@inproceedings{LangerPrommesbergerŁawrowskietal., author = {Langer, Christoph and Prommesberger, Christian and Ławrowski, Robert Damian and M{\"u}ller, F. and Schreiner, Rupert and Serbun, Pavel and M{\"u}ller, G{\"u}nter}, title = {Enhanced field emission from p-doped black silicon on pillar structures}, series = {2015 28th International Vacuum Nanoelectronics Conference (IVNC), 13-17 July 2015, Guangzhou, China}, booktitle = {2015 28th International Vacuum Nanoelectronics Conference (IVNC), 13-17 July 2015, Guangzhou, China}, publisher = {IEEE}, doi = {10.1109/IVNC.2015.7225547}, pages = {104 -- 105}, abstract = {Aligned square arrays of black silicon (b-Si) on top of pillars were fabricated on p-type silicon substrate by a deep-etching step combined with a b-Si process. Two 10×10 arrays with pillar heights of 8 μm and 20 μm and one b-Si reference sample without pillars were investigated. Integral field emission (FE) measurements of the arrays yielded rather low onset-fields between 6.4 V/μm and 13.5 V/μm and field enhancement factors between 430 and 800. The I-V curves showed typical Fowler-Nordheim behavior for low fields, whereas a saturation region was observed at higher fields. The maximum integral current in the saturation region was 8 μA at a field of 20 V/μm. The stability of the emission current was investigated over 3 hours and revealed moderate fluctuations of ± 8\% in the saturation region. Voltage scans showed well-aligned FE from nearly all pillars.}, language = {en} } @inproceedings{PrommesbergerŁawrowskiLangeretal., author = {Prommesberger, Christian and Ławrowski, Robert Damian and Langer, Christoph and Dams, Florian and Schreiner, Rupert}, title = {Realisierung von Siliziumspitzenarrays mit integrierter Gate-Elektrode f{\"u}r Anwendungen in der Vakuumsensorik}, series = {4. Landshuter Symposium Mikrosystemtechnik, Mikrosystemtechnik als Schl{\"u}sseltechnologie der Systemintegration, Tagungsband zum Symposium 12./13. M{\"a}rz 2014, Hochschule Landshut}, booktitle = {4. Landshuter Symposium Mikrosystemtechnik, Mikrosystemtechnik als Schl{\"u}sseltechnologie der Systemintegration, Tagungsband zum Symposium 12./13. M{\"a}rz 2014, Hochschule Landshut}, address = {Landshut}, isbn = {978-3-9812696-5-9}, pages = {36 -- 41}, abstract = {Bei der Feldemission (kalte Emission) k{\"o}nnen Elektronen durch ein starkes elektrisches Feld eine glatte und leitende Oberfl{\"a}che verlassen. Die Elektronen tunneln dabei durch eine Potentialbarriere, deren Breite durch ein {\"a}ußeres elektrisches Feld verkleinert wird. Durch das Hinzuf{\"u}gen einer integrierten Gate-Elektrode um eine Siliziumspitze kann die notwendige Einsatzspannung f{\"u}r Feldemission deutlich gesenkt werden. Zwischen Si-Kathode und Gate-Elektrode befindet sich dabei eine Isolationsschicht, die h{\"o}chste Anforderungen bez{\"u}glich der elektrischen Durchbruchsfestigkeit erf{\"u}llen muss. Mit einer Kombination aus Trocken- (Schichtdicke 50 nm) und Feuchtoxid (Schichtdicke 950 nm) konnte eine Isolationsschicht entwickelt werden, die im integrierten Aufbau eine minimale Durchbruchsfeldst{\"a}rke von 3,2 MV/cm aufweist. F{\"u}r die Realisierung von Siliziumkathoden mit integrierter Gate-Elektrode wurde ein bereits bestehender Herstellungsprozess um zus{\"a}tzliche Prozessschritte erweitert. Die {\"U}bertragung der lateralen Position der Spitze erfolgt durch Strukturierung des Umkehrlacks AZ5214 und einer RIE-{\"A}tzung der zuvor hergestellten SiO2-Schicht. Nach dem Entfernen der Lackschicht wird die vertikale Struktur der Siliziumspitzen durch einen RIE-{\"A}tzprozess mit den Prozessgasen SF6 und O)2 realisiert. Aus