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The current analyses present results of running ductile fracture propagation in high strength X100 line pipe steels under the influence of anisotropy. Mechanical anisotropy is commonly available in pipe products as a result of the manufacturing process, especially, those subjected to hot/cold-worked deformation. The outcomes of the present analyses show that its effect on the behavior of running ductile fracture in cracked pipes undergoing depressurization is meaningful. For instance, the Crack-Tip Opening Angle (CTOA) not only exhibits a strong dependence to the pipe's diameter size, but also to the material's anisotropy nature when compared to a hypothetical isotropic material. Moreover, laboratory scale tests such as those performed on Battelle Drop Weight Tear (BDWT) samples provide useful information about initiation of ductile crack propagation when the anisotropy features are taken into account in the material description.
In this study, the use of dry end milling of carbon fiber reinforced plastics (CFRP) as surface pretreatment for high-strength (structural) adhesive bonding was investigated. Surfaces were pretreated using different milling parameters; subsequently, they were adhesively bonded and tested. In comparison with sanding and other industrial standard pretreatment methods, the measured adhesive strength was significantly lower. Detailed surface investigations utilizing field-emission scanning electron microscopy could identify two major effects for lower adhesion strength. Intralaminar damages and microparticle residues on the created surface reduced the strength of the CFRP adhesive joints. This eventually explains results from investigations on milling pretreated repairs. By application of power ultrasound cleaning equipment and coating with low viscosity epoxy primers, the authors showed a way to overcome the discovered drawbacks and to improve bond strength significantly. Surface roughness measurements showed that the arithmetical mean roughness R(a)can be used as an effective value for assessment of mechanical pretreated CFRP surfaces as well as for the quality of necessarily following cleaning processes.
The use of non-conventional materials is nowadays of much interest in scientific community. Magneto-rheological elastomers are hybrid materials, which in presence of magnetic fields state a change in their mechanical properties. They are composed by an elastomeric matrix with embedded magnetic particles. One of the most attractive features of these materials is that as soon as the magnetic field is removed from the material, the original mechanical properties are completely recovered, with negligible differences in comparison to the original state. This paper focuses on the study of magnetic characteristics of these smart materials, such as relative permeability and demagnetizing factors, for samples with different volume concentration of ferromagnetic particles.
The paper deals with the investigation of magneto-sensitive elastomers (MSE) and their application in technical actuator systems. MSE consist of an elastic matrix containing suspended magnetically soft and/or hard particles. Additionally, they can also contain silicone oil, graphite particles, thermoplastic components, etc., in various concentrations in order to tune specific properties such as viscosity, conductivity and thermoelasticity, respectively. The focuses of investigations are the beneficial properties of MSE in prototypes for locomotion and manipulation purposes that possess an integrated sensor function. The research follows the principle of a model-based design, i.e. the working steps are ideation, mathematical modelling, material characterization as well as building first functional models (prototypes). The developed apedal (without legs) and non-wheeled locomotion systems use the interplay between material deformations and the mechanical motion in connection with the issues of control and stability. Non-linear friction phenomena lead to a monotonous forward motion of the systems. The aim of this study is the design of such mechanical structures, which reduce the control costs. The investigations deal with the movement and control of ‘intelligent’ mechanisms, for which the magnetically field-controlled particle-matrix interactions provide an appropriate approach. The presented grippers enclose partially gripped objects, which is an advantage for handling sensitive objects. Form-fit grippers with adaptable contour at the contact area enable a uniform pressure distribution on the surface of gripped objects. Furthermore, with the possibility of active shape adaptation, objects with significantly differing geometries can be gripped. To realise the desired active shape adaptation, the effect of field-induced plasticity of MSE is used. The first developed prototypes mainly confirm the functional principles as such without direct application. For this, besides the ability of locomotion and manipulation itself, further technological possibilities have to be added to the systems. The first steps are therefore being taken towards integrated MSE based adaptive sensor systems.
In the current research, magnesium and its alloys have been intensively studied as resorbable implant materials. Magnesium materials combine their good mechanical properties with bioactivity, which make them interesting for guided bone regeneration and for the application as barrier membranes. In this study, the in vitro degradation behavior of thin magnesium films was investigated in cell medium and simulated body fluid. Three methods were applied to evaluate corrosion rates: measurements of (i) the gaseous volume evolved during immersion, (ii) volume change after immersion, and (iii) polarization curves. In this comparison, measurements of H2 development in Dulbecco's modified Eagle's medium showed to be the most appropriate method, exhibiting a corrosion rate of 0.5 mm·year−1. Observed oxide and carbon contamination have a high impact on controlled degradation, suggesting that surface treatment of thin foils is necessary. The bioactivity test showed positive results; more detailed tests in this area are of interest.
Thermomechanical shape memory materials have certain disadvantages when it comes to 3D volumetric reproduction intended for rapid prototyping or robotic prehension. The need to constantly supply energy to counteract elastic retraction forces in order to maintain the required geometry, together with the inability to achieve conformal stability at elevated temperatures, limits the application of thermal shape memory polymers. Form removal also presents problems as most viscoelastic materials do not ensure demolding stability. This work demonstrates how magnetoactive boron−organo−silicon oxide polymers under the influence of an applied magnetic field can be used to achieve energy free sustainable volumetric shape memory effects over extended periods. The rheopectic properties of boron−organo−silicon oxide materials sustain form removal without mold distortion.
