5 Werkstofftechnik
Filtern
Dokumenttyp
- Zeitschriftenartikel (400) (entfernen)
Sprache
- Englisch (387)
- Deutsch (6)
- Mehrsprachig (5)
- Französisch (1)
- Russisch (1)
Schlagworte
- Additive manufacturing (26)
- Corrosion (20)
- EBSD (17)
- Additive Manufacturing (16)
- Microstructure (14)
- Creep (13)
- Transmission electron microscopy (13)
- Residual stress (12)
- Glass (11)
- Steel (11)
- Crystallization (9)
- Sintering (8)
- Aging (7)
- Fatigue (7)
- High entropy alloy (7)
- CCS (6)
- Carbon steel (6)
- Electron microscopy (6)
- High temperature corrosion (6)
- Mechanical properties (6)
- SEM (6)
- X-ray diffraction (6)
- 3D printing (5)
- Bioactive glass (5)
- CALPHAD (5)
- Ceramics (5)
- Degradation (5)
- High entropy alloys (5)
- Laser powder bed fusion (5)
- Metallic glasses (5)
- Neutron diffraction (5)
- Oxidation (5)
- Alumina (4)
- EXAFS (4)
- Electron backscatter diffraction (4)
- HIP (4)
- Heat treatment (4)
- High alloyed steel (4)
- Impurities (4)
- Kikuchi patterns (4)
- Lattice parameters (4)
- Martensite (4)
- Metallic glass (4)
- Molecular dynamics (4)
- Nanoindentation (4)
- Nanoparticles (4)
- Ontology (4)
- Pattern matching (4)
- Plastic deformation (4)
- Plasticity (4)
- Raman spectroscopy (4)
- Scanning electron microscopy (4)
- Vickers indentation (4)
- 3D-Printing (3)
- 3D-printing (3)
- AISI 316L (3)
- Binder Jetting (3)
- Calcination (3)
- Carbon fibres (3)
- Ceramic (3)
- Corrosion Fatigue (3)
- Corrosion fatigue (3)
- Coulomb explosion (3)
- Crack propagation (3)
- Crystal plasticity (3)
- Damage (3)
- Diffusion (3)
- Dislocation (3)
- Finite element analysis (3)
- Fracture (3)
- Fracture mechanics (3)
- Fracture toughness (3)
- General Materials Science (3)
- Glass transition (3)
- Grain boundary (3)
- Inconel 718 (3)
- Interfacial strength (3)
- Iron (3)
- Kikuchi diffraction (3)
- Mechanical Engineering (3)
- Mechanics of Materials (3)
- NMR spectroscopy (3)
- Nickel-based superalloys (3)
- Permeability (3)
- Phase-field (3)
- Phase-field simulation (3)
- Pitting (3)
- Reproducibility (3)
- Shape-memory alloys (3)
- Single crystal (3)
- Stress intensity factor (3)
- Superalloy (3)
- TEM (3)
- Thermal expansion (3)
- Ti-6Al-4V (3)
- Viscosity (3)
- X-ray refraction (3)
- Zirconia (3)
- AGIL (2)
- AISI 304L (2)
- Al2O3 (2)
- Alkali zinc borate glasses (2)
- Alloy design (2)
- Aluminosilicate glasses (2)
- Aluminum alloy (2)
- Aluminum alloys (2)
- Aquifer (2)
- Atom probe tomography (2)
- Bacteria (2)
- Binder jetting (2)
- Bioactivity (2)
- Bioceramics (2)
- Bone regeneration (2)
- CCUS (2)
- Calcium cobaltite (2)
- Carbon capture and storage (2)
- Carbon storage (2)
- Characterization (2)
- Chemically complex alloy (2)
- Coating (2)
- Compositionally complex alloys (2)
- Computed Tomography (2)
- Computed tomography (2)
- Condensate (2)
- CrMnFeCoNi (2)
- Crack growth (2)
- Crack healing (2)
- Crop protection products (2)
- Crystal orientation (2)
- Deep Learning (2)
- Defects (2)
- Density-based Phase-Field Modelling (2)
- Densty-based Thermodynamics (2)
- Deuterium (2)
- Diopsid (2)
- Ductile iron (2)
- Elastic constants (2)
- Electron beam-induced fragmentation (2)
- Electron diffraction (2)
- Environmental stress cracking (2)
- Environmental stress cracking (ESC) (2)
- Environmentally assisted cracking (2)
- Foaming (2)
- Fractography (2)
- Fracture surface energy (2)
- Full notch creep test (FNCT) (2)
- GFRP (2)
- Geothermal (2)
- Glass ceramic (2)
- Glass powder (2)
- Glass-ceramic (2)
- Gold (2)
- Grain boundaries (2)
- Grain boundary engineering (2)
- High Alloyed Steel (2)
- High-density polyethylene (2)
- High-entropy alloy (2)
- High-temperature corrosion (2)
- Hydrogen (2)
- IN718 (2)
- Inconel 625 (2)
- Infrared spectroscopy (2)
- Interfacial shear strength (2)
- Internal friction (2)
- Interphase (2)
- Ionic porosity (2)
- Kikuchi pattern (2)
- LPBF (2)
- LTCC (2)
- Laser Powder Bed Fusion (2)
- Laser ablation in liquid (2)
- Laser scanning microscopy (LSM) (2)
- Lattice distortion (2)
- Lattice misfit (2)
- Layerwise Slurry Deposition (2)
- Layerwise slurry deposition (2)
- Lead borate glasses (2)
- Lorenz transmission electron microscopy (2)
- Low cycle fatigue (2)
- Lunar regolith (2)
- Machine Learning (2)
- Mars (2)
- Martensitic transformation (2)
- Mass transport (2)
- Microhardness (2)
- Microstrucrue Design (2)
- Microstructural characterization (2)
- Microstructure Design (2)
- Microstructure and texture (2)
- Microstructure evolution (2)
- Modeling (2)
- Nano-powder (2)
- Native oxide (2)
- Nickel alloys (2)
- Nickel-base superalloys (2)
- Niobium alloying (2)
- Orientation precision (2)
- Ostwald ripening (2)
- Oxyfuel (2)
- P92 (2)
- Particle morphology (2)
- Phase transformations (2)
- Polyethylene (2)
- Polymer (2)
- Porosity (2)
- Preceramic polymer (2)
- Precipitation (2)
- Pressure-assisted sintering (2)
- Quasicrystal (2)
- Rapid solidification (2)
- Reaction-sintering (2)
- Relaxation (2)
- Roughness (2)
- S-Phase (2)
- SIMS (2)
- Sample preparation (2)
- Selective laser melting (2)
- Self-healing (2)
- Shear bands (2)
- Short-range order (2)
- Silicon carbide (2)
- Silicon nanowires (2)
- Single-crystals (2)
- Solubility (2)
- Sorption (2)
- Space (2)
- Spray drying (2)
- Steels (2)
- Stress corrosion cracking (2)
- Stress relaxation (2)
- Sulfidation (2)
- Sulphidation (2)
- Superalloys (2)
- Superconducting magnet (2)
- Surface treatments (2)
- Tempered martensite-ferritic steel (2)
- Tensile properties (2)
- Texture (2)
- Thermodynamics (2)
- Thermoelectric properties (2)
- Thermography (2)
- Titanium oxide (2)
- ToF-SIMS (2)
- Transmission electron microscopy (TEM) (2)
- Viscous sintering (2)
- Water content (2)
- Water speciation (2)
- Wetting (2)
- X-ray absorption spectroscopy (2)
- 12%Cr steel (1)
- 150 Years (1)
- 2PP (1)
- 316L (1)
- 3D Druck (1)
- 3D etching (1)
- 3D metallography (1)
- 3D-Metallographie (1)
- 3D-finite element modeling (1)
- 4-Dimensional scanning transmission (1)
- 9-12%Cr steel (1)
- ATZ (1)
- Abrasion (1)
- Accelerated temporal integration (1)
- Acid-leaching (1)
- Additive Fertigung (1)
- Additive manufactured Ni-base superalloys (1)
- Adolf Martens (1)
- Advanced high strength steels (1)
- Advanced wastewater treatment (1)
- Ageing (1)
- Agglomerates (1)
- Aggressive environments (1)
- Al alloys (1)
- Al-Cu alloy (1)
- Al-Cu binary alloy system (1)
- Al-Cu-Li-alloy (1)
- Alcium alkali phosphate (1)
- Alkali aluminosilicate glasses (1)
- Alkali and alkaline earth silicate and borate glass (1)