einer thermischen Oxidation bei 940 °C resultiert anschließend die Isolationsschicht zwischen Si-Kathode und Gate-Elektrode . Gleichzeitig wird diese Ansch{\"a}rfeoxidation auch zur Realisierung der endg{\"u}ltigen Spitzengeometrie verwendet. Durch die lithographische Strukturierung des Photolacks AZ5214 kann dabei die Fl{\"a}che der aufgedampften Gate-Elektrode festgelegt werden. Die Gate-Elektrode wird in einem selbstjustierenden Prozessschritt exakt konzentrisch um die Si-Spitze aufgedampft. Der gerichtete Aufdampfprozess bewirkt eine Abschattung, so dass das Oxidpl{\"a}ttchen nicht komplett von Metall ummantelt wird. Die Opferschicht aus Photolack wird mit den nicht ben{\"o}tigten Metallfl{\"a}chen in einem Lift-off-Prozess entfernt.}, language = {de} } @inproceedings{ŁawrowskiLangerPrommesbergeretal., author = {Ławrowski, Robert Damian and Langer, Christoph and Prommesberger, Christian and Dams, Florian and Serbun, Pavel and M{\"u}ller, G{\"u}nter and Schreiner, Rupert}, title = {Spitzen- und Kantenemitter aus Silizium mit einem hohen Aspektverh{\"a}ltnis f{\"u}r Ionisationsgassensoren}, series = {Mikrosystemtechnik als Schl{\"u}sseltechnologie der Systemintegration : 4. Landshuter Symposium Mikrosystemtechnik ; Tagungsband zum Symposium ; 12./13. M{\"a}rz 2014, Hochschule Landshut}, booktitle = {Mikrosystemtechnik als Schl{\"u}sseltechnologie der Systemintegration : 4. Landshuter Symposium Mikrosystemtechnik ; Tagungsband zum Symposium ; 12./13. M{\"a}rz 2014, Hochschule Landshut}, publisher = {Cluster Mikrosystemtechnik}, address = {Landshut}, isbn = {978-3-9812696-5-9}, pages = {28 -- 35}, abstract = {Durch die Optimierung von reaktivem Ionen{\"a}tzen mit induktiv gekoppeltem Plasma ist die Herstellung von verschiedenen Siliziumkathoden mit hoher Anisotropie und hohem Aspektverh{\"a}ltnis f{\"u}r Feldemissionsanwendungen m{\"o}glich. Simulationen mit COMSOL Multiphysics untermauern das Potential von solchen Spitzen- und Kantenfeldemittern. Die Ergebnisse der Simulation zeigen einen zwei- bis sechsfach h{\"o}heren Feld{\"u}berh{\"o}hungsfaktor der tiefge{\"a}tzten Strukturen im Vergleich zu identischen Emittern ohne zus{\"a}tzliche Tiefen{\"a}tzung. Feldemissionsmessungen best{\"a}tigen die Simulationsergebnisse. Der modifizierte Herstellungsprozess der Feldemitter erm{\"o}glicht somit einen zuverl{\"a}ssigen Betrieb von Feldemissionselektronenquellen bei kleineren makroskopischen Feldst{\"a}rken. Außerdem weisen die Messungen des Emissionsstroms im S{\"a}ttigungsbereich eine weitgehende Unabh{\"a}ngigkeit vom elektrischen Feld auf. Lokale Feldemissionsmessungen ergeben dadurch eine deutliche Stromstabilisierung, welche {\"u}ber große Feldst{\"a}rkenbereiche konstant bleibt. Die Nutzung der HAR-Emitter (high aspect ratio) ist damit eine gute Voraussetzung f{\"u}r einen zuverl{\"a}ssigen Betrieb der Emissionskathoden bei kleinen Feldst{\"a}rken f{\"u}r die Anwendung in Ionisationsgassensoren.}, language = {de} } @article{ŁawrowskiPrommesbergerLangeretal., author = {Ławrowski, Robert Damian and Prommesberger, Christian and Langer, Christoph and Dams, Florian and Schreiner, Rupert}, title = {Improvement of Homogeneity and Aspect Ratio of Silicon Tips for Field Emission by Reactive-Ion Etching}, series = {Advances in Materials Science and Engineering. Special issue: Advances in Smart Materials and Applications}, volume = {2014}, journal = {Advances in Materials Science and Engineering. Special issue: Advances in Smart Materials and Applications}, publisher = {Hindawi}, issn = {1687-8442}, doi = {10.1155/2014/948708}, pages = {1 -- 6}, abstract = {The homogeneity of emitters is very