This study investigates the vibration reduction of tall wind-excited buildings using a tuned mass damper (TMD) with an inerter (TMDI). The performance of the TMDI is computed as a function of the floor to which the inerter is grounded as this parameter strongly influences the vibration reduction of the building and for the case when the inerter is grounded to the earth whereby the absolute acceleration of the corresponding inerter terminal is zero. Simulations are made for broadband and harmonic excitations of the first three bending modes, and the conventional TMD is used as a benchmark. It is found that the inerter performs best when grounded to the earth because, then, the inerter force is in proportion to the absolute acceleration of only the pendulum mass, but not to the relative acceleration of the two inerter terminals, which is demonstrated by the mass matrix. However, if the inerter is grounded to a floor below the pendulum mass, the TMDI only outperforms the TMD if the inerter is grounded to a floor within approximately the first third of the building’s height. For the most realistic case, where the inerter is grounded to a floor in the vicinity of the pendulum mass, the TMDI performs far worse than the classical TMD.
In order to achieve the energy and efficiency goals in modern automotive press shops, press systems with increasingly high stroke rates are being implemented (Meinhardt in proceedings of ACI forming in car body engineering. Bad Nauheim, Germany 2012). As a side effect, the structural dynamic loads on the press and especially on the forming tool increase. Hence, to design reliable and withstanding forming tools, a detailed knowledge of the vibrations and resulting critical loads is essential. In this paper, the main focus is put on the vibration of the blankholder—the heaviest moving component in the forming tool. To predict those vibrations, a coupled multibody-finite element simulation (MBS-FEM) is conducted, which combines rigid and elastic modeling approaches. Also, an experimental validation of the blankholder vibration under operational load is carried out. To compare the numerical and experimental results—both in time and frequency domain—an 1/3-octave analysis of a blankholder’s vibrational speed is performed. The test measurements agree well with the MBS-FEM simulation.
This paper presents experimental fatigue tests on specially shaped specimens made from quenched and tempered steel 42CrMoS4 and nodular cast iron EN-GJS-600-3. The specimens are geometrically designed to resemble actual subcomponents of forming and cutting dies for sheet metal manufacturing. These subcomponents have failed in the past.Experiments are carried out using a fictive load-time function, which is a modification of an actually measured load curve and has variable mean and amplitude values. This first test series serves as a general validation of a subsequent fatigue analysis. A second test series is carried out with constant mean and amplitude values with a load ratio 𝑅≈0. Here, the load frequencies in the individual test runs are varied between f = 5 Hz and f = 45 Hz in order to investigate the influence of the frequency. Both series are performed on a servo-hydraulic testing machine.The experimental data is then statistically evaluated. The values for the scatter correlate with data from the literature. The data from the test series with the fictive load-time function can thus be used for subsequent validation of a fatigue calculation, which will be addressed in a future publication. Most significant are the findings from the second series of experiments with varied load frequencies, as a significant frequency influence could be detected. Furthermore, the hardening and softening behavior under cyclic loading and the fracture behavior of the materials are analyzed and compared with data from the literature.
Application of a Krylov subspace method for an efficient solution of acoustic transfer functions
(2021)
Solving acoustic radiation problems, arising from systems including fluid–structure interaction, is of interest in many engineering applications. Computing frequency response functions over a large frequency range is a concern in such applications. A method which solves the Helmholtz equation for multiple frequencies in one step is the matrix-Padé-via-Lanczos connection for unsymmetric systems, as presented by Wagner et al. [1]. The present work is based on Ref. [1] and presents a method for efficiently computing frequency responses over a frequency range for coupled structural-acoustic problems, where the structure and the acoustic near field are discretized with finite elements and an analytical Dirichlet-to-Neumann map approximates the far field. The method is based on a Krylov-subspace projection technique which derives a matrix-valued Padé approximation for a restricted area in the near field and the pressure field on a spherical boundary. On the spherical boundary, where the finite domain is truncated, the non-local modified Dirichlet-to-Neumann operator is applied as a low-rank update matrix. The present contribution extends this method and incorporates new techniques for a more stable model reduction through the Lanczos algorithm and a novel weighted adaptive windowing technique. Further, structural damping is incorporated, for computing the acoustic radiation of a harmonically excited plate. These computed results are compared with acoustic measurements in an anechoic chamber and verified with computational results obtained with a commercial code that uses the perfectly matched layer method.
finite element simulation of sheet metal forming, shell elements are widely used. The limits of applicability of the shell elements are sometimes disregarded, which leads to an error in predictions of important values such as springback geometry. The underlying kinematic assumptions of the shell elements do not hold where the thickness of In the metal sheet approaches the value of the radius of curvature. Complex three-dimensional material behavior effects cannot be represented precisely as the result of the simplified kinematics. Here we present a model adaptivity scheme based on a model error indicator. The model-adaptive technique presented in this paper aides to resolve only the critical areas of the structure with a three-dimensional discretization while keeping reasonable computational cost by utilizing shell elements for the rest of the structure. The model error indicator serves as a guide for subsequent automatic adaptive re-meshing of the work-piece followed by a model-adaptive finite element analysis. The accuracy of the approximation obtained by the model-adaptive technique coincides well with that of a more expensive solution obtained with solid elements only.