- Alkali-activated materials (1)
- Alloy (1)
- Alloy Safety (1)
- Alloy microstructure (1)
- Alloys (1)
- Alloys' Safety (1)
- Alpha-tricalcium phosphate (1)
- Alterung (1)
- Alumina coatings (1)
- Alumina toughened zirconia (1)
- Aluminium alloys (1)
- Aluminiumlegierung (1)
- Aluminum Alloy Aging (1)
- Amorphization (1)
- Amorphous silica (1)
- Analytical scanning electron microscopy (1)
- Angle measurement (1)
- Annealing (1)
- Anticorrosion (1)
- Approximant (1)
- Aquifer fluid (1)
- Artificial weathering (1)
- Atomistic Simulation (1)
- Atomistic simulations (1)
- Austenite-to-martensite phase transformation (1)
- Austenitic alloys (1)
- Austenitic steel 316L (1)
- Automated Bragg angle determination (1)
- Automated analysis (1)
- Automated image analysis (1)
- BTEX (1)
- Bacterial attachment (1)
- Batch reactions (1)
- Behmite (1)
- Biaxial strength (1)
- Bimodal distribution (1)
- Binders/binding (1)
- Bio Ceramic (1)
- Bio Ceramics (1)
- Bio active ceramic (1)
- Bio-ceramic engineering (1)
- Bioactive Glass (1)
- Bioactive bone grafting material (1)
- Bioactive glass scaffold (1)
- Biodiesel (1)
- Biogeochemical cycling (1)
- Biogeochemistry (1)
- Biomineralisation (1)
- Biopolymer (1)
- Biphasic calcium phosphate (1)
- Bitter technique (1)
- Blended learning (1)
- Bond energy (1)
- Bone marrow-derived mesenchymal stem cell (1)
- Borate (1)
- Borosilicate glass (1)
- Bragg angles (1)
- Brass (1)
- Bravais lattice (1)
- Bravais lattices (1)
- Brinell hardness (1)
- Brittle fracture (1)
- Brown-rot fungi (1)
- Bruchflächen (1)
- Bubble formation (1)
- Bulk metallic glasses (1)
- Burst (1)
- C. lap-shear (1)
- CALPHAD database analysis (1)
- CCUS, supercritical/dense phase CO2, carbon steels, martensitic steel, superaustenite steel, droplet corrosion (1)
- CFRP (1)
- CO2 (1)
- CO2 pipeline transport (1)
- CO2 quality (1)
- CO2 separation membranes (1)
- Cabon capture and storage (1)
- Calcium Cobaltite (1)
- Calcium alkali orthophosphate materials (1)
- Calculated intrinsic fracture toughness (1)
- Carbide phase NbC (1)
- Carbidic austempered ductile iron (1)
- Carbon Fiber Reinforced Plastics (1)
- Carbon Fibre (1)
- Carbon capture (1)
- Carbon capture storage (1)
- Carbon capture, utilization and storage technology (1)
- Carbon dioxide (1)
- Carbon nanotubes (1)
- Casing (1)
- Cavitation (1)
- Ccs (1)
- Cellular substructure (1)
- Cellulose (1)
- Cement (1)
- Cement-based materials (1)
- Ceramic multilayers (1)
- Ceramic nano particles (1)
- Ceramics 3D printing (1)
- Cerium oxide (1)
- Chalcogenides (1)
- Characterisation (1)
- Chemo-mechanical coupling (1)
- Chemometrics (1)
- Chrystal orientation (1)
- Classification (1)
- Clay ISRU (1)
- Co-firings (1)
- Co2-Storage (1)
- Cobald based alloy (1)
- Coefficient of thermal expansion (1)
- Composite (1)
- Composite recycling (1)
- Compositionally complex alloy (1)
- Concrete 3D-printing (1)
- Condensed Matter Physics (1)
- Confined catalyst (1)
- Coniophora puteana (1)
- Contact angle (1)
- Contact fatigue (1)
- Contact mechanics (1)
- Cooling rate (1)
- Coordinate measurement machine (1)
- Copper vacancies (1)
- Corrosion costs (1)
- Corrosion mechanism (1)
- Corrosion pits (1)
- Corrosion protection (1)
- Corrosion resistance (1)
- Coûts de la corrosion (1)
- CrCoNi (1)
- CrN/NbN (1)
- Crack arrest (1)
- Crack evolution (1)
- Crack growth in air (1)
- Crack initiation (1)
- Crack opening displacement (1)
- Crack tip opening displacement (1)
- Cracks (1)
- Craze–crack mechanism (1)
- Creation-relaxation algorithm (1)
- Creep behavior (1)
- Creep mechanisms (1)
- Creep strength (1)
- Creep under thermal cycling (1)
- Creep-fatigue (1)
- Creep-fatigue interaction (1)
- Critical energy release rate (1)
- Cross-sectioning (1)
- Crosslinking (1)
- Cryogenic (1)
- Cryogenic cycling (1)
- Crystal Texture (1)
- Crystal growth (1)
- Crystal growth velocity (1)
- Crystal lattice (1)
- Crystal lattice period (1)
- Crystal morphology (1)
- Crystalline defects (1)
- Crystallographic texture (1)
- Cubical shape (1)
- Cupriavidus metallidurans (1)
- Cuttlefish (1)
- Cyclic softening (1)
- Cyclic steam oxidation (1)
- Cytocompatibility (1)
- D. aging (1)
- D. creep D. viscoelasticity (1)
- DCB (1)
- DCB geometry (1)
- Data Interoperability (1)
- Data analysis (1)
- Data infrastructures (1)
- Data mapping (1)
- Data processing (1)
- Datenbank (1)
- Debinding (1)
- Debonding (1)
- Defect detection (1)
- Defects engineering (1)
- Deformation (1)
- Deformation mechanisms (1)
- Degradation signatures (1)
- Density-based Model (1)
- Density-based Thermodynamics (1)
- Density-based model (1)
- Dental (1)
- Dentine (1)
- Deposition microstructure (1)
- Design of experiment (1)
- Desorption (1)
- Destabilization (1)
- Dielectric breakdown (1)
- Dielectric properties (1)
- Diesel (1)
- Diesel Fuel (1)
- Differential scanning calorimetry (1)
- Differential scanning calorimetry (DSC) (1)
- Diffraction (1)
- Diffraction Enhanced Imaging (1)
- Diffraction contrast (1)
- Diffusivity (1)
- Digital image correlation (1)
- Digital representations (1)
- Digital workflows (1)
- Digitalization (1)
- Dimensional mismatch of crystalline lattice periods (misfit) (1)
- Directional grain growth (1)
- Dislocation avalanches (1)
- Disorientation (1)
- Dispersion process (1)
- Distributed fiber optic sensing (1)
- Diversity (1)
- Domain Ontology Development (1)
- Double notched creep specimen (1)
- Dry preparation (1)
- Drywood termite (1)
- Dwell periods (1)
- Dwell times (1)
- Dynamic recrystallization (1)
- EFTEM (1)
- EN AW-2618A (1)
- Early oxidation (1)
- Early stages (1)
- Early sulfidation (1)
- Efficiency (1)
- Elastic energy (1)
- Elastic microstructure (1)
- Elastic modulus (1)
- Elastic properties (1)
- Elasticity (1)
- Electric conductivity (1)
- Electrical insulators (1)
- Electrical resistance (1)
- Electrochemical characterisation (1)
- Electrochemical deposition (1)
- Electrochemical impedance spectroscopy (1)
- Electron back-scattered diffraction (1)
- Electron backscattered diffraction (1)
- Electron beam-induced charging (1)
- Electron energy (1)
- Electron microscopy, transmission (1)
- Electronic (1)
- Enamel (1)
- End of life (1)
- Endothelial progenitor cell (1)
- Endurance Limit (1)
- Energiedisersive Röntgenspektroskopie (1)
- Energy distribution (1)
- Environment (1)
- Environmental Stress Cracking (1)
- Epitaxial films (1)
- Epoxy Resin (1)
- Epoxy resin (1)
- Equilibrium relaxation (1)
- Eutectic (1)
