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- 6 Materialchemie (1)
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Non-destructive testing (NDT) of concrete structures is performed using pulse-echo methods. According to the type of the applied waves it can be classified as acoustic (Impact-Echo, Ultrasonics) and electromagnetic methods (Radar). The results are visualised through different imaging processes. This work is performed in the frame of a research project promoted by Deutsche Forschungsgemeinschaft (FOR384). The objective of data fusion is to use the complementary information of the different methods. Radar can detect metallic reflectors in concrete (metallic ducts and concrete reinforcement) very well. This method is not able to locate defects behind these reflectors (injecting defects, defects behind close concrete reinforcement), because the electromagnetic waves are completely reflected at metals. The acoustic methods are able to compensate this deficit i.e. Acoustic waves can penetrate through metal. But acoustic waves in the ultrasonic range are completely reflected by air layers. Air layers have smaller influence on radar propagation, so that both methods complement each other. In order to be able to combine the NDT-data from several methods records at the same volume, the different data setsmodes of signals must be adapted. The ultrasonic and radar data have to be reconstructed with programs based on the Synthetic Aperture Focusing Technique (SAFT) before data fusion. Subsequently, a conversion of the data into a uniform format has to be carried out. This is a prerequisite in order to keep the data exchange between the project partners as simple as possible. After the data sets are imported and transferred into a common reference system, they can be processed with operations according to the purpose of the investigation. Results, which have been achieved in concrete test specimen with radar and ultrasonics, will be presented and will show the feasibility of the data fusion method.
In this work, the applicability of a new 3D micro X-ray fluorescence (3D Micro-XRF) laboratory spectrometer for the investigation of historical glass objects is demonstrated. The non-destructiveness of the technique and the possibility to measure three-dimensionally resolved fluorescence renders this technique into a suitable tool for the analysis of cultural heritage objects. Although absorption and resolution effects complicate qualitative analysis of the data, layered structures can be distinguished from homogeneous samples without the need for full quantification. Different manufacturing techniques were studied in this work with the help of hand-made reference samples. With the gained knowledge it could be shown for the investigated historical glass object, that black enamel as a stained glass contour colour was used in a cold painting. The object was not fired after the application of the black enamel, but instead the adhesion of the paint was solely provided through organic binding agents and the backing with metal foils. Thus, for the manufacturing of the object, a mixture of cold painting technique with a stained glass color was used. Quantitative measurements with a 3D Micro-XRF setup at the Berlin synchrotron BESSY II confirm the assumptions drawn on the basis of the qualitative investigation with the 3D Micro-XRF spectrometer with X-ray tube excitation.
Alkali-silica reaction (ASR) is a chemical reaction within concrete which can lead over time to cracking and spalling. Due to the complexity of the problem, it still causes damage to concrete constructions worldwide.
The publication aims to illustrate the interdisciplinary research of the German Federal Institute for Materials Research and Testing (BAM) within the last 20 years, considering all aspects of ASR topics from the macro to the micro level. First, methods for characterization and assessment of ASR risks and reaction products used at BAM are explained and classified in the international context. Subsequently the added value of the research approach by combining different, preferably nondestructive, methods across all scales is explained using specific examples from a variety of research projects. Aspects covered range from the development of new test-setups to assess aggregate reactivity, to analysis of microstructure and reaction products using microscopical, spectroscopical and X-ray methods, to the development of a testing methodology for existing concrete pavements including in-depth analysis of the visual damage indicator and the de-icing salt input using innovative testing techniques. Finally, research regarding a novel avoidance strategy that makes use of internal hydrophobization of the concrete mix is presented.
In this paper, a method is presented for the numerical computation of dispersion properties and mode shapes of guided waves in plate structures. The formulation is based on the Scaled Boundary Finite Element Method. The through-thickness direction of the plate is discretized in the finite element sense, while the direction of propagation is described analytically. This leads to a standard eigenvalue problem for the calculation of wave numbers. The proposed method is not limited to homogeneous plates. Multi-layered composites as well as structures with continuously varying material parameters in the direction of thickness can be modeled without essential changes in the formulation. Higher-order elements have been employed for the finite element discretization, leading to excellent convergence for complex structures. It is shown by numerical examples that this method provides highly accurate results with a small number of nodes while avoiding numerical problems and instabilities.
