P2O3-35.5CaO-6.6Na2O-6.6K2O-3.0CaF2-1.0CuO (F3–Cu) were investigated. The dissolution and ion release kinetics were investigated on milled glass powder and crystallized particles (500–600 μm). All glasses showed the precipitation of hydroxyapatite (HAp) crystals after 7 days of immersion in simulated body fluid. No significant differences in ion release from glass and crystalline samples were detected. The influence of surface roughness on cytocompatibility and growth of preosteoblast cells (MC3T3-E1) was investigated on sintered and polished BG pellets. Results showed that sintered BG pellets were cytocompatible, and cells were seen to be well attached and spread on the surface after 5 days of incubation. The results showed an inverse relation of cell viability with the surface roughness of pellets, and cells were seen to attach and spread along the direction of scratches.
AbstractThis study applies Semantic Web technologies to advance Materials Science and Engineering (MSE) through the integration of diverse datasets. Focusing on a 2000 series age-hardenable aluminum alloy, we correlate mechanical and microstructural properties derived from tensile tests and dark-field transmission electron microscopy across varied aging times. An expandable knowledge graph, constructed using the Tensile Test and Precipitate Geometry Ontologies aligned with the PMD Core Ontology, facilitates this integration. This approach adheres to FAIR principles and enables sophisticated analysis via SPARQL queries, revealing correlations consistent with the Orowan mechanism. The study highlights the potential of semantic data integration in MSE, offering a new approach for data-centric research and enhanced analytical capabilities.
This study aims to represent an approach for transferring the materials testing datasets to the digital schema that meets the prerequisites of the semantic web. As a use case, the tensile stress relaxation testing method was evaluated and the testing datasets for several copper alloys were prepared. The tensile stress relaxation testing ontology (TSRTO) was modeled following the test standard requirements and by utilizing the appropriate upper-level ontologies. Eventually, mapping the testing datasets into the knowledge graph and converting the data-mapped graphs to the machine-readable Resource Description Framework (RDF) schema led to the preparation of the digital version of testing data which can be efficiently queried on the web.
This research deals with the development of the Vickers hardness knowledge graph, mapping the example dataset in them, and exporting the data-mapped knowledge graph as a machine-readable Resource Description Framework (RDF). Modeling the knowledge graph according to the standardized test procedure and using the appropriate upper-level ontologies were taken into consideration to develop the highly standardized, incorporable, and industrial applicable models. Furthermore, the Ontopanel approach was utilized for mapping the real experimental data in the developed knowledge graphs and the resulting RDF files were successfully evaluated through the SPARQL queries.
Today’s industrial demands challenge the research and development sector to make advances in the design and properties of materials that can withstand harsh environments. The AlMo0.5NbTa0.5TiZr refractory high-entropy superalloy (RSA), with a remarkable morphological similarity to the γ/γ' microstructure of Ni-based superalloys and promising high-temperature compressive properties, has been considered as a candidate for structural applications. However, additional properties need to be investigated in order to assess the suitability of this alloy for high temperature applications. Therefore, this work investigates the thermodynamic and microstructural stabilities of the RSA at room temperature and between 900 and 1100 °C, and their influence on the mechanical properties. Although it is possible to improve the mechanical properties at 20 °C by tuning the cooling rate, long-term high temperature exposures lead to phase instabilities that negatively influence the creep behavior.
This study investigates the room‐ and high‐temperature (650 °C) tensile and low‐cycle‐fatigue behavior of Inconel 718 produced by laser powder bed fusion (PBF‐LB/M) with a four‐step heat treatment and compares the results to the conventional wrought material. The microstructure after heat treatment is characterized on different length scales. Compared to the wrought variant, the elastic and yield properties are comparable at both test temperatures while tensile strength, ductility, and strain hardening capacity are lower. The fatigue life of the PBF‐LB/M variant at room temperature is slightly lower than that of the wrought material, while at 650 °C, it is vice versa. The cyclic stress response for both material variants is characterized by cyclic softening, which is more pronounced at the higher test temperature. High strain amplitudes (≥0.7%) at room temperature and especially a high testing temperature result in the formation of multiple secondary cracks at the transitions of regions comprising predominantly elongated grain morphology and columns of stacked grains with ripple patterns in the PBF‐LB/M material. This observation and pronounced crack branching and deflection indicate that the cracks are controlled by sharp micromechanical gradients and local crystallite clusters.