The Sandia Fracture Challenges provide a forum for the mechanics community to assess its ability to predict ductile fracture through a blind, round-robin format where mechanicians are challenged to predict the deformation and failure of an arbitrary geometry given experimental calibration data. The Third Challenge (SFC3) required participants to predict fracture in an additively manufactured (AM) 316L stainless steel bar containing through holes and internal cavities that could not have been conventionally machined. The volunteer participants were provided extensive data including tension and notched tensions tests of 316L specimens built on the same build-plate as the Challenge geometry, micro-CT scans of the Challenge specimens and geometric measurements of the feature based on the scans, electron backscatter diffraction (EBSD) information on grain texture, and post-test fractography of the calibration specimens. Surprisingly, the global behavior of the SFC3 geometry specimens had modest variability despite being made of AM metal, with all of the SFC3 geometry specimens failing under the same failure mode. This is attributed to the large stress concentrations from the holes overwhelming the stochastic local influence of the AM voids and surface roughness. The teams were asked to predict a number of quantities of interest in the response based on global and local measures that were compared to experimental data, based partly on Digital Image Correlation (DIC) measurements of surface displacements and strains, including predictions of variability in the resulting fracture response, as the basis for assessment of the predictive capabilities of the modeling and simulation strategies. Twenty-one teams submitted predictions obtained from a variety of methods: the finite element method (FEM) or the mesh-free, peridynamic method; solvers with explicit time integration, implicit time integration, or quasi-statics; fracture methods including element deletion, peridynamics with bond damage, XFEM, damage (stiffness degradation), and adaptive remeshing. These predictions utilized many different material models: plasticity models including J2 plasticity or Hill yield with isotropic hardening, mixed Swift-Voce hardening, kinematic hardening, or custom hardening curves; fracture criteria including GTN model, Hosford-Coulomb, triaxiality-dependent strain, critical fracture energy, damage-based model, critical void volume fraction, and Johnson-Cook model; and damage evolution models including damage accumulation and evolution, crack band model, fracture energy, displacement value threshold, incremental stress triaxiality, Cocks-Ashby void growth, and void nucleation, growth, and coalescence. Teams used various combinations of calibration data from tensile specimens, the notched tensile specimens, and literature data. A detailed comparison of results based of these different methods is presented in this paper to suggest a set of best practices for modeling ductile fracture in situations like the SFC3 AM-material problem. All blind predictions identified the nominal crack path and initiation location correctly. The SFC3 participants generally fared better in their global predictions of deformation and failure than the participants in the previous Challenges, suggesting the relative maturity of the models used and adoption of best practices from previous Challenges. This paper provides detailed analyses of the results, including discussion of the utility of the provided data, challenges of the experimental-numerical comparison, defects in the AM material, and human factors.
Basalt fabric composite, with different twill wave reinforcements, i.e. twill 2/2 and twill 1/3, have been studied in this work by means of experimental tests and numerical finite element (FE) simulations. As fabric reinforcements show repeating undulations of warp and fill yarn, simple mixtures law cannot be applied.
As a consequence, the mesoscopic scale, lying between the microscopic and the macroscopic one, has to be taken into account to mechanically characterize a fabric reinforced composite. The aim of this work is to evaluate the stiffness of a fabric reinforced composite in warp and fill direction. In particular a numerical FE
model, assuming elliptical sections and sinusoidal shape of the yarns, has been implemented and experimental tests have been carried out in order to validate the proposed model. Finally, the strength and the failure modes le orientation, have been experimentally investigated.
Fiber-reinforced plastic (FRP) tubes are used in many different industries, such as electrical engineering and pipeline construction. The tubes are frequently subjected to bending loads, depending on the application. In order that the dimensioning of the tubes can be ensured, analytical bending models are used to calculate the resulting stresses, strains and displacements in the individual layers of the laminate. This enables the making of a statement about the failure of the fiber-reinforced tube by choosing an appropriate failure criterion. For the use of these bending models, it is necessary to understand the respective underlying theory. The theory provides the basis for the mathematical description of the mechanical properties for a single-layered tube and using the relationships between the stresses and strains that occur in the Cylindrical coordinate system for this calculation step. For this reason, a redefinition of the compliance matrix from the transformation about the winding angle to the Cylindrical coordinate system and a modification of the stress and strain vectors is necessary, because the defined Cartesian coordinate system of the model cannot be used for wounded FRP tubes. The transformation causes an exchange of entries in the compliance matrix, which remain in the correct relationship between the particular stress and strains. This step is not specified and may lead to incorrect results due to the incorrect entry of compliances. The present publication refers to sketch on this issue and represent a simplification of the changeover to the level required by the bending models notation of vectors in the form of a permutation. In addition, a new name for the pre-acquisition of the redefined compliances is given to prevent confusion when entering the material law of a bending model. Finally, the permuted and redefined compliances are proved in an example to determine their accuracy.
Purpose:
A prepreg production device in laboratory scale is used to develop the production process of unidirectionally reinforced prepregs.
Design/methodology/approach:
The aim of the prepreg production device is to impregnate different types of reinforcement fibers with an arbitrarily selectable thermoset matrix system that completely satisfies the requirements for autoclave processing. As the prepreg production device is designed and built up modularly every module corresponds one step in the process.
Findings:
To identify the parameters of the production process and investigate its sensitivity on the material quality of both the prepreg as an uncured semi-finished product and the composite as the cured material experimental investigations regarding the resin flow, fiber volume content, mass per unit area and void content are carried out. Overall four material combinations have been investigated, where in each case the selected impregnation temperature and the width of the impregnation gap has been reproducibly varied in selected steps.
Research limitations/implications:
The experimental characterization of the prepregs and of the composite material is carried out according to German standards.
Purpose:
of this paper is experimental investigation of damping properties of unidirectionally and fabric reinforced plastics by the free decay method.
Design/methodology/approach:
For the evaluation of the presumed effect experimental structural dynamic investigations comparing unidirectionally and fabric reinforced plastics are carried out. In detail the free decay behaviour of flat beamlike specimens under fixed-free boundary conditions and relatively constant and reproducible displacement excitation is investigated. Findings: The vibrating structure has been measured by a laser scanning vibrometer PSV 400 from POLYTEC. In both cases evaluation of the results yields enhanced damping properties of the specimens with fabric reinforcement compared to the unidirectionally reinforced specimens. The results justify the presumed acting of a mesomechanic kinematic.