- Expanding cavity model (1)
- Experimental and numerical techniques (1)
- Explosive welding (1)
- Exposed metal sites (1)
- FAIR (1)
- FAIR Data Management (1)
- FAIR research data management (1)
- FIB Tomography (1)
- FSDC (1)
- Fabrication (1)
- Faceting (1)
- Facilitated activation (1)
- Failure mechanisms (1)
- Failure rate (1)
- Fatigue Testing (1)
- Fatigue crack propagation stages (1)
- Fatigue damage (1)
- Fatigue performance (1)
- Fatigue striations (1)
- Fe-Mn steels (1)
- Femtosecond laser (1)
- Ferritic steels (1)
- Ferritic–martensitic steel (1)
- Ferrous phosphate hydrate (1)
- Fiber-matrix interface (1)
- Fiber/matrix bond (1)
- Fibre reinforced plastic (1)
- Fibre/matrix bond (1)
- Fibre/matrix bonding (1)
- Filters (1)
- Finite element method (1)
- Finland (1)
- Firing (1)
- First derivative (1)
- Flowability (1)
- Fluoride nanoparticles (1)
- Fluorolytic sol−gel (1)
- Four-point bending test (1)
- Fourier series (1)
- Fourier transform infrared spectroscopy (1)
- Fracture surface analysis (1)
- Fracture surfaces (1)
- Fragility (1)
- Fraktographie (1)
- Freeze casting (1)
- Fresnoite (1)
- Friction (1)
- Friction Stir Welding (1)
- Friction stir processing (1)
- Frozen state photopolymerization (1)
- Fuel sorption (1)
- Full Notch Creep Test (1)
- Full notch creep test (1)
- Fullerite (1)
- Functional fatigue (1)
- Fungi (1)
- GD-OES (1)
- GMR (1)
- GMR sensors (1)
- Gas flow assisted powder deposition (1)
- Gefügeanalyse (1)
- Gefügerekonstruktion (1)
- General Chemistry (1)
- General Computer Science (1)
- General Engineering (1)
- Geometrical factors (1)
- Glass Ceramic (1)
- Glass capillaries (1)
- Glass crystallization stress (1)
- Glass fiber reinforced polymer (1)
- Glass fiber reinforced polymers (1)
- Glass fiber-epoxy composites (1)
- Glass fibre (1)
- Glass forming (1)
- Glass forming melts (1)
- Glass liner (1)
- Glass manufacturing (1)
- Glass-ceramics (1)
- Glass-ceramics definition (1)
- Global stability criterion (1)
- Gnomonic projections (1)
- Grade S960QL steel (1)
- Gradient-enhanced fatigue model (1)
- Grain Boundary (1)
- Grain Boundary Corrosion (1)
- Grain Boundary Phase Diagram (1)
- Grain Boundary Segregation (1)
- Grain Boundary Spinodal (1)
- Grain boundary oxidation (1)
- Grain boundary phase diagram (1)
- Grain boundary precipitates (1)
- Grain boundary structure (1)
- Grain boundary thermodynamics (1)
- Grain growth (1)
- Grain structure (1)
- Granules (1)
- Graphite (1)
- Growth kinetics (1)
- Growth rate (1)
- Hausner ratio (1)
- Heat accumulation (1)
- Heat-resistant nickel alloys (1)
- Hertzian cracks (1)
- Hierarchical microstructure (1)
- Hierarchical microstructure Premartensite (1)
- Hierarchical porosities (1)
- High - temperature (1)
- High Cycle Fatigue (1)
- High Entropy Alloy (1)
- High Entropy Alloys (1)
- High density polyethylene (1)
- High interstitial austenitic steel (1)
- High pressure (1)
- High temperature nickel-based eutectic alloys (1)
- High temperature oxidation (1)
- High temperatures (1)
- High-Entropy Alloys (1)
- High-Entropy Materials (1)
- High-entropy alloys (1)
- High-temperature oxidation (1)
- High-temperature properties (1)
- High-voltage testing (1)
- High‐temperature corrosion (1)
- Hipims (1)
- Hochleistungskeramik (1)
- Homogenization (1)
- Hot isostatic pressing (HIP) (1)
- Hot pressing (1)
- Hot stage microscopy (1)
- Hybrid Manufacturing (1)
- Hydrogel (1)
- Hydrogen diffusivity (1)
- Hydrogen permeation (1)
- Hydrogen storage (1)
- Hydrogen storage tank (1)
- Hydrothermal Ageging (1)
- Hydrous glass (1)
- Hygrothermal (1)
- IASCC (1)
- IN 718 (1)
- IR spectroscopy (1)
- ISRU (1)
- Impact damage (1)
- Impact wear (1)
- In situ diffraction (1)
- In situ tensile test (1)
- In situ thermal-annealing experiment (1)
- In-situ ED-XRD (1)
- In-situ Process Monitoring (1)
- In-situ SEM micro shear deformation (1)
- In-situ composites (1)
- In-situ diffraction (1)
- In-situ process monitoring (1)
- In-vivo (1)
- Incipient plasticity (1)
- Inclusion cluster (1)
- Inclusion size (1)
- Inconel 686 (1)
- Incremental lifetime models (1)
- Indentation (1)
- Indentation fracture toughness (1)
- Indentation hardness (1)
- Industrial and Manufacturing Engineering (1)
- Infrared nano AFM (1)
- Infrarotspektroskopie (1)
- Inkjet (1)
- Inter layer time (1)
- Interdiffusion (1)
- Interface (1)
- Interfacial Strength (1)
- Interfacial anisotropy (1)
- Interfacial free energy (1)
- Interlaboratory comparability (1)
- Intermetallic (1)
- Intermittent microplasticity (1)
- Intermodulation AFM (1)
- Internal Sulfidation (1)
- Internal Surfaces (1)
- Internal oxidation (1)
- Internal stresses (1)
- Intrinsic stress (1)
- Invar (1)
- Inverted classroom (1)
- Ion beam erosion Sectioning (1)
- Iron meteorite (1)
- Iron oxide (1)
- Irradiation (1)
- Isostatic hot pressing (HIP) (1)
- JMAK model (1)
- Joints/joining (1)
- KCl (1)
- KI (1)
- Kernel average misorientation (1)
- Keywords: Poly(ether ether ketone) (1)
- Kikuchi bands (1)
- Knowledge Graph (1)
- Knowledge Representation (1)
- Knowledge graphs (1)
- Knowledge representation (1)
- LIBS (1)
- LSD print (1)
- Laboratory X-ray diffraction (1)
- Laser (1)
- Laser Powder Bed Fusion (LPBF) (1)
- Laser beam melting (1)
- Laser beam melting (LBM) (1)
- Laser cladding (1)
- Laser powder-based directed energy deposition (1)
- Laser-induced slip casting (1)
- Lattice distortions (1)
- Lattice parameter determination (1)
- Lattice point density (1)
- Lattice rotation (1)
- Lattice structures (1)
- Lattices (1)
- Laves phase (1)
- Layered manganese oxide (1)
- Layering misalignment (1)
- Lebensdauervorhersage (1)
- Lecture films (1)
- Li-ion battery (1)
- Lifetime prediction (1)
- Light curing (1)
- Lindemann criterion (1)
- Linear elastic fracture mechanics (1)
- Linked open data (1)
- Liquid Metal Embrittlement (1)
- Liquid metal embrittlement (1)
- Liquid phase sintering (1)
- Liquid-metal embrittlement (1)
- Lithography-based technologies (1)
- Log-normal distribution (1)
- Long-term aging (1)
- Long-term calculation (1)
- Long-term storage (1)
- Low carbon steel (1)
- Low expansion (1)
- Low strain (1)
- Low-cycle fatigue (1)
- Low-loading (1)
- MGS-1 regolith simulant (1)
- MOF-74 (1)
- MOUSE (1)
- Machine learning (1)
- Magmatic and hydrothermal processes (1)
- Magnetic domain distribution (1)
- Magnetic shape memory (1)
- Magnetic stray field (1)
- Magnetic stray fields (1)
- Magnetomechanical effect (1)
- Martensitic steel (1)
- Martensitic steels (1)
- Martensitic structure (1)