The heat-resistant cast iron EN-GJSA-XNiSiCr35-5-2 (Ni-Resist D-5S) was investigated for its fatigue crack growth behavior at room and high temperatures. Force-controlled tests were carried out at constant temperatures (20 °C, 500 °C, 700 °C) without and with hold time and different load ratios. The crack growth behavior was also characterized under TMF loading (Tmin = 400 °C, Tmax = 700 °C) by applying IP and OP conditions and different load ratios. Three different techniques were combined to monitor crack growth: potential drop, thermography, and compliance method. The effect of the different loading conditions on the fatigue crack growth behavior will be presented and discussed.
In this presentation, the results of the determination of the diffraction and single-crystal elastic constants of laser powder bed fused Inconel 718 are presented. The analysis is based on high-energy synchrotron diffraction experiments performed at the Deutsches Elektronen-Synchrotron. It is shown that the characteristic microstructure of laser powder bed fused Inconel 718 impacts the elastic anisotropy and therefore the diffraction and single-crystal elastic constants. Finally, the consequences on the diffraction-based residual stress determination of laser powder bed fused Inconel 718 are discussed.
In order to be able to manipulate ceramic powder compacts and ceramic suspensions (slurries) within their volume with light, a minimum transparency of the materials is required. Compared to polymers and metals, ceramic materials are characterized by the fact that they have a wide electronic band gap and therefore a wide optical window of transparency. The optical window generally ranges from less than 0.3 µm to 5 µm wavelength. In order to focus light into the volume of a ceramic powder compact, its light scattering properties must therefore be tailored. In this study, we present the physical background and material development strategies for the application of two-photon polymerization (2PP) and selective volumetric sintering for the additive manufacturing of structures in the volume of ceramic slips and green compacts.
Manipulating ceramic powder compacts and ceramic suspensions (slurries) within their volume with light requires a minimum transparency of the materials. Compared to polymers and metals, ceramic materials are unique as they offer a wide electronic band gap and thus a wide optical window of transparency. The optical window typically ranges from below 0.3 µm up to 5µm wavelength. Hence, to penetrate with light into the volume of a ceramic powder compound, its light scattering properties need to be investigated and tailored. In the present study we introduce the physical background and material development strategies to apply two-photon-polymerization (2PP), and other volumetric methods for the additive manufacture of filigree structures within the volume of ceramic slurries.
Fully automated and decentralized fused filament fabrication of ceramics for remote applications
(2024)
Manufacturing of ceramic components in remote (i.e., geographically isolated) settings poses significant challenges where access to conventional manufacturing facilities is limited or non-existent. Fused Filament Fabrication (FFF) enables the rapid manufacturing of ceramic components with complex geometries. Parts formed by FFF require subsequent debinding and sintering to reach full density. Debinding and sintering are typically executed in separate steps with different equipment, necessitating extensive human handling which hinders process automation and may be challenging for the operator in isolated environments. This poster presents an innovative approach: the integration of all process steps into a single, fully automated system, streamlining the process and minimizing human involvement. Our system combines a dual extrusion filament printer with a porous and heat-resistant ceramic print bed. The porous print bed enables mechanical interlocking of the first printed layers, ensuring adhesion and structural integrity during FFF. Ceramic parts are printed onto thin sacrificial rafts, which are built using an interface material with the same binder as the ceramic filament. After the print is completed, the heat-resistant print bed with all parts is transferred seamlessly with a carrier system into a high-temperature furnace for debinding and sintering. During sintering the sacrificial raft is disintegrated, allowing for unconstrained sintering of the ceramic parts and easy removal of the finished parts. In conclusion, our integrated approach enables significant advancements in the fabrication of complex ceramic components in remote environments with increased efficiency and minimal human handling.
