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Eingeladener Vortrag
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The challenge of how to adequately characterize the toughness behavior of ductile cast iron (DCI) materials had been solved through the development and application of fracture mechanics concepts. Outstanding examples are found in the design and safety assessment procedures of sophisticated DCI components for wind turbines or transport and storage casks for radioactive materials. An essential requirement for these procedures is to have adequate fracture mechanics toughness data available.
Because DCI materials may substantially change their deformation, damage and fracture behavior from ductile to brittle by increasing loading rate, decreasing temperature, increasing pearlite share and increasing stress triaxiality, the corresponding experimental measuring techniques and analysis concepts have to be chosen and adapted with deliberation. Long-time experience in this field is imperative to provide valuable data.
BAM has been dealing with mechanical and fracture mechanical characterization of DCI materials for more than 30 years. This paper demonstrates state-of-the-art fracture mechanics test methods for the determination of quasi-static and dynamic fracture toughness. Among others, it is exemplarily shown for a variety of DCI materials conforming to grade EN-GJS-400 how mechanical and fracture mechanical properties are influenced by temperature, loading rate and microstructure. A major lesson to be learned is that fracture toughness data of DCI should always be discussed, reported and used in correlation with microstructural parameters.
The roll-on-roll-off passenger ferry MV ESTONIA sank during the night of 28 September 1994 in the Baltic Sea. In October 2000, divers recovered two palm-sized test pieces from the front bulkhead of the wreck. The investigators analysed these specimens to determine whether there were any indications of deliberate blasting. Since the wreck had been submerged for almost six years, it was clear that chemical traces would not be present on the surfaces of the test pieces. Therefore, the investigators performed comparative tests on shipbuilding steel to find a microstructural criterion that exclusively characterises a blast. The shipyard Jos. L. Meyer, Germany, had built the ESTONIA and supplied shipbuilding steel plates similar to that used for building the vessel in 1979/1980. The comparative tests comprised mechanical tests, shot peening tests and blasting tests using different explosives. Testing demonstrated that blasting always formed twinned ferrite grains in the microstructure over the whole cross-section of each of the 8 mm thick comparative plates. Although one of the original test pieces of the ESTONIA showed deformation twins, this was only confined up to 0.4 mm underneath the surfaces and not spread over the whole cross-section. Comparative shot peening tests produced the very same pattern of subsurface deformation twins. Therefore, the twins detected in the microsection of the test pieces of the ESTONIA wreck traced back to the shot peening process performed by the shipyard in 1979/1980 and not to a deliberate blast.
Design and safety assessment of advanced ductile cast iron (DCI) components like wind turbines or transport and storage casks for radioactive materials require appropriate material data in terms of strength and fracture toughness. Therefore, it is of vital importance to characterize and understand the deformation, damage and fracture behaviour of DCI which may substantially change from ductile to brittle by increasing loading rate, decreasing temperature and/or increasing stress triaxiality. This paper reports on recent BAM inverstigations on different qualities of the widely used DCI grade EN-GJS-400 with varying pearlite shares (none and 18% respectively). The focus was on the influences of microstructure, temperature (ambient and -40 °C) and loading rate (quasi-static to crash) on strength (YS, UTS, flow curve) and fracture mechanical properties (R-curve, crack initiation toughness, fracture toughness). Systematic metallographical and fractographical analyses were performed accompanying the whole test program and a systematics of specific damage behaviour and fracture mechanisms was derived from the results.