- Master curve (1)
- Material degradation (1)
- Material failure (1)
- Material modeling (1)
- Materials Chemistry (1)
- Materials Modelling (1)
- Materials Testing (1)
- Materials informatics (1)
- Materials science (1)
- Materials science and engineering (1)
- Matrix residual stress (1)
- Mean atomic number (1)
- Mean-field modelling (1)
- Mechanical anisotropy (1)
- Mechanical behavior (1)
- Mechanical deformation (1)
- Medium Entropy Alloys (1)
- Medium entropy alloys (1)
- Melt pool boundary (1)
- Melting (1)
- Meta material (1)
- Metal Magnetic Memory (1)
- Metal additive manufacturing (1)
- Metal and alloys (1)
- Metal magnetic memory (1)
- Metallic Glass (1)
- Metallic materials (1)
- Metals and Alloys (1)
- Methodology (1)
- Micro-shrinkages (1)
- Microplastic stress (1)
- Microplastics (1)
- Microsegregation (1)
- Microstructur (1)
- Microstructural changes of a Fe Si alloy (1)
- Microstructural evolution (1)
- Microstructure analysis (1)
- Microstructure, γ/γ' misfit (1)
- Microstrucure reconstruction (1)
- Microwave technology (1)
- Mikrostruktur (1)
- Milling (1)
- Mis-match (1)
- Misfitting precipitate (1)
- Misorientation (1)
- Mixed Ca-K-Na phosphates (1)
- Mixed conductors (1)
- Mixed-linkers (1)
- Mn-oxides (1)
- Mobility (1)
- Model (1)
- Moisture (1)
- Molecular Dynamics (1)
- Molten salt (1)
- Moon (1)
- Multiaxial deformation (1)
- Multilayer (1)
- Multilayer ceramic technology (1)
- Multilayers (1)
- Multiple cracks (1)
- NGS (1)
- Na and K rhenanites (1)
- Nano CRM (1)
- Nano-ceramic-additive-manufacturing photoresin (1)
- Nano-composite (1)
- Nano-scratch test (1)
- NanoCAM (1)
- Nanocomposites (1)
- Nanocrystalline alloys (1)
- Nanocrystalline structure (1)
- Nanoelectromechanical systems (NEMS) (1)
- Nanomaterials (1)
- Nanoparticle structure (1)
- Nanopowder (1)
- Nanoribbons (1)
- Nanoscale multilayers (1)
- Nanostructure quantification (1)
- Natural (1)
- Natural silver wires (1)
- Nb3Sn (1)
- Near Infrared Spectroscopy (1)
- Networking (1)
- Neutron Diffraction (1)
- Ni-Mn-Ga (1)
- NiMaGa (1)
- NiTi (1)
- Nickel-base alloy (1)
- Nitride (1)
- Non-destructive Materials (1)
- Non-metallic inclusions (1)
- Non-serrated inhomogeneous flow (1)
- Notch (1)
- Nucleation (1)
- Nucleation tendency (1)
- Number density (1)
- Nydrogen melting (1)
- Online Process Monitoring (1)
- Ontologies (1)
- Optical and Magnetic Materials (1)
- Optical centrifugation (1)
- Optical criterion of brittleness (1)
- Ordered/disordered structures (1)
- Ordering (1)
- Orientation (1)
- Orientation refinement (1)
- Orientation relationship (1)
- Orowan Mechanism (1)
- Osteogenesis (1)
- Oxidation protection (1)
- Oxide (1)
- Oxide coatings (1)
- Oxygen evolution reaction (1)
- PBF-LB/M/316L (1)
- PE-HD Sorption (1)
- PLS-DA (1)
- PV modules (1)
- Packaging (1)
- Parabolic flight (1)
- Parametric modeling (1)
- Particle size (1)
- Particle-bed binder jetting (1)
- Passive components and circuits (1)
- Permittivity reduction (1)
- Phase Diagram (1)
- Phase diagram (1)
- Phase field crystal (1)
- Phase field method (1)
- Phase field model (1)
- Phase separation (1)
- Phase stability (1)
- Phase transformation (1)
- Phase-Field Simulations (1)
- Phase-field model (1)
- Phase-field modelling (1)
- Phosphate (1)
- Photocleavable organosilanes (1)
- Photopolymer composites (1)
- Phototrophs (1)
- Photovoltaic modules (1)
- Physical aging (1)
- Physical properties (1)
- Phytolith (1)
- Pipeline network (1)
- Pitting corrosion (1)
- Plasma imaging (1)
- Plasma nanocoatings (1)
- Plasma spray (1)
- Platinum-group-metals (1)
- Polyaniline (1)
- Polymer analysis/characterization (1)
- Polymer composite (1)
- Polymer matrix composites (1)
- Polymer-ceramic mixtures (1)
- Polymer-matrix composites (PMC) (1)
- Polymeric Materials (1)
- Polymer–matrix composites (1)
- Polyolefins (1)
- Polypropylene (1)
- Polystyrene (1)
- Polyurethane (1)
- Porcelain (1)
- Pore (1)
- Pores (1)
- Porosification (1)
- Porous materials (1)
- Portfolio (1)
- Positron annihilation spectroscopy (1)
- Powder bed additive manufacturing (1)
- Powder bed density (1)
- Powder diffraction (1)
- Powder flow (1)
- Powder processing (1)
- Powder rheology (1)
- Powder-based processes (1)
- Powdered activated carbon (1)
- Power factor (1)
- Power law (1)
- Precipitate shape (1)
- Pressure assisted sintering (1)
- Preventive strategies (1)
- Principal stress (1)
- Principal stress components (1)
- Printing (1)
- Process (1)
- Process development (1)
- Processing window (1)
- Production scatter (1)
- Projection center (1)
- Projekt AGIL - Alterung additiv gefertigter metallischer Materialien und Komponenten (1)
- Properties (1)
- Protection (1)
- Pseudosymmetry (1)
- Pull-out composite materials (1)
- Pultruded fiber rods (1)
- Pulveraktivkohle (1)
- Quality assurance (1)
- Radon transform (1)
- Reaction Sintering (1)
- Real-time deformation (1)
- Real-time qPCR (1)
- Recommendations (1)
- Recycling (1)
- Reference data (1)
- Reference nanoparticles (1)
- Refractory alloy (1)
- Refractory high entropy alloys (1)
- Refractory superalloys (1)
- Regolith (1)
- Reheating (1)
- Rejuvenation (1)
- Relaxation fatigue (1)
- Reliability (1)
- Residual Stress (1)
- Residual strains (1)
- Residual stresses (1)
- Resistance spot welding (1)
- Resistance stress (1)
- Resonance testing (1)
- Review (1)
- Rhodonia placenta (1)
- Round Robin (1)
- S-phase (1)
- SAXS (1)
- SDC (1)
- SEM micrography (1)
- SEM wood characterization (1)
- SLM (1)
- SO2 (1)
- STEM (1)
- Safety (1)
- Safety assessment (1)
- Samarium doped ceria (1)
- Sample holder (1)
- Sand blasting (1)
- Sandwich (1)
- Scaffold (1)
- Scaffold geometry (1)
- Scaffolds (1)
- Scale-dependent behavior (1)
- Scan strategies (1)
- Scanning acoustic microscopy (SAM) (1)
- Scanning transmission electron microscopy (STEM) (1)
- Scarf joint (1)
- Scavenging effect of iron (1)
- Schadensanalyse (1)
- Schlickerdeposition (1)
- SchwarzP cells (1)
- Schwingstreifen (1)
- Schädigung (1)
- Scratches (1)
- Segregation (1)
- Segregation Engineering (1)
- Segregation engineering (1)
- Selective laser melting (SLM) (1)
- Self-Assembly (1)
- Self-organization (1)
- Semantic Data Integration (1)
- Semantic Interoperability (1)
- Semantic Web Technologies (1)
- Semantic data integration (1)
- Semantic interoperability (1)
- Semantic web (1)
- Serial sectioning (1)
- Serienschnitte (1)
- Sewage treatment plant (1)
- Shadowgraphy (1)
- Shape memory alloy (1)
- Shape memory alloys (1)
- Shear (1)
