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In civil engineering concrete is the most used building material for making infrastructures like bridges and parking decks worldwide. It is as a porous and multiphase material made of aggregates with a defined grain size distribution, cement and water as well as different additives and admixtures depending on the application. Different grain sizes are important to ensure the needed density and compressive strength.
The resulting porous cement matrix contains a mixture of flour grains (aggregates with a grain size below 125 lm) and cement particles (particle size≈50lm). Harmful species like chlorides may penetrate together with water through the capillary pore space and may trigger different damage processes. The damage assessment of concrete structures in Germany is estimated due to the quantification of harmful elements regarding to the cement content only. In the evaluation of concrete using LIBS a two-dimensional scanning is necessary to consider the heterogeneity caused by the aggregates. Therefore, a LIBS system operating with a low energy NdCr:YAG laser, a pulse energy of 3 mJ, a wavelength of 1064 nm, a pulse width of 1.5 ns and a Repetition rate of 100 Hz has been used. Different Czerny-Turner spectrometers with CCD detectors in the UV and NIR range have been used for the detection. Large aggregates (macro-heterogeneity) can be excluded from the evaluation, whereas small aggregates in the range of the laser spot size (flour grains) cannot be spatially resolved. In this work the micro heterogeneity caused by flour grains and their impact on the quantification with LIBS will be discussed. To analyze the effect of changing grain sizes and ratios, the ablation behavior has been determined and compared. Samples with defined grain sizes were made and analyzed using LIBS.
The grain size distributions were analyzed with laser diffraction (LDA).
Processing ultrasonic data by coda wave interferometry to monitor load tests of concrete beams
(2018)
Ultrasonic transmission measurements have been used for decades to monitor concrete elements, mostly on a laboratory scale. Recently, coda wave interferometry (CWI), a technique adapted from seismology, was introduced to civil engineering experiments. It can be used to reveal subtle changes in concrete laboratory samples and even large structural elements without having a transducer directly at the place where the change is taking place. Here, several load tests until failure on large posttensioned concrete beams have been monitored using networks of embedded transducers. To detect subtle effects at the beginning of the experiments and cope with severe changes due to cracking close to failure, the coda wave interferometry procedures had to be modified to an adapted step-wise approach. Using this methodology, we were able to monitor stress distribution and localize large cracks by a relatively simple technique. Implementation of this approach on selected real structures might help to make decisions in infrastructure asset management.
"INFRASTAR aims to develop knowledge, expertise and skills for optimal and reliable management of structures. The generic methodology is applied to bridges and wind turbines in relation to fatigue offering the opportunity to deal with complementary notions (such as old and new asset management, unique and similar structures, wind and traffic actions) while addressing 3 major challenges: 1/ advanced modelling of concrete fatigue behaviour, 2/new non destructive testing methods for early aged damage detection and 3/probabilistic approach of structure reliability under fatigue. Benefit of cross-experience and inter-disciplinary synergies creates new knowledge. INFRASTAR proposes innovative solutions for civil infrastructure asset management so that young scientists acquire a high employment profile in close dialogue between industry and academic partners. Modern engineering methods, including probabilistic approaches, risk and reliability assessment tools, will take into account the effective structural behaviour of existing bridges and wind turbines by exploiting monitored data. Existing methods and current state-of -the art is based on excessive conservatism which produces high costs and hinders sustainability. INFRASTAR improves knowledge for optimising the design of new structures, for more realistic verification of structural safety and more accurate prediction of future lifetime of the existing structures. That is a challenge for a sustainable development because it reduces building material and energy consumption as well as CO2 production. Within the global framework of optimal infrastructure asset management, INFRASTAR will result in a multi-disciplinary body of knowledge covering generic problems from the design stage process of the new civil infrastructures up to recycling after dismantlement. This approach and the proposed methods and tools are new and allow a step forward for innovative and effective process."
Seismic interferometry (SI) deals either with the sensible detection of changes in the subsurface or with the reconstruction of virtual signals between two receivers by crosscorrelation of signals from diffuse sources. These concepts can be applied in NDT in civil engineering for various purposes, e. g. to detect changes in bridges. Here it is demonstrated using data from a reference structure on our test site. Practical applications can be expected in the very near future.
Ultrasonic transmission measurements are used to monitor concrete elements mostly on a laboratory scale since decades.
