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To detect convective gas flow inside the large airways during high frequency oscillated ventilation (HFOV) the fluorinated contrast gas Heptafluoropropane was used for 19F-MRI. In a first study the comparison between constant flow measurements and Computational Fluid Dynamics (CFD) simulations provided a good agreement. In a following experiment oscillated flow was applied to a lung phantom consisting of ventilation bag and long pipe. The pressure wave inside the pipe was explored point-by-point and corresponding velocities were determined. With these experiments it could be shown for the first time that flow measurement during HFOV using fluorinated contrast gas is feasible.
Titanium is used in many areas due to its excellent mechanical, biological and corrosion-resistant properties. Implants often have thin and filigree structures, providing an ideal application for laser fine cutting. In literature, the main focus is primarily on investigating and optimizing the parameters for titanium sheet thicknesses greater than 1 mm. Hence, in this study, the basic manufacturing parameters of laser power, cutting speed and laser pulsing of a 200 W modulated fibre laser are investigated for 0.15 mm thick titanium grade 2 sheets. A reproducible, continuous cut could be achieved using 90 W laserpower and 2 cutting-speed. Pulse pause variations between 85–335 μs in 50 μs steps and fixed
pulse duration of 50 μs show that a minimum kerf width of 23.4 μm, as well as a minimum cut edge roughness Rz of 3.59 μm, is achieved at the lowest pulse pause. An increase in roughness towards the laser exit side, independent of the laser pulse pause, was found and discussed. The results provide initial process parameters for cutting thin titanium sheets and thus provide the basis for further investigations, such as the influence of cutting gas pressure and composition on the cut edge.
Influence of carbon content on the formation of TiC at diffusion bonded titanium-steel interface
(2023)
Hot pressing of pure Ti and various carbon steels in a temperature range of 950 – 1050 °C creates an up to 9 μm thick compound layer of TiC at the Ti/ steel interface. The calculation of the activation energy for layer formation is 126.5 - 136.7 kJ/mol, independent of the steels carbon content. As the carbon content of the steel increases, the layer thickness also increases, which provides enormous potential for the surface modification of Ti/ Ti-alloys.
Application of Magnetic Garnet Films for Magnetooptical Imaging of Magnetic Field Distributions
(2004)
Rare-earth iron garnet films of high quality can be grown by liquid phase epitaxy on paramagnetic substrates of gadolinium galliumgarnet. Such films are currently used for imaging of the spatial distribution of magnetic fields. This application is based on the Faraday rotation which can strongly be enhanced by bismuth incorporation.
The physical properties of the films can be controlled by the chemical composition, the growth conditions and the crystallographic orientation. The sensor properties like sensitivity, dynamic range, signal linearity and unambiguity must be optimized according to the application desired. These properties, however, are not independent of each other. In addition, they strongly depend on the optical wavelength. Thus, it is necessary to find compromises.
The influence of Faraday rotation, Faraday ellipticity, optical absorption, magnetic anisotropies and film thickness on the performance of a magnetooptical indicator film is investigated. Based on the swing of the photoresponse, a new optimization process is introduced. The process is experimentally verified and application examples are demonstrated.
Furthermore, two methods are presented to enhance the sensitivity of magnetooptical sensors. Using specific crystallographic orientations, an easy plane of magnetization can be induced which is inclined with respect to the film plane. If the magnetization lies in this plane a very high sensitivity is achieved. The dependence of the geometrical orientation of the easy plane on the growth direction is calculated and the sensitivity and dynamic range are derived. Experimental results of a [112] oriented garnet film are in good agreement with calculations.
Garnet films which are magnetized along the film normal due to a strong induced uniaxial anisotropy support magnetic domains. If the collapse field perpendicular to the film plane is small, such films can be used as very sensitive indicator films. Such films are easier to prepare than sensitive in-plane films. However, the spatial resolution is limited by the size of the domains. This disadvantage can be avoided by applying a bias field in the film plane. Directly at the in-plane collapse field the sensor film is in-plane magnetized yielding high spatial resolution at still high sensitivity. The variation of magnetooptical images with in-plane induction is demonstrated. Experimental results are in agreement with calculations.
A method of referencing in an extrinsic optical fiber sensor system utilizing temperature dependence of the absorption edge in a semiconductor crystal (semi-insulating iron-doped indium phosphide) is demonstrated. The intensity reference is provided by controlling the temperature of an LED source and transmission measurements with different emission spectra. A transient operation regime is introduced. The entire process is controlled by a microprocessor unit. The performance of the sensor system is investigated and it is shown that the connector losses may be compensated for. Contrary to the published works performed with GaAs crystals it was not observed that the absorption coefficient of the semiconductor follows the law for idealized direct-gap semiconductor but can be described by the so-called Urbach tail. Since the proposed sensor system comprises a single LED source, simple electronics and no optical fiber couplers it is promising for realization of low-cost fiber-optic temperature sensors, e.g. for power transformer monitoring or magnetic resonance imaging applications.
Optical fiber sensors based on intensity measurement require some form of intensity referencing to avoid errors arising from parasitic losses. Known techniques of referencing such as balanced bridge, divided beam systems or two-wavelength referencing are not suitable for low-cost applications since they use relatively complicated optical components such as multiple LED sources, couplers, filters etc. In this work a novel method of referencing in an extrinsic optical fiber sensor system utilizing temperature dependence of absorption edge in a semiconductor crystal is described. The sensor system comprises a single LED source and no optical fiber junctions. The emission spectrum of an LED depends on its temperature. The reference is provided by controlling the temperature of an LED source and transmission measurements with different emission spectra. The entire process is controlled by a microprocessor unit. Performance of a sensor system is investigated and it is shown that the losses in connectors may be compensated for.
Es werden Herstellung und Charakterisierung eines faseroptischen Elementarsensors zur Temperaturmessung vorgestellt. Der Sensorkopf in Form eines Prismas aus Indiumphosphid nutzt die Temperaturabhängigkeit der Absorptionskante des Halbleitermaterials. Aufgrund der Abmessungen des Prismas im Grenzbereich von Feinmechanik zu Mikrosystemtechnik ist ein angepasstes Herstellungsverfahren notwendig.