Research limitations/implications:
The results show that in either case the material damping in terms of the logarithmic decrement of the fabric reinforced material is higher than the material damping in of the unidirectionally reinforced material. Additionally, when the fabric reinforced specimens are addressed, in each case the plain weave reinforced specimens exhibited higher values of the material damping as the twill weave 2/2 reinforced ones.
Originality/value:
Ondulations in fabrics as a textile semi-finished product are caused by the alternating crossing of warp and fill yarns. In the mesoscopic scale the acting of a mesomechanic kinematic is presumed to enhance the damping properties under cyclic elastic deformation. For the evaluation of the presumed effect experimental structural dynamic investigations comparing unidirectionally and fabric reinforced plastics are carried out.
Purpose: A route to manufacture porous carbon fiber reinforced plastic (CFRP) for study purposes is described. Design/methodology/approach: The porous CFRP is characterized using standard techniques such as matrix digestion as well as the more sophisticated method of high resolution Microfocus X-Ray Tomography (μCT). A comparison of the results of those methods is presented. The mass gains of specimens with a wide range of porosity have been measured both in constant humidity and in alternating environments. Findings: It could be shown that severe temperature changes can temporarily increase the moisture content of porous CFRP. However, after the return to a constant environment, the moisture content returns back to saturation levels. Furthermore, it could be shown by X-Ray Tomography that even under severe climatic conditions no permanent liquid water condensates inside the pores. Research limitations/implications: Using Microfocus Computed Tomography it could be shown that even after nearly a year under hot-wet conditions and more than 150 severe temperature cycles there is no liquid water detectable inside the pores. Originality/value: In this paper the effects of severe temperature changes and high humidity on porous CFRP.
Filament wound composite structures are widely used in the field of pressure vessels, tubes, pipelines or rocket cases. The mechanical behavior of these structures is typically different from those of flat laminated structures due to an alternating lay-up sequence, winding tension and manufacturing induced imperfections. However, design and analysis issues require the same engineering data as used for laminated structures in general. It has therefore become necessary to establish an accompanying quality assurance procedure following the production process to identify the material properties of the manufactured tubes especially for the single layer. Consequently, there are three different approaches of determining the elastic moduli and tensile strengths of a filament wound laminate. Either specimens are resected from a curved tube, from a tube with plane areas or standardized flat specimens are manufactured under deviating production conditions. All approaches entail disadvantages, whether in terms of manufacturing or testing parameters including geometry, lay-up sequence, porosity, fiber tension and load direction. This study presents the discrepancies in the determination of mechanical properties of a filament wound glass-fiber-reinforced polymer tube on curved or cylindrical specimens and flat specimens produced to meet the specifications of international standards. In order to obtain material properties not only in longitudinal but also in transverse direction of the tubes, the so-called split-disk tensile test modeled after ASTM Standard D 2290, is used with tube segments.The procedures of specimen production and preparation are described in detail. Material properties such as the fiber volume and void content of the composite specimens are conducted in order to consider quality and production differences. Finally tensile tests are performed and the results are compared and discussed.
In this paper, the idea of fiber-oriented repair geometries for carbon fiber reinforced plastics (CFRP) is investigated. It considers the differing mechanical properties of unidirectional fiber reinforced material by excluding overlapping regions perpendicular to the fiber direction of the particular layer.
A mechanical and numerical comparison of tensile strength of stepped joints with continuous step lengths per ply and stepped joints with reduced step lengths in plies with fiber orientation differing from load direction is performed.
Finite element simulations show similar shear stresses. Mechanical tests of CFRP laminates with stepped joints show no significant deviation in tensile strength, in spite of a joint length reduction of nearly 40%. This leads to the possibility of a significant reduction of repair area.
Purpose:
The present work deals with the experimental investigation concerning the energy dissipation capacity of different kinds of reinforcement fibres in monolithic and hybrid layups under high velocity impact loads. The investigated kinds of fibres are carbon, glass and basalt. Design/methodology/approach:
The test panels have been impregnated with thermoset resin. Curing was done by autoclave processing. In order to obtain comparable fibre volume contents of approx. 60 % in the different layups (monolithic and hybrid without and with separating layer), curing cycles adapted to the type of layup have been identified. The resulting fibre volume content of the test panels has been determined both by weighing and experimentally by chemical extraction and calcination. The impact load was applied by an instrumented experimental setup. Thereby both commercially available bullets and bearing balls accelerated with weighted propellant in a sabot have been used as impactors. The measured values are the velocities of the bearing balls as the impactor before and after penetration of the test panels.
Findings:
In both cases the results show the energy dissipation capacity of each single kind of fibre in case of the monolithic layups as well as the enhanced properties of the hybrid stacked layups without and with the separating layer as a core material. Typical failure modes on the impact surface and on the outlet areas are identified.
Research limitations/implications:
The influence of the respective kind of impactors, namely bullets and bearing balls, on the evaluated results is identified. Thereby the bearing balls exhibited a higher degree of reproducibility due to several reasons.
Originality/value:
Fibre reinforced plastics with hybrid stacking sequences can be used as load-bearing structures and at the same time as safety structures for passengers in automotive or aerospace applications. Moreover, with the hybrid stacked composites lightweight concepts can efficiently be realized regarding energy saving issues.