Recently, coda wave interferometry, a technique adapted from seismology, has been introduced to civil Engineering experiments. It can be used to reveal subtle changes in concrete samples and even large construction elements without having a transducer directly at the location where the change is taking place. The methodology works best with embedded transducers to avoid coupling issues or excessive environmental influence. These transducers can be used for newly built and existing structures. Recently, large concrete beams have been equipped with a network of transducers and loaded until failure. Using code wave interferometry, it was possible to visualize stress fields and damaged areas.
This paper describes a novel methodology for quantitative in-situ moisture measurement without tracking agents using X-ray computed tomography (XCT). The high levels of grey-scale precision required for the measurement of moisture without tracking agents resulted in the need for an additional image calibration procedure to correct for water-related X-ray scattering and for equipment-variability related artefacts arising during in-situ testing. This calibration procedure was developed on the basis of existing principles of XCT image cor-rection. Resulting images of moisture distribution exhibit a high level of agreement with expected material behaviour. This research demonstrated that XCT can be successfully used to measure both moisture-front movement over time and changes in 3D moisture distribution within samples. This approach to moisture measurement lays the groundwork for the planned future investigation of the interaction between cracking induced by varying chemical and mechanical processes and water transport in concrete.
The goal of the Special Issue “Brittle Materials in Mechanical Extremes” was to spark a discussion of the analogies and the differences between different brittle materials, such as, for instance, ceramics and concrete. Indeed, the contributions to the Issue spanned from construction materials (asphalt and concrete) to structural ceramics, reaching as far as ice. The data shown in the issue were obtained by advanced microstructural techniques (microscopy, 3D imaging, etc.) and linked to mechanical properties (and their changes as a function of aging, composition, etc.). The description of the mechanical behavior of brittle materials under operational loads, for instance, concrete and ceramics under very high temperatures, offered an unconventional viewpoint on the behavior of brittle materials. This is not at all exhaustive, but a way to pave the road for intriguing and enriching comparisons.
New possibilities for concrete analysis 4.0 with the Laser-Induced Breakdown Spectroscopy (LIBS)
(2020)
In civil engineering the damage assessment of concrete infrastructures is an important task to monitor and ensure the estimated life-time. The aging of concrete is caused by different damage processes like the chloride induced pitting corrosion of the reinforcement. The penetration depth and the concentration of harmful species are crucial factors in the damage assessment. As a highly cost and time-consuming standard procedure, the analysis of concrete drill cores or drilling by wet-chemistry is widely used. This method provides element concentration to the total mass as aggregates and binder are homogenized. In order to provide a method that is capable to detect the element concentration regarding the cement content only, the laser-induced breakdown spectroscopy (LIBS) will be presented. The LIBS method uses a focused pulsed laser on the sample surface to ablate material. The high-power density and the laser-material interaction causes a laser-induced plasma that emits elemental and molecular line emission due to energy transition of the excited species in the plasma during the cooling phase.
As each element provides element-specific line emission, it is in principle possible to detect any element on the periodic table (spectroscopic fingerprint) with one laser shot. In combination with a translation stage the sample under investigation can be spatially resolved using a scan raster with a resolution up to 100 µm (element mapping). Due to the high spatial resolution, the element distribution and the heterogeneity of the concrete can be evaluated. By using chemometrics the non-relevant aggregates can be excluded from the data set and the element concentration can be quantified and referred to a specific solid phase like the binding matrix (cement) only. In order to analyze transport processes like diffusion and migration the twodimensional element distributions can provide deep insight into the transport through the pore space and local enrichments of elements. As LIBS is a multi-elemental method it is also possible to compare the ingress and transport process of different elements like Cl, Na, K, S, C, and Li simultaneously and evaluate cross-correlations between the different ions. Furthermore, the element mapping allows to visualize the transport along cracks. This work will show the state of the art in terms of hardware and software for an automated LIBS system as well as different application for a concrete analysis 4.0. Focus will be the application of LIBS for a fast concrete analysis.