Functional fatigue of shape-memory alloys is a considerable threat to the reliable service of actuation devices. Here, we demonstrate the essentially degradation-free cyclic phase-transformation behavior of Ni-Mn-Ga microcrystals up to one million stress-driven superelastic cycles. Cyclic dissipation amounts to about 1/5 of the bulk counterpart and remains unaffected during cycling, even after the introduction of dislocation structures via plastic straining. Plastic yielding and the transformation stress largely exceed the known bulk values. However, the transformation-stress is found to depend on plastic pre-straining, which suggests that the size-affected transformation stress is sensitive to the initial defect structure and that it can be tuned by a targeted introduction of dislocations. These findings demonstrate the high suitability of Ni-Mn-Ga as a robust shape-memory alloy in small-scale functional device engineering.
High‐temperature KCl‐induced corrosion of high Cr and Ni alloys investigated by in‐situ diffraction
(2024)
High‐temperature KCl‐induced corrosion in laboratory air was observed in situ utilizing X‐ray diffraction. High Cr‐containing model alloys (Fe‐13Cr, Fe‐18Cr‐12Ni, and Fe‐25Cr‐20Ni) were coated with KCl and exposed to dry air at 560°C. KCl‐free alloys were studied in the equivalent atmosphere as a reference. After exposure to KCl‐free environments, all alloys showed the formation of very thin oxide layers, indicating good corrosion resistance. In contrast, KCl‐bearing alloys showed distinct damage after exposure.
The characterization of really unknown phases typically uses 70 to 150 reflectors for lattice metric calculation. The determination of the lattice parameters follows with 4% accuracy. Including a Z correction up to 1% can be reached. The precision of the lattice parameters ratios (a:b:c) is, however, better than 0.1%.
Electron Back Scatter Diffraction (EBSD) is a very versatile analytical technique allowing for the characterization of material structure. Historically, diffraction images (Kikuchi patterns) registered during EBSD analysis were solved using Hough/Radon transformation. The last decade brought several novel techniques of experimental pattern analysis, focusing entirely on image analysis routines such as pattern matching, or various variants of High-Resolution EBSD. However, all the above-mentioned techniques require prior knowledge of the material structure to perform orientation analysis. The recently presented algorithm employed in Crystallographic Analysis of Lattice Metric (CALM) software, effectively removes this limitation enabling a standard-less analytical approach in EBSD systems. At its core, the CALM technique couples accurate detection of the Kikuchi bands position, with a rigid construction of reciprocal lattice resulting from translational crystal symmetry. A unique characteristic of the methodology also gives an opportunity for application in the analysis of continuous lattice changes, for example tetragonality mapping. During mapping, however, the geometry of the gnomonic projection (represented by the projection center) is continuously altered decreasing overall algorithm efficiency. The work presents an analysis of the projection center in terms of precision and accuracy.
Objectives
The aim of the study was to investigate the impact of organic additives (binder, plasticizer, and the cross-linking ink) in the formulation of water-based feedstocks on the properties of a dental feldspathic glass-ceramic material developed for the slurry-based additive manufacturing technology “LSD-print.”
Material and methods
Three water-based feldspathic feedstocks were produced to study the effects of polyvinyl alcohol (AC1) and poly (sodium 4-styrenesulfonate) (AC2) as binder systems. A feedstock without organic additives was tested as the control group (CG). Disc-shaped (n = 15) and bar (n = 7) specimens were slip-cast and characterized in the green and fired states. In the green state, density and flexural strength were measured. In the fired state, density, shrinkage, flexural strength (FS), Weibull modulus, fracture toughness (KIC), Martens parameters, and microstructure were analyzed. Disc-shaped and bar specimens were also cut from commercially available CAD/CAM blocks and used as a target reference (TR) for the fired state.
Results
In the green state, CG showed the highest bulk density but the lowest FS, while the highest FS in the green state was achieved with the addition of a cross-linking ink. After firing, no significant differences in density and a similar microstructure were observed for all slip-cast groups, indicating that almost complete densification could be achieved. The CAD/CAM specimens showed the highest mean FS, Weibull modulus, and KIC, with significant differences between some of the slip-cast groups.
Significance
These results suggest that the investigated feedstocks are promising candidates for the slurry-based additive manufacturing of restorations meeting the class 1a requirements according to DIN EN ISO 6871:2019–01.