This data article presents characteristic acoustic and flow data of a fluidic ultrasonic transducer as well as acoustic data of a commercial piezoelectric ultrasonic transducer used in non-destructive testing for civil engineering. The flow data has been acquired using hot-wire anemometry and a Pitot tube. The three-dimensional acoustic data of both devices has been acquired using a calibrated microphone. The distribution of characteristic acoustic properties of both transducers are extracted and given in addition to the raw data. The data presented in the article will be a valuable source for reference and validation, both for developing fluidic and alternate ultrasound generation technologies. Furthermore, they will give additional insight into the acoustic-flow interaction phenomena of high speed switching devices. This article is accompanying the paper Experimental Analysis of the Acoustic Field of an Ultrasonic Pulse Induced by a Fluidic Switch (Bühling et al., 2021) published in The Journal of the Acoustical Society of America, where the data is interpreted in detail and the rationale for characteristic sound properties of the fluidic transducer are given.
An approach to adhesive bond characterisation using guided acoustic waves in multi-layered plates
(2021)
An approach for the non-destructive characterisation of adhesive bonds using guided ultrasonic waves is presented. Pulsed laser radiation is used to thermoacoustically excite broadband ultrasonic waves in a multi-layered sample, consisting of a metal plate adhesively joined to a polymeric layer using synthetic resin. The resulting signals are received by a purpose-built piezoelectric transducer. Varying the distance between excitation and detection yields spatio-temporal measurement data, from which the dispersive properties of the propagating waves can be inferred using a two-dimensional Fourier transform, assuming the plates to act as coupled waveguides. Coupled multi-layered waveguides show an effect referred to as mode repulsion, where the distance between certain modes in the frequency-wavenumber domain is assumed to be a measure of coupling strength. Measurements at different stages of curing of the adhesive layer are performed and evaluated. A comparison of the results shows changes in the dispersive properties, namely an increased modal bandwidth for the fully cured sample as well as an increased modal distance.
Impulse-thermography is an active method for quantitative investigations of the near surface region of various structures. It has recently been applied and optimised to applications in civil engineering. By using either an internal or external heat source, parts of the structure under investigation are heated up and the transient heat flux is observed by recording the temperature change at the surface as a function of time. This method is very well suited for the detection of voids and honeycombing in concrete, up to concrete covers of 10 cm as well as for the location of delaminations in multi-layered systems (e.g. plaster on concrete, CFRP-laminates on concrete, asphalt on concrete). Also safety relevant defects like voids in tendon ducts and cracks in concrete could be recognised.
Application of synchrotron infrared radiation in the study of organic coatings in cross-sections
(2008)
We present a prototype for automated magnetic stray field testing of ferromagnetic roller bearings. For this purpose NDE-adapted GMR sensor arrays (giant magneto resistance) are used for the detection of surface breaking cracks. The sensors are miniaturized down to the lower µm-regime to achieve adequate spatial resolution. In doing so, sensor arrays with up to 48 elements are used to inspect the bearing surface within a few seconds only. In contrast to magnetic particle inspection (MPI), where the global magnetization requires a further inspection step and succeeding demagnetization, the presented prototype only locally magnetize the surface area in the vicinity of the GMR Sensors. For the local magnetization, the applied sub-surface magnetic field was simulated and proofed for detecting flaws with a depth of a few 10 µm. By multiplexing the sensor array with an adapted read out electronics we quasi simultaneously detect the normal field component of about 100µm above the surface. The detection of artificial notches with a depth of 40 µm and more could be resolved with a SNR better than 20 dB. The presented testing facility is fast and provides a step towards automated testing of safety relevant steel components.