Due to the high sensitivity of coda waves to the smallest structural alterations such as strain, humidity or temperature changes, ultrasonic waves are a valid means to examine entire structures employing networks of ultrasonic transducers. In order to substantiate this ex ante assessment, the viability of measuring ultrasonic waves as a valid point of reference and inference for structural changes is to be further scrutinized in this work. In order to investigate the influence of mechanical strain on ultrasonic signals, a four-point bending test was carried out on a reinforced concrete beam at Ruhr University Bochum. Thus, measurements collected from a network of selected transducer pairings arranged across the central, shear-free segment of the test specimen, were correlated to their respective strain fields. Detected ultrasonic signals were evaluated employing Coda Wave Interferometry. Such analysis comprised the initial non-cracked state as well as later stages with incremental crack depth and quantity. It was to ascertain that the test specimen can in fact be qualitatively compartmentalized into areas of compression and tension identified via Relative Velocity Changes presented in Attribute Maps. However, since results did not entail a zero crossing, i.e., neither positive nor negative values were to be calculated, only relative changes in this work displayed staggered over the height of the object under test, are discussed. Under the given methodological premises, additional information is currently required to make quantitative assertions regarding this correlation of ultrasonic and strain results. This holds true for the comparability of the ultrasonic and strain results for both non-cracked and even the cracked state.
Air-coupled ultrasonic testing is widely used in the industry for the non-destructive testing of compound materials. It provides a fast and efficient way to inspect large concrete civil infrastructures for damage that might lead to catastrophic failure. Due to the large penetration depths required for concrete structures, the use of traditional piezoelectric transducer requires high power electric systems. In this study, a novel fluidic transducer based on a bistable fluidic amplifier is investigated. Previous experiments have shown that the switching action of the device produces a high-power broadband ultrasonic signal. This study will provide further insight into the switching behaviour of the fluidic switch. Therefore, parametric CFD simulations based on compressible supersonic RANS simulations were performed, varying the inlet pressure and velocity profiles for the control flow. Switching times are analyzed with different methods, and it was found that These are mostly independent of the slope of the velocity profile at the control port. Furthermore, it was found that an inversely proportional relationship exists between flow velocity in the throat and the switching time. The results agree with the theoretical background established by experimental studies that can be found in the literature.
Muon Tomography of the Interior of a Reinforced Concrete Block: First Experimental Proof of Concept
(2021)
Quality assurance and condition assessment of concrete structures is an important topic world-wide due to the aging infrastructure and increasing traffic demands. Common topics include, but are not limited to, localisation of rebar or tendon ducts, geometrical irregularities, cracks, voids, honeycombing or other flaws. Non-destructive techniques such as ultrasound or radar have found regular, successful practical application but sometimes suffer from limited resolution and accuracy, imaging artefacts or restrictions in detecting certain features. Until the 1980s X-ray transmission was used in case of special demands and showed a much better resolution than other NDT techniques. However, due to safety concerns and cost issues, this method is almost never used anymore. Muon tomography has received much attention recently. Novel detectors for cosmic muons and tomographic imaging algorithms have opened up new fields of application, such as the investigation of freight containers. Muon imaging also has the potential to fill some of the gaps currently existing in concrete NDT. As a first step towards practical use and as a proof of concept we used an existing system to image the interior of a reference reinforced 600 kg concrete block. Even with a yet not optimized setup for this kind of investigation, the muon imaging results are at least of similar quality compared to ultrasonic and radar imaging, potentially even better. The data acquisition takes more time and signals contain more noise, but the images allowed to detect the same important features that are visible in conventional high energy X-ray tomography. In our experiment, we have shown that muon imaging has potential for concrete inspection. The next steps include the development of mobile detectors and optimising acquisition and imaging parameters.
This paper summarizes the results of research aimed at assessing cracks in reinforced concrete structures using embedded ultrasonic sensors. The diffuse ultrasonic waves were considered to evaluate the health status of the tested structures. There are different algorithms used to detect cracks in the structure, but most studies have been performed on benchmark reinforced concrete (RC) structures and in laboratory conditions. Since there were difficulties with the validity of Damage detection in real structures in the presence of environmental changes and noises, the application of advanced signal processing methods was necessary. Therefore, the wavelet transform was applied to process ultrasonic signals acquired from multiple civil structures. It is shown that the ultrasonic sensors with an applied wavelet transform algorithm on collected signals can successfully detect cracks in the laboratory as well as in a real environment. Experimental results showed a perfect match for detecting damage and quasi-static load in the presence of environmental changes. The results were confirmed with other techniques. In addition, designing an extra filter for removing noises can be avoided by using the applied algorithms. The obtained results confirmed that diffuse ultrasonic sensor methodology with the proposed algorithm is useful and effective in Monitoring real RC structures, and it is better than traditional techniques.