The Laser-Induced Slip Casting is an additive manufacturing technology specifically developed for ceramic materials using water-based ceramic slurries. The process takes place layer-by-layer in a similar fashion as top-down vat photopolymerization, selectively consolidating each layer by means of a laser energy source positioned on the top. Contrary to vat photopolymerization, in which the consolidation is achieved by selectively cross-linking a ceramic-filled resin, LIS uses water-based slurries with a low amount of organic additives (typically < 5 wt%) as feedstocks.
In LIS, a green body is formed by local evaporation of water which causes the suspension to collapse forming a cast, following a mechanism similar to slip casting. Only a small content of organic additives is needed to effectively disperse the ceramic particles and to increase the green strength.
The technology is very versatile and can be applied to all ceramic systems that can be dispersed in water. One of the main advantages is that even dark materials such as silicon carbide can be processed without issues related to light scattering and absorption.
The presentation will discuss strengths and limitations of LIS compared to other AM technologies and will highlight the latest results for alumina and for silicon carbide ceramics.
Powder bed technologies are amongst the most successful Additive Manufacturing (AM) techniques. The application of these techniques to most ceramics has been difficult so far, because of the challenges related to the deposition of homogeneous powder layers when using fine powders.
In this context, the "layerwise slurry deposition" (LSD) has been developed as a layer deposition method enabling the use of powder bed AM technologies also for advanced ceramic materials. The layerwise slurry deposition consists of the layer-by-layer deposition of a ceramic slurry by means of a doctor blade, in which the slurry is deposited and dried to achieve a highly packed powder. Not only very fine, submicron powders can be processed with low organics, but also the dense powder bed provides excellent support to the parts built. The LSD technology can be combined with binder jetting to develop the so-called “LSD-print” process. LSD-print combines the high-speed printing of binder jetting with the possibility of producing a variety of high-quality ceramics with properties comparable to traditional processing.
The latest development of this technology shows that it is possible to print ceramic parts in a continuous process by depositing a layer onto a rotating platform, growing a powder bed following a spiral motion. The unique mechanical stability of the layers in LSD-print allows to grow a powder bed several centimeters thick without any lateral support. The continuous layer deposition allows to achieve a productivity more than 10X higher compared to the linear deposition, approaching a build volume of 1 liter/hour.
Motivated by the aim of developing an additive manufacturing (AM) technology easily integrated in the process chains of the ceramic industry, the LSD-print technology was conceived as a slurry-based variation of binder jetting (BJ).
BJ and other powder bed technologies (such as powder bed fusion) are amongst the most successful AM techniques, especially for metals and polymers, thanks to their high productivity and scalability. The possibility to use commercially available feedstocks (in the form of powders or granules) makes BJ also attractive for ceramic materials. The application of these techniques to most advanced ceramics has however been difficult so far, because of the limitations in depositing homogeneous layers with fine, typically poorly flowable powders.
In this context, the "layerwise slurry deposition" (LSD) was proposed at TU Clausthal (Germany) as a slurry-based deposition of ceramic layers by means of a doctor blade. Combined with layer-by-layer laser sintering of the material, the LSD process was originally demonstrated for the rapid prototyping of silicate ceramics. Due to the difficulties in controlling the microstructure and the defect formation in laser-sintered technical ceramics, the LSD process was later combined with inkjet printing in the LSD-print technology, which has been further developed at BAM (Germany) in the past decade.
The LSD-print technology combines the high speed of inkjet printing, typical of BJ, with the possibility of producing a variety of high-quality ceramics with properties comparable to those achieved by traditional processing. Due to the mechanical stability of the powder bed, the process can also be carried out with continuous layer deposition on a rotating platform, which further increases its productivity.
This presentation will delve into 10 years of research on the LSD-print of a wide variety of technical ceramics including alumina, silicon carbides and dental ceramics. The discussion highlights how a seemingly small process and feedstock modification (from powders to slurries) has great influence on the challenges and potential of this process, which are being addressed on its path to industrialization.