- Shear load (1)
- Shear modulus (1)
- Shear strain (1)
- Shear testing (1)
- Shear thinning (1)
- Shear-band cavitation (1)
- Shear-band structure (1)
- Short range order (1)
- Short-beam strength (1)
- Silicate glass (1)
- Silicate glass-ceramics (1)
- Silicoborate glasses (1)
- Silicon Carbide (1)
- Silicon release (1)
- Silikatkeramik (1)
- Silver metallization paste (1)
- Simulation (1)
- Single crystal Ni-Base superalloys (1)
- Single crystal superalloys (1)
- Single fiber pull-out test (1)
- Single-Crystal (1)
- Single-crystal (1)
- Sinter retardation (1)
- Sintering additive (1)
- Sinus floor augmentation (1)
- Size (1)
- Size effect (1)
- Sliding simulation (1)
- Slip localization (1)
- Slip-rolling (1)
- Slow crack growth (1)
- Slow crack growth (SCG) (1)
- Slurry (1)
- Slurry optimization (1)
- Small-angle scattering (1)
- Small-scale (1)
- Smart materials (1)
- Smectite (1)
- Soda lime silicate glass (1)
- Soda-lime silicate glass (1)
- Soda-lime-silica (1)
- Soda-lime-silica glass (1)
- Sodium ion batteries (1)
- Softening temperature (1)
- Soil (1)
- Sol-gel coating (1)
- Solar panels (1)
- Solid-State-Synthesis (1)
- Solid-state-synthesis (1)
- Spar cap design (1)
- Specimen geometry (1)
- Spinodal decomposition (1)
- Split-vacancy defect complexes (1)
- Stable crack growth (1)
- Stainless steel (1)
- Standardisation (1)
- Statistics (1)
- Steam oxidation resistance (1)
- Steel P92 (1)
- Steel alloy (1)
- Stereoscopy (1)
- Strain (1)
- Strain difference (1)
- Strain energy (1)
- Stratégies deprévention (1)
- Stress distribution (1)
- Stress intensity (1)
- Stress-corrosion (1)
- Stress-strain behavior (1)
- Stress-strain-behavior (1)
- Structural composites (1)
- Structural defects (1)
- Structural dynamics (1)
- Structural health monitoring (1)
- Structural steel (1)
- Subcritical crack growth (1)
- Sulfiding (1)
- Superalloy single crystals (1)
- Superelasticity (1)
- Superlattice extrinsic stacking faults (1)
- Supersaturation (1)
- Support configurations (1)
- Support vector machines (1)
- Surface (1)
- Surface crystallization (1)
- Surface elasticity (1)
- Surface energy (1)
- Surface modification (1)
- Surface nucleation (1)
- Surface roughness (1)
- Surface stress (1)
- Surface-induced Melting (1)
- Swept wavelength interferometry (1)
- Symmetric dwell periods (1)
- Synchrotron X-ray diffraction (1)
- Synchrotron micro-tomography (1)
- Synchrotron radiations (1)
- Synthesis (1)
- T1 precipitate (1)
- TIG-welding (1)
- Technical Ceramics (1)
- Temperature (1)
- Temperature dependence (1)
- Tensile Test Ontology (1)
- Tensile strength (1)
- Tensile testing (1)
- Tetragonal distortion (1)
- Tetragonality (1)
- Thermal Cycling (1)
- Thermal cycling (1)
- Thermal desorption mass spectrometry (1)
- Thermo-mechanical loading (1)
- Thermo-mechanics (1)
- Thermoanalysis (1)
- Thermobimetal (1)
- Thermoelectric oxide (1)
- Thermoelectric oxides (1)
- Thermoelectrics (1)
- Thermogravimetrie (1)
- Thermogravimetry (1)
- Thermomechanical fatigue (1)
- Thermoplastic matrix (1)
- Thermoplastic prepreg (1)
- Thermoset composition (1)
- Thermosetting resin (1)
- Thickening (1)
- Thin films (1)
- Thin tribofilm (1)
- Thiol-ene click chemistry (1)
- Three-dimensional Bone tissue engineering (1)
- Three-dimensional tomographies (1)
- Titanium (1)
- Tooth wear (1)
- Topography (1)
- Toughness (1)
- Transformer (1)
- Transmission Kikuchi diffraction (1)
- Transmission electron microscope (TEM) (1)
- Transmissionselektronenmikroskopie (1)
- Transmittance (1)
- Transparency (1)
- Transparent ceramic (1)
- Tribology (1)
- Tricalcium Phosphate (1)
- Triply Periodical Minimal Surface (1)
- Tungsten carbide (1)
- Tungsten-Rhenium (1)
- Turbine disk (1)
- Twinning (1)
- Two-photon adsorption (1)
- Two-photon polymerization (1)
- Two-photon-polymerization (1)
- UV-irradiation (1)
- Ultrasonic assited machining (1)
- Ultrasound (1)
- Unidirectional composites (1)
- Utilization, and storage (CCUS) technology (1)
- Vacancies (1)
- Vickers hardness (1)
- Viscoelastic model (1)
- Viscoplasticity (1)
- Visual ontology development (1)
- Visualization (1)
- Vivianite (1)
- Vocabulary providers (1)
- Volatiles from thermosets (1)
- Volume changes (1)
- Volume fraction (1)
- WAXS (1)
- Water (1)
- Water Diffusion (1)
- Water droplet erosion resistance (1)
- Water in glass (1)
- Welding (1)
- Wet chemical etching (1)
- Whole-chain CCS scenario (1)
- Wood protection (1)
- Work of adhesion (1)
- X-ray Diffraction (1)
- X-ray computed tomography (CT) (1)
- X-ray diffraction analysis (1)
- X-ray tomographic (1)
- X-ray-diffraction (1)
- XPCS (1)
- XRD (1)
- Young's modulus (1)
- Young`s modulus (1)
- Young´s modulus (1)
- Young’s Modulus (1)
- Yttria stabilized zirconia (1)
- Zinc oxide (1)
- Zirconia-toughened alumina (1)
- ZnO (1)
- arbidic austempered ductile iron (1)
- battery aging mechanism (1)
- bioactive (1)
- biomaterials (1)
- bone (1)
- corrosion (1)
- current collector corrosion (1)
- depth profiles (1)
- electron microscopy (1)
- high entropy alloys (1)
- high pressure (1)
- hydrogen storage (1)
- in-situ synthesis (1)
- infrared spectroscopy (1)
- microstructural changes (1)
- negative crystal growth (1)
- oxidation (1)
- phosphate glasses (1)
- scanning electron microscopy (1)
- sulfidation (1)
- water speciation (1)
- µ-gravity (1)
- γ- и γ'-фазы, период кристаллической решетки (1)
- γ/γ' matrix (1)
- γ″ phase (1)
- θ′ phase (1)
- θ′-(Al2Cu) precipitate phase (1)
- высокие температуры (1)
- жаропрочные нике- левые сплавы (1)
- монокристалл (1)
- рентгеноструктурный анализ (1)
Organisationseinheit der BAM
- 5 Werkstofftechnik (400)
- 5.1 Mikrostruktur Design und Degradation (151)
- 5.4 Multimateriale Fertigungsprozesse (72)
- 5.2 Metallische Hochtemperaturwerkstoffe (66)
- 5.6 Glas (51)
- 5.5 Materialmodellierung (46)
- 5.0 Abteilungsleitung und andere (41)
- 5.3 Polymere Verbundwerkstoffe (39)
- 9 Komponentensicherheit (37)
- 8 Zerstörungsfreie Prüfung (34)
Paper des Monats
- ja (11)
In the past two decades, numerous relaxation or physical aging experiments of metallic glasses have revealed signatures of intermittent atomic-scale processes. Revealed via intensity cross-correlations from coherent scattering using X-ray photon correlation spectroscopy (XPCS), the observed abrupt changes in the time-domain of atomic motion does not fit the picture of gradual slowing down of relaxation times and their origin continues to remain unclear. Using a binary Lennard-Jones model glass subjected to microsecond-long isotherms, we show here that temporally and spatially heterogeneous atomic-cluster activity at different length-scales drive the emergence of highly non-monotonous intensity cross-correlations. The simulated XPCS experiments reveal a variety of time-dependent intensity-cross correlations that, depending on both the structural evolution and the 𝑞-space sampling, give detailed insights into the possible structural origins of intermittent aging measured with XPCS.