Magnetoinductive waves propagating along a line consisting of two kinds of metamaterial elements are studied. Both elements are made up by the same metallic loop but are loaded by different capacitors resulting in different resonant frequencies. The dispersion characteristics are derived from phase and amplitude measurements for the cases when the line consists of (i) identical elements and (ii) of alternating elements. Both planar (elements in the same plane as the axis of the line) and axial (elements perpendicular to the axis of the line) configurations are investigated. It is shown that in the bi-periodic arrangement of the elements, the dispersion curves have a forward wave in the lower frequency branch and a backward wave in the upper frequency branch independent of the configuration whether it is planar or axial. Comparisons between theoretical and experimental results show good agreement.
Rare-earth iron garnet films with in-plane anisotropy grown on (111)-oriented substrates can be used as magneto-optical indicator films for visualization of magnetic leakage fields in nondestructive evaluation. The influence of Faraday rotation, Faraday ellipticity, absorption and film thickness on the performance of a magneto-optical indicator film is investigated. A new optimization method is introduced and compared with the method of contrast optimization. The theory is experimentally verified and an application example is presented.
Mechanism of subwavelength imaging with bilayered magnetic metamaterials: Theory and experiment
(2007)
We present a theoretical and experimental study of a bilayered metamaterial structure for subwavelength imaging of magnetic field. The simplest version of such a structure consists of one or two linear arrays of capacitively loaded split pipe resonators. Its subwavelength physics is governed by strongly anisotropic magnetic coupling between individual resonators and by propagation of magnetoinductive waves with wavelength much shorter than the wavelength of the electromagnetic radiation in free space. It is shown that magnetoinductive waves propagating in the lateral direction are undesirable because they spread the image. Good subwavelength imaging is achieved when, due to the strong interlayer coupling, a stop band in the vicinity of the resonant frequency appears in the dispersion characteristics. The imaging properties of the single and double lens are compared and it is shown that the double lens has a superior performance. Excellent agreement is obtained between experimental and theoretical results for the magnetic field in the image plane in the operation frequency range of 30–60 MHz. It is shown that the same mechanism is responsible for image formation using bilayered planar metamaterial structures and a design of such a lens comprising two planar layers with a total of 542 elements is provided. The conclusions are not restricted to the radio frequency region because the elements can be scaled down.
Transmission properties of magnetoinductive waves propagating in two coupled one-dimensional metamaterial arrays are studied both experimentally and theoretically for the case when one of the arrays is shifted relative to the other one. Two different kinds of resonant metamaterial elements, split-pipe and spiral resonators, are investigated in the frequency bands centred at 46.2 and 586 MHz, respectively. It is shown that within a certain frequency range close to the resonant frequencies the transmission is strongly dependent on the shift. Theoretical calculations based on the impedance matrix show good agreement with the experimental results
A theoretical and experimental study of magnetic metamaterials with unit cells containing two resonant elements is presented. The properties of these structures, consisting of split rings, are governed by strongly anisotropic magnetic coupling between individual elements. This coupling leads to propagation of slow magnetoinductive waves in the vicinity of the resonant frequency. The wavelength of magnetoinductive waves is much smaller than the free-space wavelength of the electromagnetic radiation. This opens up the possibility of manipulating the near field on a subwavelength scale. We develop a theoretical formulation for coupled chains of metamaterial elements allowing the tailoring of their guiding properties in the near field. In a comprehensive analysis modes of coupled waveguides supporting forward and/or backward waves are identified and the corresponding hybridization mechanisms for dispersion equations of magnetoinductive waves are determined. Analytical predictions are verified both experimentally and numerically on a variety of coupled waveguides. The approach can be employed for the design of near-field manipulating devices.
An experimental study of the properties of magnetoinductive waves in the presence of retardation
(2006)
Magnetoinductive (MI) waves owe their existence to the magnetic coupling between metamaterial elements. First experiments confirming the existence of MI waves were carried out on capacitively loaded loops and Swiss Rolls about three orders of magnitude smaller than the operating wavelengths (5–15 m) so that the radiation effects did not play any significant role. In the present paper MI waves are studied experimentally on various types of split ring resonators of about 1 cm diameter operating in the microwave region between 1 and 2 GHz. Our results prove that retardation has a significant effect upon the propagation of MI waves.
Resonant frequencies of a combination of split rings: Experimental, analytical and numerical study
(2005)
The resonant frequencies of five different ring resonators are measured with the aid of a network analyser within the frequency range of about 1.5 to 2.8 GHz. The resonant frequencies for those configurations are also determined from numerical calculations using the commercially available MICRO-STRIPES package. The experimental and numerical results are shown to be very close to each other. Analytical results from various authors, available for three of the configurations, are also compared with the experimental results; one of them leads to a large discrepancy, but the other analytical approximations are shown to be not too far off.
Effect of disorder on the conductivity of two-phase strongly inhomogeneous highly filled composites
(2005)
The effect of the “stir” of a structure (small deviations from strict periodicity) on effective conductivity is considered. For determinate and random deviations, concentration and field dependences of the effective conductivity are found. Numerical experiments with determinate deviations are carried out for the cases of linear (with respect to the field) inclusions embedded in both a linear and nonlinear matrix. The numerical results are compared with the effective conductivity calculated analytically.
In an Enterprise Resource Planning (ERP) system, production planning is influenced by a variety of parameters. Previous investigations show that setting parameter values is highly relevant to a company’s target system. Parameter settings should be checked and adjusted, e.g., after a change in environmental factors, by material planners. In practice, updating the parameters is difficult due to several reasons. This paper presents a simulation-based decision support system, which helps material planners in all stages of decision-making processes. It will present the system prototype’s user interface and the results of applying the system to a case study.
We study experimentally and theoretically coupling mechanisms between metamaterial elements of the split ring resonator (SRR) type. We show that, depending on the orientation of the elements relative to each other, the coupling may be either of magnetic or electric type or a combination of both. Experimental results on SRRs with resonances around 1.7–1.9 GHz agree quantitatively with results of simulations (CST Microwave Studio). Further simulations provide analysis for a variety of SRRs both in the GHz and in the 20 THz frequency regions. The variety of coupling mechanisms can be employed in designing near field manipulating devices based on propagation of slow waves.