In this work we instigated the fragmentation of Au microparticles supported on a thin amorphous carbon film by irradiating them with a gradually convergent electron beam inside the Transmission Electron Microscope. This phenomenon has been generically labeled as “electron beam-induced fragmentation” or EBIF and its physical origin remains contested. On the one hand, EBIF has been primarily characterized as a consequence of beam-induced heating. On the other, EBIF has been attributed to beam-induced charging eventually leading to Coulomb explosion. To test the feasibility of the charging framework for EBIF, we instigated the fragmentation of Au particles under two different experimental conditions. First, with the magnetic objective lens of the microscope operating at full capacity, i.e. background magnetic field B = 2 T, and with the magnetic objective lens switched off (Lorenz mode), i.e. B = 0 T. We observe that the presence or absence of the magnetic field noticeably affects the critical current density at which EBIF occurs. This strongly suggests that magnetic field effects play a crucial role in instigating EBIF on the microparticles. The dependence of the value of the critical current density on the absence or presence of an ambient magnetic field cannot be accounted for by the beam-induced heating model. Consequently, this work presents robust experimental evidence suggesting that Coulomb explosion driven by electrostatic charging is the root cause of EBIF.
Following the new paradigm of materials development, design, and optimization, digitalization is the main goal in materials sciences and engineering (MSE) which imposes a huge challenge. In this respect, the quality assurance of processes and output data as well as the interoperability between applications following FAIR principles are to be ensured. For storage, processing, and querying of data in contextualized form, Semantic Web technologies (SWT) are used since they allow for machine-actionable and human-readable knowledge representations needed for data management, retrieval, and (re)use.
The project ‘platform MaterialDigital’ (PMD) aims to bring together and support interested parties from both industrial and academic sectors in a sustainable manner in solving digitalization tasks and implementing digital solutions. Therefore, the establishment of a virtual material data space and the systematization of the handling of hierarchical, process-dependent material data are focused. Core points to be dealt with are the development of agreements on data structures and interfaces implemented in distinct software tools and to offer users specific support in their projects. Furthermore, the platform contributes to a standardized description of data processing methods in materials research. In this respect, selected MSE methods are semantically represented on a prototypical basis which are supposed to serve as best practice examples with respect to knowledge representation and the creation of knowledge graphs used for material data.
Accordingly, this poster presentation illustrates demonstrators developed and deployed within the PMD project. Semantically anchored using the mid-level PMD Core Ontology (PMDco), they address data transformation leading to a novel data management which is based on semantic integrated data. The PMD data acquisition pipeline (DAP), which is fueled by traditional, diverse data formats, and a pipeline applying an electronic laboratory notebook (ELN) as data source are displayed. Additionally, the efficient combination of diverse datasets originating from different sources is demonstrated by the representation of a use case dealing with the well-known Orowan relation.
Advanced light weight applications like aircrafts and wind turbine blades are made of fibre reinforced plastics (FRP) with continuous fibre reinforcement and must withstand a high thermo-mechanical cyclic loading. The quality of the fibre matrix interface has a high impact on the fatigue life and was continuously improved over the years since the 50th. The fatigue life of glass fibre reinforced plastics (GFRP) used in aircraft industry is 10 to 100 times higher compared to glass fibre non crimp fabrics used for wind turbine blades.
To assure a constant and reliable high quality and strength of reinforcement fibres, synthetic fibre production is state of the art (CF, GF). There is a need for recycling GFRP and CFRP waste due to the upcoming use. Pyrolysis and solvolysis are more expensive than the mechanical route however enable a more sustainable recycling. Natural fibres and recycled synthetic fibres have a high scatter in quality and strength. Hence it is a challenge to optimize the production / recycling processes to get a reliable quality for any demanding (second life) application.
Chemical routes for using renewables resources and recycling, is going to be a good approach especially for polymer-matrix systems to get 100% quality (back) compared to the state of the art.
Finally, a proper design, life-time extension and repair is preferable to recycling to keep the carbon footprint as low as possible.
Addressing a strategy for publishing open and digital research data, this article presents the approach for streamlining and automating the process of storage and conversion of research data to those of semantically queryable data on the web. As the use case for demonstrating and evaluating the digitalization process, the primary datasets from low‐cycle‐fatigue testing of several copper alloys are prepared. The fatigue test ontology (FTO) and ckan.kupferdigital data management system are developed as two main prerequisites of the data digitalization process. FTO has been modeled according to the content of the fatigue testing standard and by reusing the basic formal ontology, industrial ontology foundry core ontology, and material science and engineering ontology. The ckan.kupferdigital data management system is also constructed in such a way that enables the users to prepare the protocols for mapping the datasets into the knowledge graph and automatically convert all the primary datasets to those machine‐readable data which are represented by the web ontology language. The retrievability of the converted digital data is also evaluated by querying the example competency questions, confirming that ckan.kupferdigital enables publishing open data that can be highly reused in the semantic web.