Purpose:
A review regarding the acting mechanisms of structural dynamic material damping in fabric reinforced composites is presented. Design/methodology/approach:
Mechanical acting principles identified by different investigations are considered. Aspects of the determination and calculation of structural mechanical material properties of fabric reinforced composites are described. Approaches intending the description and classification of ondulations in fabrics reinforced single layers are demonstrated.
Findings:
The mesomechanic geometry of fabrics is not considered sufficiently by relatively simple homogenization approaches. Yet, it significantly affects its structural dynamic material properties, especially the dynamic ones.
Research limitations/implications:
In each case the different damping mechanisms act coupled and occur at the same time. Therefore a separation procedure is required in any case. Practical implications: Against the background of the comparison and remarks of the presented papers a reasonable further procedure is recommended. Thereby, FE-calculations with a parametrical variation of the mesomechanic geometry in order to identify kinematic correlations due to geometric constraints are suggested.
Originality/value:
The idea of the representation of the geometric conditions in terms of a degree of ondulation is described. Such a non-dimensional specific value representing the intensity of the ondulation would enable the comparability of the results of different kinds of investigations.
Purpose:
A parametric characterization of a mesomechanic kinematic caused by ondulation in fabric reinforced composites is investigated by numerical investigations.
Design/methodology/approach:
Due to the definition of plain representative sequences of balanced plain-weave and twill-weave 2/2 fabric reinforced single layers based on sines the variable geometric parameters are the amplitude and the length of the ondulation.
Findings:
The mesomechanic kinematic can be observed in the FE analyses for both kinds of fabric constructions.
Research limitations/implications:
The FE analyses consider elasticity and contraction due to Poisson effects, respectively, of the model under selected longitudinal strains. Practical implications: The results are evaluated at relevant positions on the centre-line of the ondulated warp-yarn of the plain representative model. A direct and linear coupling in case of the transversal kinematic behaviour, and thereby a corresponding definite reduction of the evaluated longitudinal strains in terms of the difference of the applied and determined longitudinal strains is identified.
Originality/value:
Both characteristic purely kinematic reactions due to geometric constraints directly depend on the introduced degree of ondulation. This non-dimensional parameter relates amplitude and length of one complete ondulation, and thus represents the intensity of the ondulation of the respective fabric construction.
A parametric characterization of a mesomechanic kinematic caused by ondulation in fabric reinforced composites is investigated by analytical and numerical investigations. Due to the definition of plain representative sequences of balanced plain-weave fabric reinforced single layers based on sines the variable geometric parameters are the amplitude and the length of the ondulation. The mesomechanic kinematic can be observed in both the analytic model and the FE-analyses. The analytic model yields hyperbolic correlations due to the strongly simplifying presumptions that neglect elasticity. In contrast the FE-analyses yield linear correlations in much smaller amounts due to the consideration of elastic parts, yet distinctly.
This paper deals with experimental investigations concerning energy dissipation capacity of different kinds of reinforcement fibres in monolithic and hybrid layups under high-velocity impact loads. The investigated kinds of fibres are carbon, glass and basalt fibres. Therefore test panels, using the same thermoset resin, were built up and cured by autoclave processing. The fibre volume content of the test panels has been determined. Furthermore the influence of a separating layer at selected positions in the hybrid stacked panels was investigated. The results show the influence and the energy dissipation capacity of each single kind of fibre
and the enhanced properties for the hybrid layups by hybrid stacking sequences and the use of a separating core material.
The aim of this study is to compare two different standardized testing procedures, tensile testing and Mode-I double cantilever beam (DCB) testing, to evaluate a possible correlation between the dominant failure in glass fibre-reinforced plastics and their according acoustic emissions (AE). AE is processed by using a burst collection of all recorded transient signals and is further analysed with the k-means clustering algorithm. To generate damage related AE, a series of experiments for tensile testing and Mode-I DCB testing is performed on 16-layer glass fibre/epoxy specimens with a cross-ply lay-up for tensile and an unidirectional lay-up for Mode-I DCB testing. Three sensors at tensile testing and one sensor at Mode-I DCB testing gather AE data. The results of clustered burst signals show a good accordance between both testing procedures, with a similar weighted peak frequency (WPF) range in each classified cluster. In total, three different clusters are determined. An assignment of these three clusters to the three dominant damage mechanisms, visually observed by microscopy, is suggested.
Plastic design allows the exploitation of the full resistance of steel structures by taking advantage of stress–redistributions due to plastic strains exceeding the yield strain. Especially in seismic design the utilization of material reserves and the formation of plastic hinges play an important role. In devastating earthquakes in Northridge (USA) and Kobe (Japan) brittle fracture of welded connections in steel moment frames occurred prior to formation of plastic hinges and utilization of plastic material reserves. The subsequent research works resulted in improved design rules and recommendations for these kinds of failure. But to guarantee sufficient ductile performance of these connections also in the upper shelf region, plastic and earthquake resistant design rules should take into account degradation of strain capacity and toughness properties due to quasi static and especially seismic loading.
In the scope of the current European project “Plastotough”, the main objective is to derive quantified toughness design rules in the upper shelf based on the strain requirements opposed to strain capacities. This paper gives an overview over the research work in performance and shows recent results from experimental and numerical analyses performed within this project for monotonic and cyclic loading.
This paper explores the efficacy of employing local damage models, normally applied to ductile material systems manufactured by subtractive techniques, to additively manufactured laboratory specimens. While these specimens were ductile and metallic, their additive character (i.e. porosity and surface roughness) could have had potential to activate multiple life-limiting failure paths, thus obfuscating failure prediction. Herein, two damage models are considered and compared: the micromechanical Gurson–Tvergaard–Needleman model and a Crack Band model of the strain-based, phenomenological genre. Simulations used to calibrate elastic and plastic material properties and predict damage in a novel, non-standard specimen were quasi-static, explicit. Both damage models proved capable in resolving the experimentally-observed failure path and associated loading conditions. The analyses described herein were made as part of the Third Sandia Fracture Challenge.
