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Forschungsbericht 2016
(2016)
Purpose – The purpose of this paper is to demonstrate the processability of cohesive PE-HD particles in laser beam melting processes (LBM) of polymers. Furthermore, we present a characterization method for polymer particles, which can predict the quality of the powder deposition via LBM processes. Design/methodology/approach – This study focuses on the application of dry particle coating processes to increase flowability and bulk density of PE-HD particles. Both has been measured and afterwards validated via powder deposition of PE-HD particles in a LBM machine. Findings – For efficient coating in a dry particle coating process, the PE-HD particles and the attached nanoparticles need to show similar surface chemistry, i.e. both need to behave either hydrophobic or hydrophilic. It is demonstrated that dry particle coating is appropriate to enhance flowability and bulk density of PE-HD particles and hence considerably improves LBM processes and the resulting product quality. Originality/value – At present, in LBM processes mainly polyamide (PA), 12 particles are used, which are so far quite expensive in comparison to, for example, PE-HD particles. This work provides a unique and versatile method for nanoparticulate surface modification which may be applied to a wide variety of materials. After the coating, the particles are applicable for the LBM process. Our results provide a correlation between flowability and bulk density and the resulting product quality.
Im Rahmen dieses Beitrags wird das Schmelzeemulgieren als Verfahren zur Herstel-lung von Polymermikropartikeln vorgestellt. In diesem Prozess wird zunächst ein Polymergranulat in einer kontinuierlichen Phase in Gegenwart geeigneter Additive in einem Rührbehälter aufgeschmolzen, die Rohemulsion in einer Rotor-Stator-Einheit feinemulgiert und anschließend zu einer Suspension abgekühlt. Der Einfluss von Prozessparametern und Systemzusam-mensetzung auf das Emulgierergebnis wird diskutiert und die Anwendbarkeit des Verfahrens für polymere Mikropartikeln anhand von Polypropylen (PP) und Polyethylen (PE-HD) dargestellt. Die erhaltenen Suspensionen werden zur Überführung in Pulverform sprühgetrocknet und die Fließeigenschaften des Pulvers analysiert. Durch trockenes Beschichten mit pyrogener Kieselsäure kann die Fließfähigkeit der erhaltenen Partikeln weiter verbessert werden. Das Verfahren bietet somit einen neuen Zugang zur Herstellung neuer Ausgangsmaterialien für die Additive Fertigung.
Forschung 2019
(2019)
Forschung 2018
(2018)
In the paper first results regarding the realisation of gradient and multi-material parts manufactured by Laser Beam Melting in powder bed of metals and polymers are published. Gradient properties of additively manufactured metal parts can be achieved by varying the composition of alloying components in the powder and adapting process strategies. As an alternative to atomizing pre-alloyed materials, mixtures of different powders are investigated. For realizing multi-material-parts from polymers, at first relevant material properties concerning compatibility have to be analysed. Therefore the paper shows the main requirements for compatibility between different materials and also first results regarding the compatibility of polymer powders and possible combinations for the manufacturing of multi-material components by laser beam melting of polymers.
Neue Prozessstrategien zur Herstellung von Multi- Material-Bauteilen und Gradientenwerkstoffen
(2012)
Das additive Fertigungsverfahren, dem gemeinhin die größten Potentiale zugesprochen werden, ist das Laserstrahlschmelzen im Pulverbett von Kunststoffen (LSS-K) und von Metallen (LSS-M). Wie bei anderen Techniken der additiven Fertigung werden Bauteile direkt aus CAD-Dateien ohne zusätzliche Werkzeuge bei enormer konstruktiver Freiheit gefertigt. Die resultierenden Werkstoffeigenschaften sind vergleichbar mit konventionelleren Prozessrouten wie etwa dem Spritzgießen thermoplastischer Polymere beziehungsweise auf der Seite der Metalle dem Schmieden oder Gießen. Derzeit wird der Einsatz des LSS zur Fertigung von Endprodukten in kleinen Stückzahlen erschwert von nicht ausreichender Prozessstabilität und, insbesondere bei Kunststoffen, von der eingeschränkten Werkstoffauswahl. Bisher werden für beide Werkstoffklassen Bauteile aus jeweils einem einzigen Ausgangsmaterial hergestellt. Näherungsweise erzeugt LSS also einheitliche Materialeigenschaften über das gesamte Bauteil hinweg. Ein Ansatz, der in den Teilprojekten A5 und B6 des Sonderforschungsbereichs 814 verfolgt wird, ist die Realisierung von Multi-Material-Bauteilen mittels LSS-K beziehungsweise LSS-M.
First results regarding the realisation of multi-material components manufactured by Laser Beam Melting of polymers and metals are published. For realising composite structures from polymer powders by additive manufacturing, at first relevant material properties regarding compatibility have to be analysed. The paper shows the main requirements for compatibility between different materials and offers first results in form of a compatibility matrix of possible combinations for composite structures.For achieving gradient properties of additively manufactured metal parts by using composite materials the composition of alloying components in the powder and adapted process strategies are varied. As an alternative to atomizing pre-alloyed materials, mixtures of different powders are investigated.
The joint strength is gaining importance in quasi -simultaneous laser transmission welds, especially in structural components. A correlation between the joint strength and a process characteristic is a basic requirement for selecting the best process parameter setting. In this work, the temperature is measured during welding polyamide 6 by using a scanner-integrated pyrometer with an InGaAs-detector. The filtering of the heat radiation in the upper joining partner is taken into account by calibrating the mea surement system. By this, the measured temperature signal represents the temperature in the joining zone. A correlation is found between the measured temperature and the resulting joint strength. Moreover, high joint strengths are also seen for welds with short welding times, as far as the temperature is sufficiently high. With this knowledge, a process window can be derived easily in order to produce welds with high strength and short welding times.