This data article presents a set of primary, analyzed, and digitalized mechanical testing datasets for nine copper alloys. The mechanical testing methods including the Brinell and Vickers hardness, tensile, stress relaxation, and low-cycle fatigue (LCF) testing were performed according to the DIN/ISO standards. The obtained primary testing data (84 files) mainly contain the raw measured data along with the testing metadata of the processes, materials, and testing machines. Five secondary datasets were also provided for each testing method by collecting the main meta- and measurement data from the primary data and the outputs of data analyses. These datasets give materials scientists beneficial data for comparative material selection analyses by clarifying the wide range of mechanical properties of copper alloys, including Brinell and Vickers hardness, yield and tensile strengths, elongation, reduction of area, relaxed and residual stresses, and LCF fatigue life. Furthermore, both the primary and secondary datasets were digitalized by the approach introduced in the research article entitled “Toward a digital materials mechanical testing lab” [1]. The resulting open-linked data are the machine-processable semantic descriptions of data and their generation processes and can be easily queried by semantic searches to enable advanced data-driven materials research.
Development of efficient portable sensors for accurately detecting biomarkers is crucial for early disease diagnosis, yet remains a significant challenge. To address this need, we introduce the enhanced luminescence lateral-flow assay, which leverages highly luminescent upconverting nanoparticles (UCNPs) alongside a portable reader and a smartphone app. The sensor’s efficiency and versatility were shown for kidney health monitoring as a proof of concept. We engineered Er3+- and Tm3+-doped UCNPs coated with multiple layers, including an undoped
inert matrix shell, a mesoporous silica shell, and an outer layer of
gold (UCNP@mSiO2@Au). These coatings synergistically enhance emission by over 40-fold and facilitate biomolecule conjugation, rendering UCNP@mSiO2@Au easy to use and suitable for a broad range of bioapplications. Employing these optimized nanoparticles in lateral-flow assays, we successfully detected two acute kidney injury-related biomarkers-kidney injury molecule-1 (KIM-1) and neutrophil gelatinase-associated lipocalin (NGAL)-in urine samples. Using our sensor platform, KIM-1 and NGAL can be accurately detected and quantified
within the range of 0.1 to 20 ng/mL, boasting impressively low limits of detection at 0.28 and 0.23 ng/mL, respectively. Validating our approach, we analyzed clinical urine samples, achieving biomarker concentrations that closely correlated with results obtained via ELISA. Importantly, our system enables biomarker quantification in less than 15 min, underscoring the performance of our novel UCNP-based approach and its potential as reliable, rapid, and user-friendly diagnostics.
AbstractGallium fluoride phosphate glasses feature low refractive index, high energy radiation resistance, wide transmission range, and favorable emission characteristics of rare‐earth dopants. For the development of optimized glass compositions, a fundamental understanding of these properties in terms of glass structure is sought. We report nuclear magnetic resonance (NMR) structural studies of glasses in the system xGa(PO3)3–(40 − x)GaF3–20BaF2–20ZnF2–20SrF2 (x = 5, 10, 15, 20, and 25 mol%). 31P NMR results with 71Ga recoupling show that the network structure is dominated by P–O–Ga linkages, and no P–O–P linkages exist. 71Ga NMR results show that Ga is mainly six‐coordinated featuring a mixed fluoride/phosphate coordination. Quantitative estimates of this ligand distribution around gallium were obtained by 71Ga{31P} spin echo double resonance (REDOR) measurements. Photophysical properties suggest changes in the Eu(III) ligand distribution toward a fluoride‐dominated environment at low P/F ratio while the glass network is largely sustained by bridging oxygen atoms via P–O–Ga linkages.