important for the performance of field emission (FE) devices. Reactive-ion etching (RIE) and oxidation have significant influences on the geometry of silicon tips. The RIE influences mainly the anisotropy of the emitters. Pressure has a strong impact on the anisotropic factor. Reducing the pressure results in a higher anisotropy, but the etch rate is also lower. A longer time of etching compensates this effect. Furthermore an improvement of homogeneity was observed. The impact of uprating is quite low for the anisotropic factor, but significant for the homogeneity. At low power the height and undercut of the emitters are more constant over the whole wafer. The oxidation itself is very homogeneous and has no observable effect on further variation of the homogeneity. This modified fabrication process allows solving the problem of inhomogeneity of previous field emission arrays.}, language = {en} } @inproceedings{ŁawrowskiPrommesbergerLangeretal., author = {Ławrowski, Robert Damian and Prommesberger, Christian and Langer, Christoph and Dams, Florian and Schreiner, Rupert}, title = {Influence of reactive ion etching parameters on the geometry of silicon tip cathodes for field emission}, series = {Applied Research Conference 2013, ARC 2013 : 17th and 18th October 2013, Deggendorf}, booktitle = {Applied Research Conference 2013, ARC 2013 : 17th and 18th October 2013, Deggendorf}, publisher = {Shaker}, address = {Aachen}, isbn = {978-3-8440-2274-2}, pages = {67 -- 69}, language = {en} } @incollection{ŁawrowskiPrommesbergerLangeretal., author = {Ławrowski, Robert Damian and Prommesberger, Christian and Langer, Christoph and Dams, Florian and Schreiner, Rupert}, title = {Feldemissionselektronenquellen basierend auf Siliziumemittern mit hohen Aspektverh{\"a}ltnis}, series = {Forschungsbericht der OTH Regensburg 2013}, booktitle = {Forschungsbericht der OTH Regensburg 2013}, address = {Regensburg}, pages = {47 -- 48}, language = {de} } @inproceedings{MingelsBornmannLuetzenkirchenHechtetal., author = {Mingels, Stephan and Bornmann, Benjamin and L{\"u}tzenkirchen-Hecht, Dirk and M{\"u}ller, G{\"u}nter and Langer, Christoph and Prommesberger, Christian and Schreiner, Rupert}, title = {Electric Field Dependence of Photoemission from n- and p-type Si Crystals}, series = {Proceedings, 35th International Free Electron Laser Conference (FEL 2013) : New York, NY, USA, August 26-19, 2013}, booktitle = {Proceedings, 35th International Free Electron Laser Conference (FEL 2013) : New York, NY, USA, August 26-19, 2013}, editor = {Scholl, Caitlin and Schaa, Volker R.W.}, publisher = {Curran}, address = {Red Hook, NY}, isbn = {9783954501267}, pages = {339 -- 343}, abstract = {The performance of free electron lasers depends on the brilliance of the electron source. Nowadays photo-cathodes (e.g. Cs2Te) are used despite of their high emittance. To develop robust and more brilliant cathodes we have built up an UHV system which enables systematic photoemission (PE) measurements with a tunable pulsed laser (hv) at high electric fields (E). First results on Au and Ag crystals revealed only low quantum efficiency (QE) due to fast electron relaxation. Hence, we have started QE(hv,E) investigations on n- and p-Si wafers. Resonant PE was observed above as well as below the work function O, which can be assigned to optical transitions in the electronic band structure or explained by thermally excited states at the bottom of the conduction band. As expected, only low QE values were achieved even for n-Si probably due to surface oxide. Moreover, a significant rise of the QE peaks above O were obtained for n-Si at E >8 MV/m but limited by the occurrence of parasitic field emission from dust particles.