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A new approach to coat PA12 powders with laser-generated nanoparticles for selective laser sintering
(2018)
The modification of selective laser sintering (SLS) powder materials by nanoadditives offers the possibility to adapt the powder properties to the laser sintering process or the resulting part properties. To avoid agglomeration of the nanofiller, a new approach in which surfactant-free laser-generated colloidal nanoparticles are adsorbed onto the polymer surface directly in an aqueous solution is demonstrated. Based on this novel approach, polyamide 12 (PA12) powders are decorated with metal and oxide nanoparticles and processed via SLS. Electron microscopy and confocal laser scanning imaging are utilized to analyze the dispersion of the filler.
This study increases the basic understanding of optical material properties of polymer powders used in selective laser sintering (SLS). Therefore, different polymer powder materials were analyzed regarding their optical material properties with an integration spheres measurement setup. By the measurements a direct connection between the absorption behavior of the solid material and the overall optical material characteristics of the same material in powdery form could be shown. The results were used to develop an advanced explanation model for the optical material properties of powders. At present, existing explanation models only consider the occurring of multiple reflections in the gaps between the particles to explain the overall optical material properties of powder materials. Thus, by also considering the absorption behavior of the single particles, the basic understanding of the beam-matter interaction and their effect on the optical material properties of powder materials can be expanded.
Qualification and modification of new polymer powders for laser beam melting using Ulbricht spheres
(2014)
The restricted amount of available materials for Laser Beam Melting (LBM) of polymers is one of the main limitations for expanding the technology. Current qualification methods deal with problems like inadequate powder flowability or high part porosities among others but do not offer a detailed analysis of the important beam-matter-interaction between powder particles and electro-magnetic laser radiation. In this paper, polyethylene powder is qualified for the LBM process and specifically analyzed regarding the optical material properties of the powder for a wavelength of 10.6 μm. By admixing graphite as absorption intensifier the change of the optical material properties and the thereby connected processing parameters are analyzed. Furthermore an explanation approach is given to explain the relation between different transmittances of different powder particles and the optical material properties of the polymer powders.
Conventional Selective Laser Sintering of polymers is restricted to the processing of single materials. The fabrication of components consisting of different material regions is a challenge which cannot be realized by standard coating devices basing on blades or rollers. Thus, advanced coating and deposition techniques are needed which enable the precise and reliable control over very small powder quantities in order to prepare arbitrary powder patterns with high accuracy and repeatability. In this report, the delivery of polymer powder by vibrating nozzles inside laser sintering machines is investigated. Therefore, a steel nozzle attached to a piezo actuator is integrated into a machine, whereas the nozzle itself features internal channels which allow the precise control over the powder temperature using heat transfer oil. The setup is used to study the influence of different system configurations on the powder deposition characteristics as resolution and layer surface roughness. The results show that temperature influences the mass flow depending on the material used and that a precise deposition of powder pattern with microscale resolution is possible with optimized parameters. Finally, the multimaterial powder pattern is fused by a new illumination strategy of laser sintering which is called Simultaneous Intensity-Selective Laser Sintering in order to demonstrate the potential of this new approach.