Viscous crack healing in soda–lime–magnesium–silicate–ZrO<sub>2</sub> glass matrix composites
(2024)
AbstractThe present study investigates the influence of the crystal volume content on viscous crack healing in glass ceramic glass sealants. To ensure constant microstructure during healing, soda–lime–magnesium silicate glass matrix composites with varied volume fractions of ZrO2 filler particles were used. Crack healing was studied on radial cracks induced by Vickers indentation, which were stepwise annealed to monitor the healing progress by confocal laser scanning microscopy. Confirming previous studies, healing of radial cracks in pure glass was found delayed by global flow phenomena like crack widening and crack edge and tip rounding to minimize the sample surface. With increasing ZrO2 filler content, these global flow phenomena were progressively inhibited whereas local flow phenomena like sharp crack tip healing could still occur. As a result, crack healing was even accelerated by filler particles up to a maximum filler content of 17 vol% whereas crack healing was fully suppressed only at 33 vol% filler content.
Advanced optical materials inspired by natural minerals and non-toxic light elements, such as the Hackmanites (Na8Al6Si6O24(Cl,S)2), find vast possibilities of applications as they can simultaneously perform photochromism and persistent luminescence (PersL). In this work, we have explored a rapid and energy-efficient microwaveassisted (MASS) methodology for the synthesis of PersL and photochromic hackmanites. In addition, we have prepared hackmanite materials using a zeolite-free precursor to control the Na–Al–Si ratio and study its influence on the materials photoluminescent properties. The PersL hackmanites showed a white-bluish emission color, with up to 2 h of emission time. Zeolite-free photochromic materials were able to change the color from white to purple/blue efficiently with a few seconds of 254 nm excitation, but the usage of zeolite precursors enhanced the overall optical performance. Microwave synthesis times of 10–40 min were demonstrated to be optimal, as longer times boosted the formation of nepheline spurious phase, which decreases luminescence efficiency. In this way, the MASS method led to a reduction of reaction time up to 98 %, yielding hackmanite materials with similar photoluminescent or photochromic properties compared to those obtained by a 24 h conventional solid-state synthesis. This work represents a significant improvement toward coupling eco-friendly synthetic processes to
eco-friendly solid-state materials for PersL illumination and PersL/photochromism optical marking.
Grain boundary embrittlement in medium-Mn steels and liquid metal embrittlement (LME) in Zn-coated high strength steels are among key challenges on the way of safe application of sustainable steels for automotive industry. Using a novel density-based model for grain boundaries, we reveal that the affinity of a grain boundary to attract Mn and Zn atoms result in a segregation transition accompanied by interfacial structural changes. In case of the Zn, the simulations show that the amount of segregation abruptly increases with decreasing temperature, while the Zn content in the alloy, required for triggering the segregation transition, decreases. The results are discussed in the context of CALPHAD-integrated density-based grain boundary phase diagrams.
Low-Temperature High Stress (LTHS) creep plays a crucial role in Ni-base Superalloys, particularly affecting components like blades near the root. Below 850°C, the precipitate microstructure remains stable, characterized by periodically arranged ’ cubic precipitates surrounded by the -matrix. In these conditions, macroscopic traces of cubic slip have been observed in <111> oriented tensile specimens, whereas their microscopic origin has been a topic of debate. Furthermore, in LTHS conditions, Superlattice Intrinsic, Extrinsic Stacking Faults (SISF/SESF), or micro-twins are also frequently reported in crept specimens. Usually, these mechanisms are investigated separately, so that a unified picture and a detailed understanding of these mechanisms and their activation conditions have only recently emerged in the literature, despite the intensive investigations of the last decades.
The objective of this work is to develop a dislocation-based constitutive law that includes these recent developments. In particular, the pseudo-cubic slip mechanism is considered as resulting from the lack of hardening in <111> oriented tensile specimens and is represented by a novel estimate of the back-stresses based on the spectral decomposition of a tensorial representation of the back-stress. An additional novelty is that SISF- and SESF-related slip systems are accounted for as distinct slip systems with corresponding dislocation densities. The model has been implemented as a user-defined constitutive law for commercial Finite Element codes and identified as well as validated with data from the literature obtained with <001>, <011> and <111> oriented crystals tested in tension and compression creep.