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The mechanical and microstructural investigation of polymer parts (polyamide 12) fabricated by Selective Laser Sintering as part of a Round Robin initiative is presented. The paper focuses on the microstructural analysis of the Round Robin samples and their evaluation regarding their effect on mechanical properties with respect to each other. Therefore optical microscopy on microtomed samples, X-ray computed tomography and Differential Scanning Calorimetry is used to determine the morphology of residual particle cores and of internal pores.
The mechanical properties of polymer parts built by Selective Laser Sintering are strongly related to the internal microstructure which differs with the applied production parameters. The paper focuses on the back tracing of the pore morphology of laser sintered polyamide-12 samples to the process parameters. Therefore, a data base is used which is supplied by a Round Robin initiative and includes mechanical tensile tests and the microstructural analysis of the pore morphology of several different sample charges built with different machines. The pore morphologies (porosity, pore density, pore shape and pore arrangement) measured by X-ray computed tomography are compared and discussed regarding the employed parameters and the resulting mechanical properties. The investigations point out that pore density is a superior indicator than porosity for mechanical issues. This is especially valid along the build direction since pore morphology has shown to be strongly anisotropic. Moreover, the analysis revealed that pore density is strongly affected by the process temperature, which is proved to be essential for the fabrication of mechanical robust parts using Selective Laser Sintering.
In this paper, the use of electrophotographic polymer powder transfer for the preparation of multi-material layers is discussed with respect to the application in powder bed-based additive manufacturing technologies as selective laser sintering (SLS). Therefore, the challenges of this task are considered verifying the critical process steps in order to develop a concept for an electrophotograhic laser sintering machine. On that basis, an experimental setup with a two-chamber design is realized which enables the investigation of the electrophotographic powder transfer at typical process conditions of SLS. Using this setup, transfer tests of polypropylene powder patterns were performed and qualitatively analyzed by photographic imaging. The results confirm the high potential of the application of electrophotography for multi-material powder deposition and show how a residual electrophotographic powder deposition can be achieved in general, which is independent from the already produced part height, in order to build up three-dimensional multi-material components.