This paper investigates the damage behavior of thermoset and thermoplastic fiber-reinforced composites. The specimens were subjected to low-velocity impacts (LVI) to produce barely visible impact damages (BVID). To compare the dependency of the matrix system and the laminate lay-up on the impact damage, four test series were set up. Therefore, laminates with an epoxy (EP) and a polyether ether ketone (PEEK) matrix in a quasi-isotropic (QI) [+45/0/-45/90]2s and an orthotropic (OT) fiber lay-up [0/90]4s were manufactured. To eliminate the influence of variant fiber systems, the thermoplastic tape and the thermoset prepreg contain similar carbon fibers (CF). After impact testing with three different impact energies, inner damages were investigated by using ultrasonic analyses. To get a deeper understanding of the interior damage mechanisms, cross sections of the damaged areas were examined via reflected light microscopy. By using these destructive and non-destructive test methods, significant differences in the damage behavior of composites with thermoplastic and thermoset matrix systems were identified for both laminate lay-ups.
Experimental investigations are conducted to quantify the influence of specimen thickness and orientation on the mechanical properties of selective laser melted stainless steel 316 L. The results indicate that the mechanical strength and ductility increase with increasing specimen thickness until a saturation value is reached from a specimen thickness of about 2 mm. Specimen orientation dependency is pronounced for thin specimens (<1.5 mm), whereas only small deviations in strength are observed for thicker specimens with orientations of 30°, 45° and 90° to build direction. The mechanical properties of the specimen orientation of 0° to build direction shows great deviation to the other orientations and the smallest overall strength. A reliable design of selective laser melted components should account for specimen thickness and orientation, e. g. by a correction factor. Furthermore, it is recommended to avoid loads vertical (90°) and parallel (0°) to build direction to guarantee higher ductility and strength.
New calibration method for high and low triaxiality and validation on SENT specimens of API X70
(2013)
The determination of the exact mechanical properties of material is essential for an optimal and safe design of linepipes. It is especially important for the prevention of over-engineering and the reliable assessment of complex accidental loading, such as extreme bending due to loss of buoyancy of support, or abrupt ground movement. Currently, the focus of research in offshore deepwater installations and linepipes is towards pre-cracked structures with high triaxiality stress states and complex loading histories. At the same time, low triaxiality stress states must be correctly studied in order to represent shear dominated failure in pipes. A comprehensive experimental and numerical program was undertaken to determine the mechanical properties of the traditional API X70 grade of steel. The material was characterized for anisotropic plasticity, fracture initiation and uncracked ductility for various states of stress. The same material was also used for pre-cracked fracture toughness assessment. The experimental program included flat and round specimens. The first type of tests on flat butterfly-shaped, central hole, notched and circular disk specimens; were selected to address the low stress triaxiality range. Tests on round notched bar specimens and SENT fracture mechanics tests extended the characterization and verification process to higher stress triaxiality values. This program covered a wide range of stress conditions and demonstrated their effect on the material resistance to crack extension. Each test conducted was numerically simulated using solid finite element models, matching the exact geometric and loading history features. The numerical simulation provided information on the local stress and strain fields around the location of the potential or existing cracks. Based on the above hybrid experimental/numerical technique tailored for pipe applications, the MMC fracture model was calibrated. The model relates the material ductility not only to stress triaxiality but also to the Lode parameter. The predictive capabilities of the MMC were then evaluated in the case of SENT testing, used extensively in the pipeline industry. It was shown that the present fracture model calibration can describe fracture behavior of SENT experiments.
The Park–Paulino–Roesler (PPR) potential-based model is a cohesive constitutive model formulated to be consistent under a high degree of mode-mixity. Herein, the PPR’s generalization to three-dimensions is detailed, its implementation in a finite element framework is discussed, and its use in single-core and high performance computing (HPC) applications is demonstrated. The PPR model is shown to be an effective constitutive model to account for crack nucleation and propagation in a variety of applications including adhesives, composites, linepipe steel, and microstructures.
An over-the-counter methodology to predict fracture initiation and propagation in the challenge specimen of the Second Sandia Fracture Challenge is detailed herein. This pragmatic approach mimics that of an engineer subjected to real-world time constraints and unquantified uncertainty. First, during the blind prediction phase of the challenge, flow and failure locus curves were calibrated for Ti–6Al–4V with provided tensile and shear test data for slow (0.0254 mm/s) and fast (25.4 mm/s) loading rates. Thereafter, these models were applied to a 3D finite-element mesh of the non-standardized challenge geometry with nominal dimensions to predict, among other items, crack path and specimen response. After the blind predictions were submitted to Sandia National Labs, they were improved upon by addressing anisotropic yielding, damage initiation under shear dominance, and boundary condition selection.
The effect of laser-hybrid welds on deformation and failure behaviour of fracture mechanics specimens is investigated in order to provide quantitative prediction of damage tolerance and residual strength. The simulation of crack initiation and crack extension in hybrid welds is performed by applying GTN damage model. The identification of damage parameters requires combined numerical and experimental analyses. The tendency to crack path deviation during crack growth depends strongly on the constraint development at the interface between base and weld metal. In order to quantify the influence of local stress state on the crack path deviation, the initial crack location is varied. Finally, the results from fracture mechanics tests are compared to real component, beam-column-connection, with respect to fracture resistance.