This paper proposes two stochastic programming models for master production scheduling with capacity-load factor scenarios. In contrast to other work on production planning with load-dependent lead times or dynamic capacity loads, we iteratively build a set of realistic capacity-load factor scenarios by simulating the realization of the master production schedules in a rolling horizon environment. Therefore, we integrate the models into a hierarchical production planning and control system that is common in industrial practice and measure the effective capacity-load factors. With these factors, we resolve the master production scheduling problem. Toa evaluate the performance of the proposed models, we compare the stochastic models with the common approach to reduce the nominally available capacity for master production scheduling. In our experiments, the stochastic models significantly reduce the tardiness of production orders caused by capacity bottlenecks.
Adaptive surface microstructures are used extensively in nature to control various surface properties such as wettability, adhesion, self-cleaning, drag reduction, etc. Regulation of these properties can be achieved with the appropriate employment of a multitude of smart materials, whose characteristics/response can be controlled by noncontact stimuli, e.g., light, heat, or magnetic field. One of the very promising magneto-regulable smart materials are magnetoactive elastomers (MAEs). They are comprised of a compliant polymer matrix with embedded micrometer-sized ferromagnetic particles. The particles interact with each other and a magnetic field. This results in remarkable tunability of the physical properties of MAEs. This paper reports a fast, resilient, and tailored method for direct surface micromachining of MAEs that enables micro-structuring without mechanical contact between the tool and the material, bypassing the usual constraints of conventional fabrication methods. It is shown that it is possible to fabricate a large variety of different microstructure geometries whose precision is limited predominantly by the size of magnetic particles. Lamellar structures with a high aspect ratio (up to 6:1) oriented either perpendicularly to the surface, can be strongly bent by applying magnetic fields in the range of 0–250 mT.
The characteristics of both direct and converse magnetoelectric (ME) interactions in bilayer composite structures comprising layers of a commercially available magnetostrictive permendur CoFe alloy and different piezoelectric PZT ceramics are investigated in detail by the method of harmonic field modulation. It is shown that, given the optimum DC magnetic bias field, a high piezomagnetic coefficient in the alloy leads to increased efficiency of ME interactions. The resonant behavior of frequency dependencies of the magnetoelectric voltage is explained by excitation of bending and planar mechanical oscillations in the structures. The results are of interest for developing highly sensitive AC magnetic field sensors and magnetoelectric transducers for energy harvesting from mechanical vibrations.
Resonant frequencies of a split-ring resonator: Analytical solutions and numerical simulations
(2004)
A set of differential equations describing the current andvoltage distribution in a split-ring resonator is derived and solved ana-lytically. The resonant frequencies may be obtained from the solution of a characteristic equation. An approximate solution for the lowest reso-nant frequency agrees with that obtained by heuristic arguments. The analytical results are supported by numerical simulations
An equivalent circuit, consisting of bulk and distributed elements, is derived for describing the properties of a potential metamaterial element capable of providing negative effective permeability. It is the singly split double ring (SSDR), a special case of the split ring resonator (J. B. Pendry et al., IEEE Trans. Microwave Theory Tech. 47, 2075 (1999)), obtained when the gap capacitance in the inner ring is infinitely large. The variables are the inter-ring voltage and the currents flowing in the inner and outer rings. The excitation is assumed in the form of a spatially constant temporally varying magnetic field. The functions, showing the angular variation of the variables, are found by solving a set of differential equations with boundary conditions imposed at the position of the split. It is shown from the analytical solution that the SSDR can have resonant frequencies in the full spectrum from very low to very high frequencies. It is pointed out in particular that whenever the mean diameter of the ring is equal to an odd multiple of the half wavelength it is always possible to find a set of parameters which will give rise to resonance. As examples the resonant frequencies are determined for eight sets of parameters. Results are also derived by replacing the distributed circuit with a number of discrete circuits. It is finally shown that the results obtained from the equivalent circuit model are in excellent agreement with those derived from the MICRO-STRIPES numerical package which solves Maxwell’s equations in the time domain.
Produktionswirtschaft
(2022)
Dieses Buch bietet eine einsteigerfreundliche Einführung in die für industrielle Betriebe maßgebliche Aufgabe der Produktionswirtschaft. Im Zentrum steht dabei das operative Produktionsmanagement. Hierzu gehören die erfolgswirksame Bewirtschaftung der Produktionsfaktoren Mensch, Betriebsmittel und Material, der Einsatz von Information sowie die Planung und Steuerung der industriellen Produktion. Mithilfe zahlreicher Unternehmensbeispiele und Übungsaufgaben wird der Leser durch produktionswirtschaftliche Grundlagen sowie durch Ablauf und Inhalt zentraler Prozesse in der Industrie geleitet. Auch die aktuelle Diskussion um das Thema Industrie 4.0 und cyber-physische Produktionssysteme werden lesefreundlich und mit konkretem Anwendungsbezug präsentiert.
Transmission spectra of wet human teeth and dentin slices, together with blood of different flow rates were investigated over a wide spectral range, from visible to terahertz (THz) light. The results make it possible to find the optimum light frequency for an all-optical determination of pulpal blood flow and, consequently, for clinically diagnosis of tooth vitality.
The Trilopede
(2012)
19F Gas Flow Measurement of C3F7H During Constant Flow and High Frequency Oscillatory Ventilation
(2013)
The aim of the current study is the development of MRI methods that enable the investigation of gas flow mechanisms during high frequency oscillatory ventilation. This work includes flow measurements during three constant flows (19.9, 30.6 and 41.4 L min-1) and the comparison to direct numerical simulations (DNS) using a second-order-acurate finite-volume method and to data measured with a volume flow meter. 19F-MRI, DNS and flow meter data are in good agreement. Flow measurements during HFOV of 4 Hz were successfully performed and velocity profiles could be recorded at different phases of the ventilation cycle.
