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- Temperature sensing (2) (entfernen)
The luminescence intensity ratio (LIR) of the green emissions of the near-infrared excited NaYF4:Yb3+,Er3+ nanocrystals is a promising method for temperature sensing. Here, the influence of excitation power density, excitation pulse length, excitation wavelength, silica shell, and solvent on the LIR and its temperature response is reported. The primary objective is to study the LIR mechanism and the impact of measurement and environmental parameters on the calibration and precision of the LIR. The LIR value is demonstrated to be unaffected by the excitation intensity in the studied range. This result is essential, considering the application feasibility of the LIR method as temperature sensor, where the effective excitation power density depends on the sample matrix and the distance excitation light travels in the sample. The pulsed excitation, however, results in an increase in the LIR value upon short pulse width. Silanization of bare nanocrystals has no effect on the LIR values, but the local warming of H2O samples under laser exposure results in slightly increased LIR values compared to other solvents; D2O, oleic acid, and dimethyl sulfoxide. The thermal quenching of luminescence lifetimes of Er3+ emission is proved to be too weak for sensing applications.
We introduce the optical frequency domain reflectometry (OFDR) technique based on intensity modulation frequency sweep measurement for distributed disturbance measurement in optical fibres. By evaluating interferometric Rayleigh scattering changes along the fibre, strain and temperature changes are detected with 100 nε sensitivity and 10 mK resolution. The vibration frequencies for low frequencies and up to the kHz-range can be obtained from power change Evaluation in the spatial domain. This novel OFDR approach is a low-cost alternative for distributed disturbance measurement up to distances of several kilometres.