Reliable measurement of the size of polydisperse, complex-shaped commercial nanopowders is a difficult but necessary task, e.g., for regulatory requirements and toxicity risk assessment. Suitable methods exist for the accurate characterization of the size of non-aggregated, stabilized, spherical and monodisperse nanoparticles. In contrast, industrial nanoscale powders usually require dedicated sample preparation procedures developed for the analysis method of choice. These nano-powders tend to agglomerate and/or aggregate, a behavior which in combination with an innate broad particle size distribution and irregular shape often significantly alters the achievable accuracy of the measured size parameters. The present study systematically tests two commercially available nanoscale powders using different sample preparation methods for correlative analysis by scanning electron microscopy, dynamic light scattering, Brunauer–Emmet–Teller method and differential mobility analysis. One focus was set on the sample preparation by embedding nanoparticles in carbon-based hot-mounting resin. Literature on this topic is scarce and the accuracy of the data extracted from cross sections of these particles is unclearly stated. In this paper systematic simulations on the deviation of the size parameters of well-defined series of nanoparticles with different shapes from the nominal value were carried out and the contributing factors are discussed.
AbstractHigh-strength aluminum alloys used in aerospace and automotive applications obtain their strength through precipitation hardening. Achieving the desired mechanical properties requires precise control over the nanometer-sized precipitates. However, the microstructure of these alloys changes over time due to aging, leading to a deterioration in strength. Typically, the size, number, and distribution of precipitates for a quantitative assessment of microstructural changes are determined by manual analysis, which is subjective and time-consuming. In our work, we introduce a progressive and automatable approach that enables a more efficient, objective, and reproducible analysis of precipitates. The method involves several sequential steps using an image repository containing dark-field transmission electron microscopy (DF-TEM) images depicting various aging states of an aluminum alloy. During the process, precipitation contours are generated and quantitatively evaluated, and the results are comprehensibly transferred into semantic data structures. The use and deployment of Jupyter Notebooks, along with the beneficial implementation of Semantic Web technologies, significantly enhances the reproducibility and comparability of the findings. This work serves as an exemplar of FAIR image and research data management.
Knowledge representation in the Materials Science and Engineering (MSE) domain is a vast and multi-faceted challenge: Overlap, ambiguity, and inconsistency in terminology are common. Invariant (consistent) and variant (context-specific) knowledge are difficult to align cross-domain. Generic top-level semantic terminology often is too abstract, while MSE domain terminology often is too specific. In this paper, an approach how to maintain a comprehensive MSE-centric terminology composing a mid-level ontology–the Platform MaterialDigital Core Ontology (PMDco)–via MSE community-based curation procedures is presented. The illustrated findings show how the PMDco bridges semantic gaps between high-level, MSE-specific, and other science domain semantics. Additionally, it demonstrates how the PMDco lowers development and integration thresholds. Moreover, the research highlights how to fuel it with real-world data sources ranging from manually conducted experiments and simulations with continuously automated industrial applications.
This study investigates the sintering and crystallization behavior and kinetic of the bioactive glass (BG) 13–93 with nominal composition (in mol%): 54.6 SiO2 - 1.7 P2O3 - 22.1 CaO - 6.0 Na2O - 7.9 K2O - 7.7 MgO. Sintering and crystallization were investigated non-isothermally for various particle size fractions smaller than 315 μm as well as for bulk samples. Densification was not hindered by the presence of crystalline phases across all particle size fractions. Afterwards, wollastonite was found as the dominant crystal phase at higher temperature which resorb primary surface precipitation-like quartz crystallites. The growth direction shifts into volume when the sample surface is nearly covered. The crystal growth rate of wollastonite was calculated from the crystalline surface layer thickness measured during heating. The findings of this study are relevant for the high temperature processing of BG 13–93.
The unusual behavior observed in the coefficient of thermal expansion and specific heat capacity of CrFeNi, CoCrNi, and CoCrFeNi medium/high-entropy alloys is commonly referred to as the K-state effect. It is shown to be independent of the Curie temperature, as demonstrated by temperature-dependent magnetic moment measurements. CoCrFeNi alloy is chosen for detailed characterization; potential reasons for the K-state effect such as texture, recrystallization, and second-phase precipitation are ruled out. An examination of the electronic structure indicates the formation of a pseudo-gap in the Density of States, which suggests a specific chemical interaction between Ni and Cr atoms upon alloying. Hybrid Monte Carlo/Molecular Dynamic (MC/MD) simulations indicate the presence of non-negligible chemical short-range order (CSRO). Local lattice distortions are shown to be negligible, although deviations around Cr and Ni elements from those expected in a fully disordered structure are experimentally observed by X-ray absorption spectroscopy. The determined bonding distances are in good agreement with MC/MD calculations. A mechanism is proposed to explain the anomalies and calorimetric experiments and their results are used to validate the mechanism.