Reinforced concrete bridges are iconic parts of modern infrastructure. They are designed for a minimum service life of 100 years. However, environmental factors and/or inappropriate use might cause overload and accelerate the deterioration of bridges. In extreme cases, bridges could collapse when necessary maintenance lacks. Thus, the permanent monitoring for structure health assessment has been proposed, which is the aim of structural health monitoring (SHM). Studies in laboratories have shown that ultrasonic (US) coda wave interferometry (CWI) using diffuse waves has high sensitivity and reliability to detect subtle changes in concrete structures. The creation of micro-cracks might be recognized at an early stage. Moreover, large-volume structures can be monitored with a relatively small number of US transducers. However, it is still a challenge to implement the CWI method in real SHM practical applications in an outdoor environment because of the complex external factors, such as various noise sources that interfere with the recorded signals. In this paper, monitoring data from a 36-m long bridge girder in Gliwice, Poland, instrumented with embedded US transducers, thermistors, and vibrating wire strain gauges, is presented. Noise estimation and reductionmethods are discussed, and the influence of traffic, as well as temperature variation, are studied. As a result, the relative velocity variation of US waves following the temperature change with a very high precision of 10−4% is shown, and a good bridge health condition is inferred. The influence of lightweight real traffic is negligible. The study verified the feasibility of the implementation of the CWI method on real bridge structures.
With a goal to improve our understanding of the relationships between microstructural features and ultrasonic signal behavior, concrete specimens of varying water-to-cement ratio were imaged using X-ray computed tomography (CT), and subsequently subjected to ultrasonic testing. From the CT scans, measurements were made of cement paste density and number of interfaces. Ultrasonic signals produced using a through-transmission configuration were analyzed and fit to a diffusion model to separate absorption from scattering attenuation. The results showed that at the frequencies tested, ultrasonic dissipation rate correlated weakly with paste density, while diffusivity correlated well with number of interfaces, but only if entrained air is considered separately. Cement paste density was found to be very well predicted by diffusivity, leading to a clear power-law relationship between diffusivity and compressive strength.
Hydration is the exothermic reaction between anhydrous cement and water, which forms the solid cement matrix of concrete. Being able to evaluate the hydration is of high interest for the use of both conventional and more climate-friendly building materials. The experimental monitoring is based on temperature or moisture measurements. The first needs adiabatic conditions, which can only be achieved in laboratory. The latter is often measured comparing the weight of the material sample before and after oven drying, which is time-consuming. This study investigates the moisture content of two cement-based and two calcium sulphate based mixtures for the first 90 days by using the calcium carbide method and oven drying at 40 °C and 105 °C (Darr method). Thereby, the amount of chemically bound water is determined to derive the degree of hydration. The calcium carbide measurements highly coincide with oven drying at 40 °C. The calcium carbide method is therefore evaluated as a suitable alternative to the time-consuming Darr drying. The prompt results are seen as a remarkable advantage and can be obtained easily in laboratory as well as in the field.
The knowledge of the thermal parameters of a particular concrete is essential for thermal design of a building, but also could help to identify and assess the state of a concrete structure. Active thermography has the potential to be applied onsite and to provide a fast investigation of thermal properties. In this work, three different concrete samples were investigated by active thermography in reflection and in transmission setup. It was found that this method yields the same results without direct contact as the Transient Plane Source (TPS) method as an established inspection tool.