Detecting Defects Reliably
(2015)
The integration of a broadband pyrometer in a 3-D scanner enables a continuous and local temperature measurement during the quasi-simultaneous laser transmission welding process. Welding tests on polyethylene samples show that defects can be clearly identified based on the temperature signal, despite a high scanning velocity.
A pyrometer, integrated into a 3D‐scanner, offers the possibility to measure the weld seam temperature at quasi‐simultaneous laser transmission welding. Experimental studies have shown that gaps located in the joining zone can be identified by a temperature rise even at a high scanning velocity. This enables the implementation of algorithms for observation and control strategies.
Fehlstellen sicher erkennen
(2015)
Predicting the core temperature during welding is an ambitious aim in many research works. In this work, a 3D-scanner with integrated pyrometer is characterized and used to measure the temperature during quasi-simultaneous laser transmission welding of polyamide 6. However, due to welding in an overlap configuration, the heat radiation emitted from the joining zone of a laser transmission weld has to pass through the upper polymer, which is itself a semi-transparent emitter. Therefore, the spectral filtering of the heat radiation in the upper polymer is taken into account by calibrating the pyrometer for the measurement task. Thermal process simulations are performed to compare the temperature field with the measured temperature signal. The absorption coefficients of the polymers are measured, in order to get precise results from the computation. The temperature signals during welding are in good agreement with the computed mean temperature inside the detection spot, located in the joining area. This is also true for varying laser power, laser beam diameter and the carbon black content in the lower polymer. Both, the computed mean temperature and the temperature signal are representing the core temperature. In order to evaluate the spatial sensitivity of the measurement system, the emitted heat radiation from both polymers is calculated on basis of the computed temperature field. Hereby it is found, that more than 90 percent of the detected heat radiation comes from the joining area, which is a crucial information for contact-free temperature measurement tasks on semi-transparent polymers.
Production of optical and medical devices makes high demands on cleanliness, precision, visual appearance and reliability. Advantages of laser transmission welding – contactless input of energy, high precision, no adhesives and no particle formation – can be fully exploited for this use. For absorber-free welding, lasers emitting in the polymers’ intrinsic absorption spectrum between 1.6 μm and 2 μm are used. Focusing the laser beam with high NA provides large intensity gradients inside the specimen and enables selective fusing of the joining zone without affecting the surface. Since a molten upper surface leads to visible and palpable irregularities and causes warpage, the verticalexpansion of the weld seam is crucial. To meet the high quality and reliability required in the medical and optical industry, online monitoring of the seam is necessary. The aim of this work is the localization and evaluation of the weld seam using pyrometry. First, the emitted thermal radiation is computed, enabling signal analysis regarding origin and spectrum. Thus, assessment of measurement spectrum and forecast of the signal in dependence on seam shape and position is possible. Finally, welding tests with Topas 8007-04 are performed at 200 mm/s feed rate and monitored with 100 kHz. The comparison of tracked data with thin-cuts demonstrates that weld seam localization by pyrometry is possible, enabling online assessment of the process.
We investigate the mechanical and microstructural properties of a diamond-like carbon coating (DLC) which is deposited by plasma enhanced chemical vapor deposition (PECVD) onto an alumina/aluminosilicate glass composite used for biomedical applications. Ball-on-ring tests yield a fracture strength that is essentially influenced by the surface topology/roughness. The surface topology of the coating is investigated by atomic force microscopy (AFM). Tribology tests and nanoindentation represent the wear resistance and hardness; these are properties that are mainly influenced by the microstructural properties of the DLC coating. This microstructure is investigated by transmission electron microscopy (TEM) and analyzed by parallel electron energy loss spectroscopy (PEELS). For the general applicability of the coated composite, the interfacial adhesion of the DLC coating on the comparably rough substrate (roughness amplitudes and wavelengths are in the micrometer range) is important. Therefore, we focus on TEM investigations that show the interface to be free of gaps and pores that we, together with a characteristic microstructure adjacent to the interface, relate to the excellent adhesion. The interlayer consists of a high density of SiC grains, part of them directly bound to the substrate, and part of them bound to other SiC grains. This interlayer is followed by an essentially different region of the coating as concerns the microstructure; this region consists of nanocrystalline diamond particles embedded in an amorphous carbon matrix. It is this heterogeneous microstructure to which we attribute (i) the good adhesion based upon the interface stabilizing SiC grains, and (ii) the high hardness and wear resistance based upon the diamond nanocrystals in the coating.
The morphology and microstructure of an Al2O3 glass composite (trade name In-Ceram, Vita Zahnfabrik) were studied using scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The composite was produced by infiltration of a lanthanum-based glass throughout a porous Al2O3 body. This alumina body was formed by three classes of particles differing in size and shape: faceted particles typically ≤4 μm in diameter, platelets of average diameter 8 μm, 1.5 μm thickness, and small spheres 0.4 μm in diameter. The outstanding strength properties of the composite (600 MPa, ball-on-ring test) are a result of the high wetting capability of the glass phase on the Al2O3 surface. In addition, plastic strain relaxation in the faceted particles by dislocation formation compensates partially for residual stresses and impedes crack formation at the glass/Al2O3 interface.