Irradiation assisted stress corrosion cracking (IASCC) is a form of intergranular stress corrosion cracking that occurs in irradiated austenitic alloys. It requires an irradiated microstructure along with high temperature water and stress. The process is ubiquitous in that it occurs in a wide range of austenitic alloys and water chemistries, but only when the alloy is irradiated. Despite evidence of this degradation mode that dates back to the 1960s, the mechanism by which it occurs has remained elusive. Here, using high resolution electron backscattering detection to analyze local stress-strain states, high resolution transmission electron microscopy to identify grain boundary phases at crack tips, and decoupling the roles of stress and grain boundary oxidation, we are able to unfold the complexities of the phenomenon to reveal the mechanism by which IASCC occurs. The significance of the findings impacts the mechanical integrity of core components of both current and advanced nuclear reactor designs worldwide.
AbstractThe high-temperature corrosion behaviors of the equimolar CrCoNi medium-entropy alloy and CrMnFeCoNi high-entropy alloy were studied in a gas atmosphere consisting of a volumetric mixture of 10% H2O, 2% O2, 0.5% SO2, and 87.5% Ar at 800 °C for up to 96 h. Both alloys were initially single-phase fcc with a mean grain size of ~ 50 μm and a homogeneous chemical composition. The oxide layer thickness of CrMnFeCoNi increased linearly with exposure time while it remained constant at ~ 1 μm for CrCoNi. A Cr2O3 layer and minor amounts of (Co,Ni)Cr2O4 developed on the latter while three oxide layers were detected on the former, i.e., a thin and continuous chromium rich oxide layer at the oxide/alloy interface, a dense (Mn,Cr)3O4 layer in the center and a thick and porous layer of Mn3O4 and MnSO4 at the gas/oxide interface. Additionally, a few metal sulfides were observed in the CrMnFeCoNi matrix. These results were found to be in reasonable agreement with thermodynamic calculations.
Extended X-ray absorption fine structure (EXAFS) conducted on an equiatomic MoNbTaW bcc medium-entropy alloy that was annealed at 2273 K reveals unexpectedly small 1st and 2nd shell element-specific lattice distortions. An experimental size-mismatch parameter, δexp, is determined to be ca. 50% lower than the corresponding calculated value. Around W, short-range order (SRO) preferring 4d elements in the 1st and 2nd shells persists. A Nb-W ordering is found, which is reminiscent of ordering emerging at lower temperatures in the B2(Mo,W;Ta,Nb)- and B32(Nb,W)-phases. With high-temperature ordering preferences in fcc also foreshadowing low-temperature phase, these findings suggest a general feature of high-temperature SRO.
A giant Zn segregation transition is revealed using CALPHAD-integrated density-based modeling of segregation into Fe grain boundaries (GBs). The results show that above a threshold of only a few atomic percent Zn in the alloy, a substantial amount of up to 60 at.% Zn can segregate to the GB. We found that the amount of segregation abruptly increases with decreasing temperature, while the Zn content in the alloy required for triggering the segregation transition decreases. Direct evidence of the Zn segregation transition is obtained using high-resolution scanning transmission electron microscopy. Base on the model, we trace the origin of the segregation transition back to the low cohesive energy of Zn and a miscibility gap in Fe-Zn GB, arising from the magnetic ordering effect, which is confirmed by ab-initio calculations. We also show that the massive Zn segregation resulting from the segregation transition greatly assists with liquid wetting and reduces the work of separation along the GB. The current predictions suggest that control over Zn segregation, by both alloy design and optimizing the galvanization and welding processes, may offer preventive strategies against liquid metal embrittlement.
This study investigates the room‐ and high‐temperature (650 °C) tensile and low‐cycle‐fatigue behavior of Inconel 718 produced by laser powder bed fusion (PBF‐LB/M) with a four‐step heat treatment and compares the results to the conventional wrought material. The microstructure after heat treatment is characterized on different length scales. Compared to the wrought variant, the elastic and yield properties are comparable at both test temperatures while tensile strength, ductility, and strain hardening capacity are lower. The fatigue life of the PBF‐LB/M variant at room temperature is slightly lower than that of the wrought material, while at 650 °C, it is vice versa. The cyclic stress response for both material variants is characterized by cyclic softening, which is more pronounced at the higher test temperature. High strain amplitudes (≥0.7%) at room temperature and especially a high testing temperature result in the formation of multiple secondary cracks at the transitions of regions comprising predominantly elongated grain morphology and columns of stacked grains with ripple patterns in the PBF‐LB/M material. This observation and pronounced crack branching and deflection indicate that the cracks are controlled by sharp micromechanical gradients and local crystallite clusters.
AbstractThis study applies Semantic Web technologies to advance Materials Science and Engineering (MSE) through the integration of diverse datasets. Focusing on a 2000 series age-hardenable aluminum alloy, we correlate mechanical and microstructural properties derived from tensile tests and dark-field transmission electron microscopy across varied aging times. An expandable knowledge graph, constructed using the Tensile Test and Precipitate Geometry Ontologies aligned with the PMD Core Ontology, facilitates this integration. This approach adheres to FAIR principles and enables sophisticated analysis via SPARQL queries, revealing correlations consistent with the Orowan mechanism. The study highlights the potential of semantic data integration in MSE, offering a new approach for data-centric research and enhanced analytical capabilities.
In this work we instigated the fragmentation of Au microparticles supported on a thin amorphous carbon film by irradiating them with a gradually convergent electron beam inside the Transmission Electron Microscope. This phenomenon has been generically labeled as ‘‘electron beam-induced fragmentation’’ or EBIF and its physical origin remains contested. On the one hand, EBIF has been primarily characterized as a consequence of beam-induced heating. On the other, EBIF has been attributed to beam-induced charging eventually leading to Coulomb explosion. To test the feasibility of the charging framework for EBIF, we instigated the fragmentation of Au particles under two different experimental conditions. First, with the magnetic objective lens of the microscope operating at full capacity, i.e. background magnetic field 𝐵 = 2 T, and with the magnetic objective lens switched off (Lorenz mode), i.e. 𝐵 = 0 T. We observe that the presence or absence of the magnetic field noticeably affects the critical current density at which EBIF occurs. This strongly suggests that magnetic field effects play a crucial role in instigating EBIF on the microparticles. The dependence of the value of the critical current density on the absence or presence of an ambient magnetic field cannot be accounted for by the beam-induced heating model. Consequently, this work presents robust experimental evidence suggesting that Coulomb explosion driven by electrostatic charging is the root cause of EBIF.
In this work we instigated the fragmentation of Au microparticles supported on a thin amorphous carbon film by irradiating them with a gradually convergent electron beam inside the Transmission Electron Microscope. This phenomenon has been generically labeled as “electron beam-induced fragmentation” or EBIF and its physical origin remains contested. On the one hand, EBIF has been primarily characterized as a consequence of beam-induced heating. On the other, EBIF has been attributed to beam-induced charging eventually leading to Coulomb explosion. To test the feasibility of the charging framework for EBIF, we instigated the fragmentation of Au particles under two different experimental conditions. First, with the magnetic objective lens of the microscope operating at full capacity, i.e. background magnetic field B = 2 T, and with the magnetic objective lens switched off (Lorenz mode), i.e. B = 0 T. We observe that the presence or absence of the magnetic field noticeably affects the critical current density at which EBIF occurs. This strongly suggests that magnetic field effects play a crucial role in instigating EBIF on the microparticles. The dependence of the value of the critical current density on the absence or presence of an ambient magnetic field cannot be accounted for by the beam-induced heating model. Consequently, this work presents robust experimental evidence suggesting that Coulomb explosion driven by electrostatic charging is the root cause of EBIF.