}, language = {en} } @inproceedings{SchreinerPrommesbergerLangeretal., author = {Schreiner, Rupert and Prommesberger, Christian and Langer, Christoph and Dams, Florian and Serbun, Pavel and Bornmann, Benjamin and Navitski, Aliaksandr and M{\"u}ller, G{\"u}nter}, title = {Highly uniform and stable electron field emission from B-doped Si-tip arrays for applications in integrated vacuum microelectronic devices}, series = {25th International Vacuum Nanoelectronics Conference (IVNC) - Jeju, Korea (South), 09.07. - 13.07.2012}, booktitle = {25th International Vacuum Nanoelectronics Conference (IVNC) - Jeju, Korea (South), 09.07. - 13.07.2012}, publisher = {IEEE}, address = {Piscataway, NJ.}, isbn = {978-1-4673-1984-3}, issn = {2380-6311}, doi = {10.1109/IVNC.2012.6316857}, pages = {1 -- 2}, abstract = {In order to improve the uniformity and field emission stability of p-type silicon tip arrays for pulsed sensor applications, we have systematically studied the influence of the fabrication parameters on the tip shape and the specific operating conditions. Based on detailed design calculations of the field enhancement, we have fabricated a series of hexagonal arrays of B-doped Si-tips in a triangular arrangement, each containing a different number of tips (91, 575 and 1300) of 1 μm height, 20 nm apex radius, and 20 μm pitch. The field emission properties of both individual tips and complete arrays were investigated with by field emission scanning microscopy. The current plateaus of these tips typically occur at about 10 nA and 60 V/μm field level. In this carrier depletion range, single tips provide the highest current stability (<; 4\%) and optical current switching ratios of ~2.5. Rather homogeneous emission of the tip arrays leads to an almost linear scaling of the saturation current (2 nA/tip) and to a much improved current stability (<; 1\%) measured over 1 hour.}, language = {en} } @inproceedings{BornmannMingelsSerbunetal., author = {Bornmann, Benjamin and Mingels, Stephan and Serbun, Pavel and L{\"u}tzenkirchen-Hecht, Dirk and M{\"u}ller, G{\"u}nter and Prommesberger, Christian and Langer, Christoph and Dams, Florian and Schreiner, Rupert}, title = {Photosensitivity of electron field emission from B-doped Si-tip arrays}, series = {25th International Vacuum Nanoelectronics Conference (IVNC) ; Jeju, Korea (South), 09.07.2012 - 13.07.2012}, booktitle = {25th International Vacuum Nanoelectronics Conference (IVNC) ; Jeju, Korea (South), 09.07.2012 - 13.07.2012}, publisher = {IEEE}, isbn = {978-1-4673-1984-3}, issn = {2380-6311}, doi = {10.1109/IVNC.2012.6316980}, pages = {1 -- 2}, abstract = {The electron current from field-emitting B-doped Si-tip arrays under illumination was studied. An improved cathode design with a patch of 271 tips yielded a reproducible cathode current between 0.2-2000 nA in the electric field range of 3.8-6.6 V/μm. The plateau in the Fowler-Nordheim plot shows the actual carrier depletion and leads to a very stable emission at ~1 μA with a current noise of less than 3.3 \%. Color-filtered halogen lamp illumination was used to investigate the photo-sensitivity of the saturation current. The intensity-normalized current switching ratio increases nonlinearly with the photon energy. This hints either for secondary generation in the conduction band or deeper valence band excitation. The first is supported by a rough estimation of the quantum efficiency. Further experiments with a tunable laser and electron spectroscopy are planned.