Mechanical properties of biological tissue represent important diagnostic information and are of histological relevance (hard lesions, "nodes" in organs: tumors; calcifications in vessels: arteriosclerosis). The problem is, that such information is usually obtained by digital palpation only, which is limited with respect to sensitivity. It requires intuitive assessment and does not allow quantitative documentation. A suitable sensor is required for quantitative detection of mechanical tissue properties. On the other hand, there is also some need for a realistic mechanical display of those tissue properties. Suitable actuator arrays with high spatial resolution and real-time capabilities are required operating in a haptic sensor actuator system with different applications. The sensor system uses real time ultrasonic elastography whereas the tactile actuator is based on electrorheological fluids. Due to their small size the actuator array elements have to be manufactured by micro-mechanical production methods. In order to supply the actuator elements with individual high voltages a sophisticated switching and control concept have been designed. This haptic system has the potential of inducing real time substantial forces, using a compact lightweight mechanism which can be applied to numerous areas including intraoperative navigation, telemedicine, teaching, space and telecommunication.
Robotergreifer
(2004)
Manual tasks in industrial production are often monotonous, leading to a decrease in concentration and motivation of the worker and thus to deficiencies in the products. With quality as well as performance requirements getting more and more stringent, workers need additional support by their work environment. We developed a novel approach providing worker assistance and inline quality assurance for manual workplaces. The prototypical system Smart Workbench (SWoB) uses a multimodal sensor interface consisting of a 3D depth sensor in combination with a 2D camera to control quality aspects of the product and track the work progress. The bidirectional flow of information is handled via an image processing driven gestural interface and the displaying of advice directly on the work surface. In this paper the developed system is introduced and the current state of evaluating its industrial usage with a manual quality control and packaging task reported.
Transmission spectra of wet human teeth and dentin slices, together with blood of different flow rates were investigated. The measurements carried out over a wide spectral range, from visible light down to terahertz radiation. The results make it possible to find the optimum light frequency for an all-optical determination of pulpal blood flow and, consequently, for clinically diagnosis of tooth vitality.
A solution methodology is introduced for the efficient computation of the acoustic field over restricted domains and for a frequency window. Typically, such partial field solutions include, for example, surfaces enclosing the radiating structure or even single points in the computational domain. The multiple-frequency partial-field (MFPF) method starts out by reformulating the finite element matrix system into a suitable shifted form. The DtN map is used as a radiation boundary condition and is interpreted as a low rank update of the matrix problem. The shifted standard form is then approximated by a rational matrix-valued Padé approximant and solved simultaneously over a frequency range. To obtain the Padé approximation, a banded unsymmetric Lanczos process is applied on the standard shifted form exploiting the matrix Padé-via-Lanczos connection. Numerical examples show the feasibility of the outlined procedure.
Heutzutage werden Strukturen häufig aufwendig konstruiert und nachträglich mithilfe von numerischen Verfahren optimiert. Dennoch kommt es zu erheblichen Schäden infolge von Ermüdungsbrüchen bei wechselnd beanspruchten Bauteilen. Ein Großteil dieser Schäden hat den Ursprung in den im Inneren herrschenden Spannungszuständen, den sogenannten Eigenspannungen.
Diese Eigenspannungen heben sich innerhalb des Bauteils auf und führen zu keiner Formabweichung des Bauteils, weswegen diese Spannungen in Form und Lage nur schwer detektierbar sind und sich häufig negativ auf die Betriebsfestigkeit von Strukturen auswirken.
Mithilfe neuartiger numerischer Methoden können thermomechanische Simulationen angefertigt und Verformungen, sowie Spannungszustände abgeleitet werden. Durch diese Optionen ergeben sich neue Anwendungen, die das Potenzial von Fertigungsverfahren in Hinblick auf die Ausnutzung spezieller Eigenschaften neu eröffnen. Durch die geschickte Anwendung und Vernetzung der Simulation mit der Fertigung können Eigenspannungen gezielt in Lage und Richtung schon während der Produktion des Bauteils eingebracht werden. Im theoretischen Vergleich zu konventionell gefertigten Bauteilen entstehen Strukturen, die hinsichtlich ihrer Bauteillebensdauer optimiert sind.
Der vorliegende Artikel skizziert die neu entwickelte Prozesskette für detailgenaue Rekonstruktion von Geometrien anhand medizinischer Bilddaten sowie die Herstellung von transparenten Modellen für experimentelle Untersuchungen mit bildgebenden Strömungsmessverfahren. Die Geometriedaten und Modelle werden für systematische Untersuchungen der komplexen Transportvorgänge in den Atemwegen bei künstlicher Beatmung mittels Hochfrequenzoszillationsventilation (HFOV) verwendet.
Comprehensive experimental and numerical parameter studies on the impact of isolated vortex generator pairs and complex vortex generator arrays onto a strong shock-/boundary layer interaction are presented within the context of this thesis. The effects of vortices, especially as they interact with each other are discussed in terms of their impact on the boundary layer development, the shock characteristics and the overall aerodynamic performance of the aerofoil. The presented results have been obtained from wind tunnel experiments with a simple flat plate with superimposed pressure gradient as well as with a more comprehensive model of a supercritical transonic aerofoil. In addition complex numerical parameter studies on a supercritical aerofoil in free stream conditions have been conducted. This work is designed for gaining a better understanding of the fundamental mechanisms of vortex generator/shock/boundary-layer interaction in order to achieve improved flight performance in terms of drag reduction, avoidance or at least postponement of separation onset and shock oscillation as well as lift improvement by application of optimised vortex generator configurations.
Im Rahmen dieser Arbeit werden experimentelle und numerische Parameterstudien von einzelnen Wirbelgeneratorpaaren und komplexeren Wirbelgeneratoranordnungen bezüglich ihres Einflusses auf eine starke Stoß-/Grenzschicht-Wechselwirkung vorgestellt. Dabei werden die Einflüsse von Wirbeln, insbesondere die Auswirkungen ihrer Wechselwirkungen untereinander, auf das Grenzschichtverhalten, die Stoßcharakteristik und insgesamt auf die aerodynamische Leistung des betrachteten Profils diskutiert. Dazu wurden sowohl Windkanalversuche am einfachen Modell einer ebenen Platte mit aufgeprägtem Druckgradienten sowie an einem Modell eines superkritischen transsonischen Profils durchgeführt. Ergänzend wurden komplexe nume-rische Parameteruntersuchungen an einem Profil in freier Anströmung ausgeführt. Es ist das Ziel, ein besse-res Verständnis der Mechanismen der Wirbelgenerator-/Stoß-/Grenzschicht-Wechselwirkung zu gewinnen, um durch optimierte Anwendung von Wirbelgeneratoren eine Verbesserung der Flugleistungen erzielen zu können. Die Schwerpunkte liegen dabei auf der Reduktion des Widerstandes, der Vermeidung bzw. Verzöge-rung von Strömungsablösung und Stoßschwingung sowie auf der Erhöhung des Auftriebs.