Validation of novel ultrasonic phased array borehole probe by using simulation and measurement
(2022)
Low-frequency ultrasonic testing is a well-established non-destructive testing (NDT) method in civil engineering for material characterization and the localization of cracks, reinforcing bars and delamination. A novel ultrasonic borehole probe is developed for in situ quality assurance of sealing structures in radioactive waste repositories using existing research boreholes. The aim is to examine the sealing structures made of salt concrete for any possible cracks and delamination and to localize built-in components. A prototype has been developed using 12 individual horizontal dry point contact (DPC) shear wave transducers separated by equidistant transmitter/receiver arrays. The probe is equipped with a commercially available portable ultrasonic flaw detector used in the NDT civil engineering industry. To increase the sound pressure generated, the number of transducers in the novel probe is increased to 32 transducers. In addition, the timed excitation of each transducer directs a focused beam of sound to a specific angle and distance based on the previously calculated delay time. This narrows the sensitivity of test volume and improves the signal-to-noise ratio of the received signals. In this paper, the newly designed phased array borehole probe is validated by beam computation in the CIVA software and experimental investigations on a half-cylindrical test specimen to investigate the directional characteristics. In combination with geophysical reconstruction methods, it is expected that an optimised radiation pattern of the probe will improve the signal quality and thus increase the reliability of the imaging results. This is an important consideration for the construction of safe sealing structures for the safe disposal of radioactive or toxic waste.
During their life span, concrete structures interact with many kinds of external mechanical loads. Most of these loads are considered in advance and result in reversible deformations. Nevertheless, some of the loads cause irreversible, sometimes unnoticed changes below the macroscopic scale depending on the type and dimension of the impact. As the functionality of concrete structures is often relevant to safety and society, their condition must be known and, therefore, assessed on a regular basis. Out of the spectrum of non-destructive monitoring methods, Coda Wave Interferometry using embedded ultrasonic sensors is one particularly sensitive technique to evaluate changes to heterogeneous media. However, there are various influences on Coda waves in concrete, and the interpretation of their superimposed effect is ambiguous. In this study, we quantify the relations of uniaxial compression and uniaxial tension on Coda waves propagating in normal concrete. We found that both the signal correlation of ultrasonic signals as well as their velocity variation directly reflect the stress change in concrete structures in a laboratory environment. For the linear elastic range up to 30% of the strength, we calculated a velocity variation of −0.97‰/MPa for compression and 0.33%/MPa for tension using linear regression. In addition, these parameters revealed even weak irreversible changes after removal of the load. Furthermore, we show the time-dependent effects of shrinkage and creep on Coda waves by providing the development of the signal parameters over time during half a year together with creep recovery. Our observations showed that time-dependent material changes must be taken into account for any comparison of ultrasonic signals that are far apart in time. The study’s results demonstrate how Coda Wave Interferometry is capable of monitoring stress changes and detecting even small-size microstructural changes. By indicating the stated relations and their separation from further impacts, e.g., temperature and moisture, we anticipate our study to contribute to the qualification of Coda Wave Interferometry for its application as an early-warning system for concrete structures.
To complement the information provided by deterministic seismic imaging at length scales above a certain resolution limit we present the first application of adjoint envelope tomography (AET) to experimental data. AET uses the full envelopes of seismic records including scattered coda waves to obtain information about the distribution of absorption and small-scale heterogeneity which provide complementary information about the investigated medium. Being below the resolution limit this small-scale structure cannot be resolved by conventional tomography but still affects wave propagation by attenuating ballistic waves and generating scattered waves. Using ultrasound data from embedded sensors in a meter-sized concrete specimen we image the distribution of absorption and heterogeneity expressed by the intrinsic quality factor Q−1 and the fluctuation strength ɛ that characterizes the strength of the heterogeneity. The forward problem is solved by modeling the 2-D multiple nonisotropic scattering in an acoustic medium with spatially variable heterogeneity and attenuation using the Monte-Carlo method. Gradients for the model updates are obtained by convolution with the back-propagated envelope misfit using the adjoint formalism in analogy to full waveform inversion.
We use a late coda time window to invert for absorption and an earlier time window to infer the distribution of heterogeneity. The results successfully locate an area of salt oncrete with increased scattering and concentric anomalies of intrinsic attenuation. The resolution test shows that the recovered anomalies constitute reasonable representations of internal structure of the specimen.
NMR is becoming increasingly popular for the investigation of building materials as it is a non-invasive technology that does not require any sample preparation nor causes damage to the material. Depending on the specific application it can offer insights into properties like porosity and spatial saturation degree as well as pore structure. Moreover it enables the determination of moisture transport properties and the (re-)distribution of internal moisture into different reservoirs or chemical phases upon damage and curing. However, as yet most investigations were carried out using devices originally either designed for geophysical applications or the analysis of rather homogeneous small scale (< 10 mL) samples. This paper describes the capabilities of an NMR tomograph, which has been specifically optimized for the investigation of larger, heterogeneous building material samples (diameters of up to 72 mm, length of up to 700 mm) with a high flexibility due to interchangeable coils allowing for a high SNR and short echo times (50 - 80 m s).