We investigate the mechanical and microstructural properties of a diamond-like carbon coating (DLC) which is deposited by plasma enhanced chemical vapor deposition (PECVD) onto an alumina/aluminosilicate glass composite used for biomedical applications. Ball-on-ring tests yield a fracture strength that is essentially influenced by the surface topology/roughness. The surface topology of the coating is investigated by atomic force microscopy (AFM). Tribology tests and nanoindentation represent the wear resistance and hardness; these are properties that are mainly influenced by the microstructural properties of the DLC coating. This microstructure is investigated by transmission electron microscopy (TEM) and analyzed by parallel electron energy loss spectroscopy (PEELS). For the general applicability of the coated composite, the interfacial adhesion of the DLC coating on the comparably rough substrate (roughness amplitudes and wavelengths are in the micrometer range) is important. Therefore, we focus on TEM investigations that show the interface to be free of gaps and pores that we, together with a characteristic microstructure adjacent to the interface, relate to the excellent adhesion. The interlayer consists of a high density of SiC grains, part of them directly bound to the substrate, and part of them bound to other SiC grains. This interlayer is followed by an essentially different region of the coating as concerns the microstructure; this region consists of nanocrystalline diamond particles embedded in an amorphous carbon matrix. It is this heterogeneous microstructure to which we attribute (i) the good adhesion based upon the interface stabilizing SiC grains, and (ii) the high hardness and wear resistance based upon the diamond nanocrystals in the coating.
The corrosion behaviour of WE43 magnesium alloys using the mini cell system was studied. Voltammetry and impedance spectroscopy were applied to study on the one hand the effect of microstructure of the working electrode and on the other hand the effect of proteins in the electrolyte. Two types of alloy samples were produced (i) by permanent mould casting and (ii) by gas atomization followed by extrusion. The results showed that the microstructure was strongly influenced by the production process. The extruded samples showed an improved homogeneity of phase distribution compared with cast samples as it was aimed for. Due to increased homogeneity it was expected to find higher corrosion resistance. However, the electrochemical results are contradictory and suggest an additional phase in the extruded microstructure. Using energy dispersive X-ray spectroscopy (EDX) the secondary magnesium rare earths (RE) phase of extruded samples showed differing composition than of cast samples as well as additional oxide phases. After the samples were electrochemically investigated in cell medium with and without fetal calf serum (FCS), an impact of FCS was detected in voltammetry due to the length of the polarisation curve. As the tip of the mini cell in contact with the working electrode is small, developing gases tend to spread on the working electrode and break the contact of liquid to the counter electrode; which results in disrupting the current flow. This effect was more pronounced when rising the voltage and was found reduced when using electrolytes with FCS. Impedance spectra were slightly deformed by FCS, seen as a kinetic effect but not as a basic differing corrosion reaction. The insight into the effects of FCS was provided by the mini cell system as this system enables to collect entire series of measurements. In contrast of two single measurements, those series reflected the slight difference caused by FCS. The focus of the electrochemical corrosion study was set on the first half hour of immersion.
Electrophoretic chitosan deposits on stainless steel AISI 316 L were produced and characterized. The coating quality (thickness, defectiveness, corrosion protection ability) was seen to depend on the electric field used for EPD. Corrosion studies in concentrated simulated body fluid (SBF5) demonstrated that the surface characteristics of AISI 316 L can be positively influenced by the chitosan coating.
This review comprehensively covers research carried out in the field of degradable coatings on Mg and Mg alloys for biomedical applications. Several coating methods are discussed, which can be divided, based on the specific processing techniques used, into conversion and deposition coatings. The literature review revealed that in most cases coatings increase the corrosion resistance of Mg and Mg alloys. The critical factors determining coating performance, such as corrosion rate, surface chemistry, adhesion and coating morphology, are identified and discussed. The analysis of the literature showed that many studies have focused on calcium phosphate coatings produced either using conversion or deposition methods which were developed for orthopaedic applications. However, the control of phases and the formation of cracks still appear unsatisfactory. More research and development is needed in the case of biodegradable organic based coatings to generate reproducible and relevant data. In addition to biocompatibility, the mechanical properties of the coatings are also relevant, and the development of appropriate methods to study the corrosion process in detail and in the long term remains an important area of research.
Mg and Mg alloys are becoming more and more of interest for several applications. In the case of biomaterial applications, a special interest exists due to the fact that a predictable degradation should be given. Various investigations were made to characterize and predict the corrosion behavior in vitro and in vivo. Mostly, the simple oxidation of Mg to Mg2+ ions connected with adequate hydrogen development is assumed, and the negative difference effect (NDE) is attributed to various mechanisms and electrochemical results. The aim of this paper is to compare the different views on the corrosion pathway of Mg or Mg alloys and to present a neglected pathway based on thermodynamic data as a guideline for possible reactions combined with experimental observations of a delay of visible hydrogen evolution during cyclic voltammetry. Various reaction pathways are considered and discussed to explain these results, like the stability of the Mg+ intermediate state, the stability of MgH2 and the role of hydrogen overpotential. Finally, the impact of MgH2 formation is shown as an appropriate base for the prediction of the degradation behavior and calculation of the corrosion rate of Mg and Mg alloys.
The characterization of oxygen diffusion zone in titanium and the effect of this zone on macroscopic properties are still of high interest for a base to predict and to enhance life time of titanium and titanium alloy components. The aim of this study was to contribute to the understanding of the impact of oxygen on fatigue properties of oxygen diffusion hardened Ti and Ti alloys. Oxygen diffusion hardening implies two process steps, first the oxidation of the surface and secondly the diffusion of oxygen into metal matrix. Due to the one-step treatment used in this study the oxidation step could take place easily avoiding scaling and grain boundary diffusion. In spite of this precaution, the fatigue properties in the present study were found to be decreased after the performed oxygen diffusion hardening. The reason for the reduction of mechanical properties were claimed to be oxide clusters on the surface acting as crack initiation sites. Comparison and discussion with literature revealed varying partially contradictory fatigue results. Therefore precise analysis of the fatigue failure is necessary as a base for further development of the oxygen diffusion hardening.