The finite element simulation program COMSOL Multiphysics® was used to simulate the emission efficiency of a silicon tip electron source in triode configuration for different geometries and electrode potentials. The simulation predicts a maximum emission efficiency of 84% for an optimized structure. In a second simulation a gate electrode was concentrically arranged above a single CNT column. Here, the efficiency was simulated as a function of gate hole geometry, electrode potentials and distances between the electrodes. The simulation shows that a conical shape of the gate hole results in an efficiency up to nearly 100%.
The study on electrical properties for both 2,3,7,8,12,13,17,18-octaethyl-21,23H-porphine Cu (II) (Cu-porphyrin) and 2,3,7,8,12,13,17,18-octaethyl-21,23H-porphine (porphyrin) thin film, which were fabricated using spin coating method was conducted. Porphyrins were diluted with chloroform of various concentrations (0.05 mg/ml, 0.1 mg/ml, 0.5 mg/ml, 2.0 mg/ml and 3.0 mg/ml). The solution was spin coated on top of glass substrates. A layer of aluminum was evaporated on top of the organic thin film through thermal evaporation and shadow mask was placed on top of the organic thin film where two electrodes with a gap of 50 μm were formed. Surface morphology of the organic thin film was observed by scanning electron microscope (SEM) and profilometer. Different concentrations of organic solutions greatly affected the molecular packing and arrangement order of the organic thin film and thickness of the organic layer and eventually affected electrical properties of the devices.
Early meta-level: deeper understanding of connectivity-states and consequences for state definition
(2015)
The electron current from field-emitting B-doped Si-tip arrays under illumination was studied. An improved cathode design with a patch of 271 tips yielded a reproducible cathode current between 0.2-2000 nA in the electric field range of 3.8-6.6 V/μm. The plateau in the Fowler-Nordheim plot shows the actual carrier depletion and leads to a very stable emission at ~1 μA with a current noise of less than 3.3 %. Color-filtered halogen lamp illumination was used to investigate the photo-sensitivity of the saturation current. The intensity-normalized current switching ratio increases nonlinearly with the photon energy. This hints either for secondary generation in the conduction band or deeper valence band excitation. The first is supported by a rough estimation of the quantum efficiency. Further experiments with a tunable laser and electron spectroscopy are planned.
The influence of laser illumination on the integral as well as on the energy-resolved electron currents from well-defined p-doped Si-tip arrays was investigated. First results have provided stable cathode currents between 100 nA and 500 μA in a field range of 2-20 V/μm. Green laser illumination resulted in an enhanced cathode current and an increased population of the conduction band which can be seen in the spectra. Charging of the cathode surface, however, leads to a shift and broadening of the spectra which complicate their analysis. Therefore, further experiments with a rotatable cathode and a varying number of tips as well as with a tunable laser are planned.
A micromachined process to assemble homogeneous and reproducible tip arrays for field emission applications is developed and characterized. As substrate material p- as well as n-doped silicon is used. Lateral position of the tips is defined by structuring silicon dioxide to discs in a photolithographic process. Vertical structure of the tips is defined by a combination of RIE dry etching with controlled anisotropy and thermally oxidization of silicon in order to sharpen the tips. Hence field emitter arrays (FEAs) can be assembled both as bare and coated cathodes. To assemble field emission diodes, this fabrication process allows placing a metal anode in a micrometer order distance to the tips by a self-aligning procedure. The anode is placed in an evaporation process whereupon sharpening oxide is used as isolator between anode and cathode. Electrical characterization of the cathodes showed very good homogeneity, well alignment and stability over time of emission current from all tips (i.e. 100% efficiency).
The performance of free electron lasers depends on the brilliance of the electron source. Nowadays photo-cathodes (e.g. Cs2Te) are used despite of their high emittance. To develop robust and more brilliant cathodes we have built up an UHV system which enables systematic photoemission (PE) measurements with a tunable pulsed laser (hv) at high electric fields (E). First results on Au and Ag crystals revealed only low quantum efficiency (QE) due to fast electron relaxation. Hence, we have started QE(hv,E) investigations on n- and p-Si wafers. Resonant PE was observed above as well as below the work function O, which can be assigned to optical transitions in the electronic band structure or explained by thermally excited states at the bottom of the conduction band. As expected, only low QE values were achieved even for n-Si probably due to surface oxide. Moreover, a significant rise of the QE peaks above O were obtained for n-Si at E >8 MV/m but limited by the occurrence of parasitic field emission from dust particles.
Vortex-Generator Pairs for Vortex-Induced Heat-Transfer Enhancement in Heat-Exchanger Channels
(2010)
The objective of the presented work is to investigate possibilities for increasing the heattransfer in heat-exchanger channels for aircraft applications by using flow-manipulating devices. Focal point of the investigation are different arrangements of vortex-generator pairs within a generic heat-exchanger channel. The DLR URANS CFD solver THETA has been used to carry out numerical simulations of the laminar flow within a rectangular channel with integrated vortex generators. In particular, the analysis of the interaction of generated vortices with the stratified thermal boundary layer, the impact of vortical flow structures on heated walls and the enforced mixed-convection flow is of special interest. The final goal is the evaluation of the applicability of oppositely arranged vortex-generator pairs for the enhancement of vortex-induced heat-transfer.
Efficient and reliable field emission from silicon tip arrays for miniaturized electron sources
(2011)
Silicon-based cathodes with precisely aligned field emitter arrays (FEA) applicable for miniaturized electron sources were successfully developed and fabricated. The cathode chips contain about 3×105 Si tips/cm2 in a triangular array with a tip height of 2.5 μm, tip radius of 20 nm, and lateral distance between tips of 20 μm. Amazingly homogeneous and well-aligned field emission (FE) from all tips (i.e. 100% efficiency) and maximum stable currents of typically 0.1 μA for p- and 0.6 μA for n-type Si were reproducibly achieved. Current-voltage characteristics of p-type Si tips exhibit the expected saturation at around 10 nA due to limited supply of electrons from a depletion layer, while the n-type Si tips show the usual FN behaviour. Additional coating of the Si tips with a 10 nm Au layer resulted in at least 5 times higher average FE current levels i.e. typically 3 μA but lead, however, to a 30% increase of the onset voltage.