The corner echo is a well-known effect in ultrasonic testing, which allows detection of surface breaking cracks with predominantly perpendicular orientation to the surface as, for example, corrosion cracks in metal pipes or shafts. This echo is formed by two planes, the surface of the crack and the surface which the crack breaks. It can also be classified as a half-skip method, since a reflection of the pulse occurs on the backwall before the reflection at the defect takes place. In combination with the diffraction from the crack tip, the corner echo also allows crack sizing. As shown in this paper, the corner reflection can be used in civil engineering for nondestructive inspection of concrete. Commercially available low frequency ultrasonic arrays with dry point contact sources generate SH transversal waves with sufficient divergence of the sound field in order to detect corner reflections. Ultrasonic line-scans and area-scans were acquired with a linear array on flat concrete specimens, and the data were reconstructed by the Synthetic aperture focusing technique. If the angles and the area of reconstruction are chosen accordingly, the corner echo reflection can be distinguished from other ultrasonic information. The corner echo can thus be used as a method for deciding whether a crack is a partial-depth crack or a full-depth crack and thus for obtaining a statement about crack depth. This paper presents corresponding experimental results obtained on concrete specimens with artificial test defects and cracks induced under controlled conditions.
The ultrasonic echo technique is frequently used in non-destructive testing (NDT) of concrete structures for thickness measurements, geometry determinations as well as localization of built-in components. To improve ultrasonic imaging of complex structures in concrete, we transferred a geophysical imaging technique, the reverse time migration (RTM), to NDT in civil engineering. In contrast to the conventionally used synthetic aperture focusing technique (SAFT) algorithms, RTM is a wavefield continuation method in time and uses the full wave equation. Thus, RTM can handle complicated wave propagations in any direction without dip limitation. In this paper, we focused on the application and evaluation of a two-dimensional (2D) elastic RTM algorithm considering compressional waves, vertically polarized shear waves, and Rayleigh waves. We tested the elastic RTM routine on synthetic ultrasonic echo data generated with a 2D concrete model consisting of several steps and circular air inclusions. As these complex structures can often be found in real-world NDT use cases, their imaging is especially important. By using elastic RTM, we were able to clearly reproduce vertical reflectors and lower edges of circular air voids inside our numerical concrete model. Such structures cannot be imaged with conventional SAFT algorithms. Furthermore, the used elastic RTM approach also yielded a better reconstruction of a horizontal reflector and upper boundaries of circular air inclusions. Our encouraging results demonstrate that elastic RTM has the potential to significantly improve the imaging of complex concrete structures and, thus, is a step forward for detailed, high-quality ultrasonic NDT in civil engineering.
Large-language models (LLMs) such as GPT-4 caught the interest of many scientists. Recent studies suggested that these models could be useful in chemistry and materials science. To explore these possibilities, we organized a hackathon. This article chronicles the projects built as part of this hackathon. Participants employed LLMs for various applications, including predicting properties of molecules and materials, designing novel interfaces for tools, extracting knowledge from unstructured data, and developing new educational applications. The diverse topics and the fact that working prototypes could be generated in less than two days highlight that LLMs will profoundly impact the future of our fields. The rich collection of ideas and projects also indicates that the applications of LLMs are not limited to materials science and chemistry but offer potential benefits to a wide range of scientific disciplines.
Locating and sizing delaminations is a common inspection task in the maintenance and quality control of construction and rehabilitation. Their detection is an important area of application of nondestructive testing in civil engineering (NDT-CE). To improve this application, NDT test systems and test solutions must be compared, for which specimens containing well-defined delaminations are needed to serve as a reference. Currently, there are no widely accepted procedures available for creating such flaws locally and reproducibly. This study presents procedures for creating artificial delaminations repeatably and as close as possible to natural delaminations. To produce the discontinuities only substances were used which can occur in concrete components and do not affect the application of NDT-CE methods. Ultrasonic pulse-echo (UPE) was used to test the flaws in the specimens. The delaminations were created by applying expansive mortar in prepared through holes. Three specimens with two delaminations each were built and tested using UPE.