A density-based phase field model is developed where the free energy functional is explicitly linked with molecular dynamics and is referred to as the Molecular Phase Field Method (MoPF). MoPF simulations involve expressing interatomic potentials in terms of density to form a density based free energy functional. Inputs to this functional are taken from atomistics such that the phase field density profile matches the corresponding density profile from atomistic simulations. We analyze our results by comparing the MoPF calculated excess interfacial energies with excess interfacial energies calculated using molecular dynamics associated with several nickel grain boundaries. Additionally, a comparison is made between our results and the interfacial energies of a \Sigma7 boundary across a variety of FCC systems simulated using density functional theory. The MoPF method is able to successfully predict grain boundary free energy trends between grain boundary and material types offering an atomistically informed mesoscale formulation for studying grain boundary physics.
The digitalization of materials science and engineering (MSE) is currently leading to remarkable advancements in materials research, design, and optimization, fueled by computer‐driven simulations, artificial intelligence, and machine learning. While these developments promise to accelerate materials innovation, challenges in quality assurance, data interoperability, and data management have to be addressed. In response, the adoption of semantic web technologies has emerged as a powerful solution in MSE. Ontologies provide structured and machine‐actionable knowledge representations that enable data integration, harmonization, and improved research collaboration. This study focuses on the tensile test ontology (TTO), which semantically represents the mechanical tensile test method and is developed within the project Plattform MaterialDigital (PMD) in connection with the PMD Core Ontology. Based on ISO 6892‐1, the test standard‐compliant TTO offers a structured vocabulary for tensile test data, ensuring data interoperability, transparency, and reproducibility. By categorizing measurement data and metadata, it facilitates comprehensive data analysis, interpretation, and systematic search in databases. The path from developing an ontology in accordance with an associated test standard, converting selected tensile test data into the interoperable resource description framework format, up to connecting the ontology and data is presented. Such a semantic connection using a data mapping procedure leads to an enhanced ability of querying. The TTO provides a valuable resource for materials researchers and engineers, promoting data and metadata standardization and sharing. Its usage ensures the generation of finable, accessible, interoperable, and reusable data while maintaining both human and machine actionability.
Objectives
The aim of the study was to investigate the impact of organic additives (binder, plasticizer, and the cross-linking ink) in the formulation of water-based feedstocks on the properties of a dental feldspathic glass-ceramic material developed for the slurry-based additive manufacturing technology “LSD-print.”
Material and methods
Three water-based feldspathic feedstocks were produced to study the effects of polyvinyl alcohol (AC1) and poly (sodium 4-styrenesulfonate) (AC2) as binder systems. A feedstock without organic additives was tested as the control group (CG). Disc-shaped (n = 15) and bar (n = 7) specimens were slip-cast and characterized in the green and fired states. In the green state, density and flexural strength were measured. In the fired state, density, shrinkage, flexural strength (FS), Weibull modulus, fracture toughness (KIC), Martens parameters, and microstructure were analyzed. Disc-shaped and bar specimens were also cut from commercially available CAD/CAM blocks and used as a target reference (TR) for the fired state.
Results
In the green state, CG showed the highest bulk density but the lowest FS, while the highest FS in the green state was achieved with the addition of a cross-linking ink. After firing, no significant differences in density and a similar microstructure were observed for all slip-cast groups, indicating that almost complete densification could be achieved. The CAD/CAM specimens showed the highest mean FS, Weibull modulus, and KIC, with significant differences between some of the slip-cast groups.
Significance
These results suggest that the investigated feedstocks are promising candidates for the slurry-based additive manufacturing of restorations meeting the class 1a requirements according to DIN EN ISO 6871:2019–01.
Functional fatigue of shape-memory alloys is a considerable threat to the reliable service of actuation devices. Here, we demonstrate the essentially degradation-free cyclic phase-transformation behavior of Ni-Mn-Ga microcrystals up to one million stress-driven superelastic cycles. Cyclic dissipation amounts to about 1/5 of the bulk counterpart and remains unaffected during cycling, even after the introduction of dislocation structures via plastic straining. Plastic yielding and the transformation stress largely exceed the known bulk values. However, the transformation-stress is found to depend on plastic pre-straining, which suggests that the size-affected transformation stress is sensitive to the initial defect structure and that it can be tuned by a targeted introduction of dislocations. These findings demonstrate the high suitability of Ni-Mn-Ga as a robust shape-memory alloy in small-scale functional device engineering.
Mean-field modeling and phase-field simulation of grain growth under directional driving forces
(2024)
Directional grain growth is a common phenomenon in the synthetic and natural evolution of various polycrystals. It occurs in the presence of an external driving force, such as a temperature gradient, along which grains show a preferred, yet competitive, growth. Novel additive manufacturing processes, with intense, localized energy deposition, are prominent examples of when directional grain growth can occur, beneath the melting pool. In this work, we derive a phenomenological mean-field model and perform 3D phase-field simulations to investigate the directional grain growth and its underlying physical mechanisms. The effect of the intensity of driving force is simulated and systematically analyzed at the evolving growth front as well as various cross-sections perpendicular to the direction of the driving force. We found that although the directional growth significantly deviates from normal grain growth, it is still governed by a power law relation <R> α tⁿ with an exponent n ~ 0.6–0.7. The exponent n exhibits a nontrivial dependence on the magnitude of the directional driving force, such that the lowest growth exponent is observed for intermediate driving forces. We elaborate that this can originate from the fact that the forces at grain boundary junctions evolve out of balance under the influence of the directional driving force. With increasing the driving forces, the growth exponent asymptotically approaches a value of n ≈ 0.63, imposed by the largest possible grain aspect ratio for given grain boundary energies. The current combined mean-field and phase-field framework pave the way for future exploration in broader contexts such as the evolution of complex additively manufactured microstructures.
The current lack of quantitative knowledge on processing-microstructure–property relationships is one of the major bottlenecks in today’s rapidly expanding field of additive manufacturing. This is centrally rooted in the nature of the processing, leading to complex microstructural features. Experimentally-guided modeling can offer reliable solutions for the safe application of additively manufactured materials. In this work, we combine a set of systematic experiments and modeling to address creep anisotropy and its correlation with microstructural characteristics in laser-based powder bed fusion (PBF-LB/M) additively manufactured Inconel-738LC (IN738LC). Three sample orientations (with the tensile axis parallel, perpendicular, and 45° tilted, relative to the building direction) are crept at 850 °C, accompanied by electron backscatter secondary diffraction (EBSD), scanning electron microscopy (SEM) and transmission electron microscopy (TEM) investigations. A crystal plasticity (CP) model for Ni-base superalloys, capable of modeling different types of slip systems, is developed and combined with various polycrystalline representative volume elements (RVEs) built on the experimental measurements. Besides our experiments, we verify our modeling framework on electron beam powder bed fusion (PBF-EB/M) additively manufactured Inconel-738LC. The results of our simulations show that while the crystallographic texture alone cannot explain the observed creep anisotropy, the superlattice extrinsic stacking faults (SESF) and related microtwinning slip systems play major roles as active deformation mechanisms. We confirm this using TEM investigations, revealing evidence of SESFs in crept specimens. We also show that the elongated grain morphology can result in higher creep rates, especially in the specimens with a tilted tensile axis.