We report on the design, fabrication and characterization of p-type silicon field emitter arrays for the application in compact fast switchable electron sources. Since standard silicon technology has been used to prepare the devices, they can be easily integrated with other silicon based sensors and electronic components, too. The emitter arrays consist of approx. 3×105 tips per cm2, with a tip radius less than 20 nm. By using self-aligned processes, an integrated gate electrode with a diameter of 3 μm was placed concentrically around the tips. A mesh of silicon-beams with a grating period of 100 μm and beam width of 20 μm forms the anode of the electron source. A glass wafer (thickness 300 μm) acts as spacer between anode and Si-tip cathode. Characterization of the field emission properties of the emitter arrays was performed by high resolution field emission scanning microscopy. The emitter arrays exhibit a highly stable and very homogeneous emission. A maximum stable current of 0.1 μA per tip was found. A saturation level in the voltage current characteristics, which was found at around 10 nA, supports current stabilisation and will enable optical modulation of the emission current.
We have fabricated a test chip with various hexagonal arrays of B-doped Si tips (height ~ 3 μm, apex radius <; 30 nm, number 1-4447, resistivity 4 Ωcm, 100 orientation) in triangular arrangement (pitch 10 μm, density 1.16×10 6 cm -2 ) in order to systematically investigate the field emission current scaling with the number N of tips. Regulated voltage scans for 1 nA revealed rather efficient emission from nearly all tips of the arrays at an average field of 15 V/μm. The expected current plateau was always obtained at fields around 20 V/μm, but its width strongly increased with N. In this carrier depletion range, the single tip provided a much higher stability (<; 5%) of the current (2-3 nA) than at lower (>; 50 %) and higher currents (>; 30%). Integral current measurements of the hexagonal arrays resulted in a statistically improved current stability (<; 1%) but only a weak increase of the total current with N 0.28 yet. These results will be discussed with respect to the remaining inhomogeneity of the tips.
In order to optimize our field-emitting silicon structures, the influence of geometric parameters like aspect ratio, aperture angle and curvature on the field enhancement factor was investigated by finite element simulations. A universal geometric model consisting of a rounded triangle and elliptic curvatures was taken for modeling a variety of different silicon tip as well as ridge structures. Whereas, a high dependency of the field enhancement on the aperture angle was found, the simulations show that the elliptic curvature affects the field enhancement only marginal.
Mechanical cues such as extracellular matrix stiffness and movement have a major impact on cell differentiation and function. To replicate these biological features in vitro, soft substrata with tunable elasticity and the possibility for controlled surface translocation are desirable. Here we report on the use of ultra-soft (Young’s modulus <100 kPa) PDMS-based magnetoactive elastomers (MAE) as suitable cell culture substrata. Soft non-viscous PDMS (<18 kPa) is produced using a modified extended crosslinker. MAEs are generated by embedding magnetic microparticles into a soft PDMS matrix. Both substrata yield an elasticity-dependent (14 vs. 100 kPa) modulation of α-smooth muscle actin expression in primary human fibroblasts. To allow for static or dynamic control of MAE material properties, we devise low magnetic field (≈40 mT) stimulation systems compatible with cell-culture environments. Magnetic field-instigated stiffening (14 to 200 kPa) of soft MAE enhances the spreading of primary human fibroblasts and decreases PAX-7 transcription in human mesenchymal stem cells. Pulsatile MAE movements are generated using oscillating magnetic fields and are well tolerated by adherent human fibroblasts. This MAE system provides spatial and temporal control of substratum material characteristics and permits novel designs when used as dynamic cell culture substrata or cell culture-coated actuator in tissue engineering applications or biomedical devices.
Mechanical properties of biological tissue represent important diagnostic information and are of histological and pathological relevance. Malignant tumors are significantly stiffer and more immobile than surrounding healthy tissue. Hard calcifications in vessels occur due to arteriosclerosis. The problem is, that such information is usually not available or can only be obtained by manual palpation, which is subjective and limited in sensitivity. It requires intuitive assessment and does not allow quantitative documentation. Unfortunately, none of the established medical imaging equipment such as magnetic resonance imaging (MRI) or X-ray computed tomography (CT) can provide direct measure of tissue elasticity. On the one hand a suitable sensor is required for quantitative measurement of mechanical tissue properties. On the other hand there is also some need for a realistic haptic display of such tissue properties. Suitable actuator arrays with high spatial resolution acting in real time are required. A haptic sensor actuator system is presented in this paper including a sensitive sensor part and an actuator array for different applications. The mechanical consistency of an object is to be locally specified using a sensor system and represented perceptibly in a remote position on an actuator system for the user. The sensor system uses ultrasound (US) elastography, whereas the actuator array is based on electrorheological (ER) fluids.
Reduction of femoral shaft fractures in vitro by a new developed reduction robot system "RepoRobo"
(2004)
Closed reduction of the long bones is associated with the use of
considerable force. This force must be maintained for the reduction maneuver and fixation process. At present, apart from the extension table or the large AO distractor, only rather inadequate reduction aids are available. A solution to this problem is being sought in the form of a robotic system with which precision can be improved and the holding effort reduced. In the research project presented here, a synthetic femur with integrated tensioned mainspring and a 32-A3 type
fracture served as a bone reduction model. The fracture was stabilized with a standard AO fixator. A Stäubli robot (model RX130) was converted by appropriate modification so that it could be used for the reduction of femoral shaft fractures in vitro. The robot was equipped with a pneumatic 2-fingered gripper, on which the fingers have
been modified so that they can grip the AO fixator clamp. A Force-Feedback-Sensor was inserted between the gripper and the robot to obtain online recordings of the forces and moments in all three axes. With this setup it is possible to achieve precise reduction of the fracture in all planes under visual control.
