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  • Munnik, F. (7)
  • Reinholz, Uwe (6)
  • Radtke, Martin (5)
  • Bjeoumikhov, A. (3)
  • Buchriegler, J. (3)
  • Petric, M. (3)
  • Scharf, O. (3)
  • Wedell, R. (3)
  • Nowak, S.H. (2)
  • Renno, A.D. (2)
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  • Lodine (1)
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Organisationseinheit der BAM

  • 6 Materialchemie (2)
  • 6.3 Strukturanalytik (2)
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Road to micron resolution with a color X-ray camera – polycapillary optics characterization (2017)
Nowak, S. H. ; Petric, M. ; Buchriegler, J. ; Bjeoumikhov, A. ; Bjeoumikhova, Z. ; von Borany, J. ; Munnik, F. ; Radtke, Martin ; Renno, A. D. ; Reinholz, Uwe ; Scharf, O. ; Tilgner, J. ; Wedell, R.
In a color X-ray camera spatial resolution is achieved by means of a polycapillary optic conducting X-ray photons from small regions on a sample to distinct energy dispersive pixels on a CCD matrix. At present, the resolution limit of color X-ray camera systems can go down to several microns and is mainly restricted by Pixel dimensions. The recent development of an efficient subpixel resolution algorithm allows a release from pixel size, limiting the resolution only to the quality of theoptics. In this work polycapillary properties that influence the spatial resolution are systematized and assessed both theoretically and experimentally. It is demonstrated that with the current technological Level reaching one micron resolution is challenging, but possible.
Iodine in alluvial platinum-palladium nuggets: evidence for biogenic precious-metal fixation (2011)
Cabral, A.R. ; Radtke, Martin ; Munnik, F. ; Lehmann, B. ; Reinholz, Uwe ; Riesemeier, Heinrich ; Tupinambá, M. ; Kwitko-Ribeiro, R.
Synchrotron radiation-induced X-ray fluorescence (SR-XRF) spectrometry was applied to determine iodine concentrations in alluvial Pt–Pd aggregates with delicate morphological features from Córrego Bom Sucesso, Minas Gerais, Brazil. The millimetre-sized botryoidal and rod-shaped grains of alluvial Pt–Pd–Hg intermetallic compounds have surprisingly high concentrations of iodine, in the range from 10 to ~ 120 μg/g. Because iodine is a strongly biophile element, known to be enriched in peatlands and plant remains in soils by microbial activity, its concentration in the Pt–Pd nuggets suggests biogenic precious-metal fixation in the aqueous alluvial milieu. Biogenic and inorganic processes, such as bioreduction and electrochemical metal accretion, could mutually have contributed to the growth of nanoparticles, formed on organic templates, to millimetric Pt–Pd nuggets.
Accurate stopping power determination of 15N ions for hydrogen depth profiling by a combination of ion beams and synchrotron radiation (2012)
Zier, M. ; Reinholz, Uwe ; Riesemeier, Heinrich ; Radtke, Martin ; Munnik, F.
Hydrogen analysis is of particular importance in thin film technology and it is often necessary to obtain a depth profile. The method with the best depth resolution is NRA using the 6385 keV resonance of the 1H(15N,αγ)12C nuclear reaction. The correct quantification of the depth and concentration scales in the measured hydrogen profiles relies on accurate stopping power values. We present a method to deduce these values from a combination of two techniques: NRA and X-ray reflectometry (XRR). This method is applied to the determination of the stopping power of ~6.4 MeV 15N ions in H-containing amorphous Si-layers (a-Si:H). Density-independent stopping powers at different H concentrations are determined by combining the results from NRA and XRR with an overall uncertainty of 3.3%, showing good agreement with SRIM values. This work shows exemplary the methodology for future evaluation of stopping powers for quality assurance in NRA.
Iodine detection in a heavy matrix, a comparison of PIXE and XRF (2010)
Munnik, F.
Spatially-resolved analysis of natural minerals as carriers of high-tech metals and Rare Earth Elements: comparison of EPMA, PIXE and Sy-µXRF (2012)
Reinholz, Uwe ; Munnik, F.
Sub-pixel resolution with a color X-ray camera (2015)
Nowak, S.H. ; Bjeoumikhov, A. ; Von Borany, J. ; Buchriegler, J. ; Munnik, F. ; Petric, M. ; Radtke, Martin ; Renno, A.D. ; Reinholz, Uwe ; Scharf, O. ; Wedell, R.
The color X-ray camera SLcam® is a full-field, single photon detector providing scanning-free, energy and spatially resolved X-ray imaging. Spatial resolution is achieved with the use of polycapillary optics guiding X-ray photons from small regions on a sample to distinct energy dispersive pixels on a charged-coupled device detector. Applying sub-pixel resolution, signals from individual capillary channels can be distinguished. Therefore, the SLcam® spatial resolution, which is normally limited to the pixel size of the charge-coupled device, can be improved to the size of individual polycapillary channels. In this work a new approach to a sub-pixel resolution algorithm comprising photon events also from the pixel centers is proposed. The details of the employed numerical method and several sub-pixel resolution examples are presented and discussed.
Examples of XRF and PIXE imaging with few microns resolution using SLcam® a color X-ray camera (2015)
Nowak, S.H. ; Bjeoumikhov, A. ; Von Borany, J. ; Buchriegler, J. ; Munnik, F. ; Petric, M. ; Renno, A.D. ; Radtke, Martin ; Reinholz, Uwe ; Scharf, O. ; Strüder, L. ; Wedell, R. ; Ziegenrücker, R.
We present results of recent development of the color X-ray camera, type SLcam®, allowing detection of X-ray images with few microns resolution. Such spectral resolution is achieved with the use of high-quality polycapillary optics combined with sub-pixel resolution. Imaging of Siemens star resolution test chart reveals that the resolution limit of SLcam® can go down to nearly 5µm. Several real sample examples of measurements carried out at the laboratory, synchrotron, and particle-induced X-ray emission beamlines are shown. This is the first time SLcam® is used as particle-induced X-ray emission detector.
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