Silicon-based cathodes with precisely aligned field emitter arrays of sharp tips applicable for miniaturized electron sources were successfully fabricated and characterized. This was made possible by an improved fabrication process using wet thermal oxidation, wet etching, and reactive-ion etching steps with adjustable anisotropy. As substrate materials, both p-doped silicon and n-doped silicon were used. The cathode chips contain about 3 × 10 5 Si tips/cm 2 in a triangular array with tip heights of 2.5 μm, tip radii of less than 30 nm, and spacing of 20 μm. Well-aligned field emission (FE) and excellent homogeneity from all tips (i.e., 100% efficiency) and maximum stable currents of typically 0.1 μA (0.6 μA) for p (n)-type Si were reproducibly achieved. The current-voltage characteristics of the p-Si tips exhibit the expected saturation at around 10 nA with around ten times better current stability, whereas the n-Si tips show the usual Fowler-Nordheim behavior. Additional coating of the Si tips with 5-nm Cr and 10-nm Au layers resulted in improved stability and at least five times higher average FE current limits (about 3 μA) at about 30% higher operation voltage.
The homogeneity of emitters is very important for the performance of field emission (FE) devices. Reactive-ion etching (RIE) and oxidation have significant influences on the geometry of silicon tips. The RIE influences mainly the anisotropy of the emitters. Pressure has a strong impact on the anisotropic factor. Reducing the pressure results in a higher anisotropy, but the etch rate is also lower. A longer time of etching compensates this effect. Furthermore an improvement of homogeneity was observed. The impact of uprating is quite low for the anisotropic factor, but significant for the homogeneity. At low power the height and undercut of the emitters are more constant over the whole wafer. The oxidation itself is very homogeneous and has no observable effect on further variation of the homogeneity. This modified fabrication process allows solving the problem of inhomogeneity of previous field emission arrays.
In this paper, we study the effect of skill-biased technological change on unemployment and wage inequality in the presence of a link between social benefits and average income. In this case, an increase in the productivity of skilled workers and hence their wage leads to an increase in average income and hence in benefits. The increased fallback income, in turn, makes unskilled workers ask for higher wages. As higher wages are not justified by respective productivity increases, unemployment rises. More generally, we show that skill-biased technological change leads to increasing unemployment of the unskilled and to a moderately increasing wage inequality when benefits are endogenous. The model provides a theoretical explanation for diverging dynamics in wage inequality and unemployment under different social benefits regimes: Analyzing the social legislation in 14 countries, we find that benefits are linked to the evolution of average income in Continental Europe but not in the U.S. and the UK. Given this institutional difference, our model predicts that skill-biased technological change leads to rising unemployment in Continental Europe and rising wage inequality in the U.S. and the UK....
This paper addresses the efficient solution of acoustic problems in which the primary interest is obtaining the solution only on restricted portions of the domain but over a wide range of frequencies. The exterior acoustics boundary value problem is approximated using the finite element method in combination with the Dirichlet-to-Neumann (DtN) map. The restriction domain problem is formally posed in transfer function form based on the finite element solution. In order to obtain the solution over a range of frequencies, a matrix-valued Padé approximation of the transfer function is employed, using a two-sided block Lanczos algorithm. This approach provides a stable and efficient representation of the Padé approximation. In order to apply the algorithm, it is necessary to reformulate the transfer function due to the frequency dependency in the nonreflecting boundary condition. This is illustrated for the case of the DtN boundary condition, but there is no restriction on the approach which can also be applied to other radiation boundary conditions. Numerical tests confirm that the approach offers significant computational speed-up.
A Krylov subspace projection method which provides simultaneous solutions of the Helmholtz equation at multiple frequencies in one solution step is presented. The projector is obtained with an unsymmetric block Lanczos algorithm applied to a transfer function derived from a finite element discretization. This approach is equivalent to a matrix-valued Padé approximation of the transfer function. The proposed method is an extension of the formulation presented in [J. Comput. Acoust. 8 (2000) 223] to unsymmetric systems and allows the treatment of a much wider range of practical problems, including near-field and fluid–structure interaction computations
Aerospace and automotive industries employ three main techniques to set up joints between metal and fibre reinforced plastics parts (FRP); adhesive bonding, mechanical fastening with rives/bolts and a hybrid combination. A new joint technique has been developed to combine the two advantageous mechanisms form-closure and adhesion in a fibre-friendly way. Prior is established through metal structures (pins) which are perpendicularly welded onto metal surfaces with an arc-welding-process. They intrude into the FRP during lay-up and therefore set up a first connection. The composite-matrix is responsible for latter adhesive bonding and final form closure. Finite-element-analyses of cylindrically shaped joints are carried out to get detailed knowledge of the influence of parameters like pin-number, pin-position, pin-height, pin-form sleeve-geometry, and stiffness behaviour. Long calculation times of 3D-models lead to the introduction of a corresponding 2D-axisymmetric-model which is used to run parameter-studies within a reasonable time. For this novel technique the combination of fibre-friendly form closure and adhesive bonding of interface plays a major role. A well selected amount of vertical reinforcements, their placement and geometrical dimensions will lead to a stiffer joint. Goal is to minimize fibre-deletion and overlap length to improve load-transfer and joint-strength, to reduce weight in high-strength-applications as well as the avoidance of safety rivets.
The high surface to volume ratio of nanoparticles allows a detailed experimental study of the surface phenomena associated with solid bridging. Besides bulk analyses, the local view on the structure and composition via HRTEM is particularly essential. 50 nm core shell particles consisting of a silicon (Si) core and a SiO2 shell were used as model system to understand surface phenomena appearing for Si-based nanostructures. Evaporative drying from de-ionized water shows the most significant bridging effect based on SiO2. There is only a localized deposition of oxides between the particles during the drying process and no overall oxidation. For the deposition material, silicates are the most likely candidates.
Piezoelectric actuators are well established for use in expensive optical equipment. Within the last decade, relatively inexpensive piezoelectric actuators have become established technology in pneumatic switching and the first piezoelectrically driven impactive robot grippers are just starting to emerge. Although this article concentrates largely on the use of piezoelectric actuators for use in robot gripping systems, the potential for applications outside this field is immense.
Shape memory materials fulfill an important role in both actuation and mechanical coupling between actuators and associated dynamic systems. The simplest techniques are thermally based and in addition to the more common shape memory alloys there are also shape memory polymers. These have similar characteristics to those of their metallic cousins, but there the relationship stops. The basic physical principles are very different and this paper attempts to outline the current state-of-the-art to those already involved with the technology and perhaps open a fresh chapter in smart materials to those who are new to it.
This paper reports the first step in the development of a tactile array suitable for the presentation of haptic information in virtual reality. The system is based on the electric field dependence of the viscosity of electrorheological fluids. The simulation, as well as the experimental realization of single tactels is described. The mathematical approach is based on the Eckart model (Eckart W 2000 Continuum Mech. Thermodyn. 12 341–62) and its validity is demonstrated by comparing the resulting yield stress with the experimental results from Wunderlich (2000 Dissertation Universität Erlangen-Nürnberg). Two different tactel designs are realized and the experimental results are compared with numerical simulation. The design of modification B is shown to be applicable for the realization of an actuator array with high spatial resolution.
The performance of thermal conductivity vacuum gauges can be improved by a well-designed geometry. The lower measurement range limit is determined by the size of the active sensing area and the thermal conduction heat losses through the supporting structures. The upper measurement range is limited by the distance between the heated element and the cold reference plane. Silicon based MEMS-technology gives the possibility to fabricate both sensing structures with suitable areas out of low thermal conductive materials and narrow gaps in order to extend the measurement range in both directions. In this work we present a MEMS-process to fabricate high thermal resistance sensor structures. The rectangular sensitive areas are anchored by four beams and are structured out of low thermal conductive PECVD-siliconnitride films with 1 µm in thickness. The metallic heating structure is completely embedded in the SiN-layer. Both sensitive area and its support beams were released from the silicon bulk material by anisotropic underetching. In this way a free-supporting structure with a gap of 150 μm to the silicon substrate was formed. The influence of the filament geometry and temperature was systematically investigated to determine the properties of the chips as thermal conductivity vacuum gauges. The temperature of the sensitive area was held constant by a self-balancing bridge circuit and the heating power was measured by a Δ-Σ-ADC. The average solid state thermal conductivity is in the order of 106WK1. The measuring range of the most sensitive structures covers 8 orders of magnitude from 105 mbar to 1000mbar.
We report on the field emission properties of GaN LED surfaces. The textured extraction facet acts both as light scattering layer in order to increase the light extraction efficiency of the LED as well as nanostructured cathode surface for the field emission (FE) of electrons. The LED emits blue light with a peak wavelength of around 450 nm. The FE properties were investigated by a scanning microscope. Integral measurements as well as regulated voltage scans for 1 nA FE current over an area of 400 * 400 µm2were used to investigate both overall and local FE properties. A high number of well-distributed emitters with an average field enhancement factor ß of 85 and stable integral emission currents up to 100 µA at an electric field of 80 V/µm (Øanode= 880 µm) were found. Photo-field-emission spectroscopy (PFES) using a tunable pulsed laser revealed an enhanced photo absorption of the InGaN/GaN quantum well structures near the emission wavelength of the LED (<3.5 eV), whereas at high photon energies (>4.1 eV) photoemission from the GaN surface was observed.
In order to improve the uniformity and field emission stability of p-type silicon tip arrays for pulsed sensor applications, we have systematically studied the influence of the fabrication parameters on the tip shape and the specific operating conditions. Based on detailed design calculations of the field enhancement, we have fabricated a series of hexagonal arrays of B-doped Si-tips in a triangular arrangement, each containing a different number of tips (91, 575 and 1300) of 1 μm height, 20 nm apex radius, and 20 μm pitch. The field emission properties of both individual tips and complete arrays were investigated with by field emission scanning microscopy. The current plateaus of these tips typically occur at about 10 nA and 60 V/μm field level. In this carrier depletion range, single tips provide the highest current stability (<; 4%) and optical current switching ratios of ~2.5. Rather homogeneous emission of the tip arrays leads to an almost linear scaling of the saturation current (2 nA/tip) and to a much improved current stability (<; 1%) measured over 1 hour.
Flame sprayed Al-12Si coatings for the improvement of the adhesion of composite casting profiles
(2008)
In this study, flame sprayed Al-12Si coatings were produced on the surface of inlays (aluminum profiles) of composite castings parts. The aim was to enhance the strength between the joining partners inlay and cast. Due to the high surface roughness and the presence of pores in the coatings, combined with the formation of an intermetallic phase at the interface, the adhesion of flame sprayed inlays could be enhanced by a factor of 2 compared to blank inlays and by a factor of 1.3 when compared to sand-blasted inlays. However, results also show that gaps are present, mostly at the interface between the inlays and the flame sprayed coatings, and these gaps have a negative effect on the joining strength of the composite casting parts. Therefore, optimizing the adhesion of the coating on the Al profiles via an improvement in both the sand-blasting and the flame spraying parameters would be beneficial for further enhancement of the adhesion of composite casting parts.
The application of robotics in manufacturing industry is increasingly spreading to other fields such as service, security and medical, and more recently into orthopedic surgery. Most research projects to date have concentrated on the lighter side of non‐invasive surgery, camera, laser guidance, light cutting and milling through bone. Just as in industrial production and processing applications, the choice of robot and its accompanying control and programming system is absolutely paramount. This simple fact has been justified in recent research dealing with the heavier forms of fracture repositioning robotics in accident surgery. This paper discusses the development of the complete system including robot, end‐effector and sensors.
The magnetoelectric response of bi- and symmetric trilayer composite structures to pulsed magnetic fields is experimentally investigated in detail. The structures comprise layers of commercially available piezoelectric (lead zirconate titanate) and magnetostrictive (permendur or nickel) materials. The magnetic-field pulses have the form of a half-wave sine function with duration of 450 µs and amplitudes ranging from 500 Oe to 38 kOe. The time dependence of the resulting voltage is presented and explained by theoretical estimations. Appearance of voltage oscillations with frequencies much larger than the reciprocal pulse length is observed for sufficiently large amplitudes (~1-10 kOe) of the magnetic-field pulse. The origin of these oscillations is the excitation of bending and planar acoustic oscillations in the structures. Dependencies of the magnetoelectric voltage coefficient on the excitation frequency and the applied magnetic field are calculated by digital signal processing and compared with those obtained by the method of harmonic field modulation. The results are of interest for developing magnetoelectric sensors of pulsed magnetic fields as well as for rapid characterization of magnetoelectric composite structures.