}, language = {en} } @inproceedings{LangerPrommesbergerDamsetal., author = {Langer, Christoph and Prommesberger, Christian and Dams, Florian and Serbun, Pavel and Bornmann, Benjamin and Mingels, Stephan and M{\"u}ller, G{\"u}nter and Schreiner, Rupert}, title = {Si-Feldemissionskathoden f{\"u}r Anwendungen in miniaturisierten Ionisationsvakuumsensoren}, series = {Verhandlungen der Deutschen Physikalischen Gesellschaft e.V. (DPG), Regensburg, 10. - 15. M{\"a}rz 2013}, booktitle = {Verhandlungen der Deutschen Physikalischen Gesellschaft e.V. (DPG), Regensburg, 10. - 15. M{\"a}rz 2013}, publisher = {Deutsche Physikalische Gesellschaft e.V.}, abstract = {Feldemissionselektronenquellen sind aufgrund ihrer prinzipiellen Vorteile gegen{\"u}ber Gl{\"u}hkathoden bereits seit l{\"a}ngerer Zeit Gegenstand der Forschung und werden bisher nur in einigen Spezialanwendungen erfolgreich eingesetzt. Hierbei werden Einzelspitzen mit Spannungen im kV-Bereich und Str{\"o}men im nA-Bereich betrieben. Dagegen werden f{\"u}r miniaturisierte Sensorsysteme eher Spannungen von ca. 100 V und Str{\"o}me von ca. 1 mA ben{\"o}tigt. Dazu wurden bisher meist Feldemissionskathoden mit CNTs vorgeschlagen, welche f{\"u}r Anwendungen in der Halbleiterindustrie aufgrund des Kohlenstoffanteils nicht erw{\"u}nscht sind. Ziel unserer Arbeit ist es, Si-basierte Elektronenquellen zu realisieren, die mit anderen miniaturisierten Vakuumsensoren auf einem Chip integrierbar sind. Mithilfe eines optimierten Herstellungsprozesses konnten wir p-Si-Spitzenarrays mit Spitzenradien von wenigen nm realisieren [1]. Messungen an diesen Strukturen zeigen ein sehr homogenes Emissionsverhalten, das vor allem im S{\"a}ttigungsbereich bei Emissionsstr{\"o}men von ca. 10 nA pro Spitze zeitlich stabil (Schwankungen < 5 \%) und optisch schaltbar (Faktor > 2.5) ist [2].}, language = {de} } @inproceedings{PrommesbergerDamsLangeretal., author = {Prommesberger, Christian and Dams, Florian and Langer, Christoph and Schreiner, Rupert and Rutkowski, S. and Bornmann, Benjamin and M{\"u}ller, G{\"u}nter}, title = {Simulation of electron trajectories of a field emission electron source in triode configuration by using finite element methods}, series = {24th International Vacuum Nanoelectronics Conference (IVNC), 2011 : 18 - 22 July 2011, Historische Stadthalle Wuppertal, Germany}, booktitle = {24th International Vacuum Nanoelectronics Conference (IVNC), 2011 : 18 - 22 July 2011, Historische Stadthalle Wuppertal, Germany}, publisher = {IEEE}, address = {Piscataway, NJ}, isbn = {978-3-00-035081-8}, issn = {2380-6311}, pages = {144 -- 145}, abstract = {The finite element simulation program COMSOL Multiphysics® was used to simulate the emission efficiency of a silicon tip electron source in triode configuration for different geometries and electrode potentials. The simulation predicts a maximum emission efficiency of 84\% for an optimized structure. In a second simulation a gate electrode was concentrically arranged above a single CNT column. Here, the efficiency was simulated as a function of gate hole geometry, electrode potentials and distances between the electrodes. The simulation shows that a conical shape of the gate hole results in an efficiency up to nearly 100\%.}, language = {en} } @inproceedings{BachmannDamsDuesbergetal., author = {Bachmann, Michael and Dams, Florian and D{\"u}sberg, F. and Hofmann, Martin and Pahlke, Andreas and Langer, Christoph and Ławrowski, Robert Damian and Prommesberger, Christian and Schreiner, Rupert}, title = {Stability investigation of high aspect ratio n-type silicon field emitter arrays}, series = {2015 28th International Vacuum Nanoelectronics Conference (IVNC), 13-17 July 2015, Guangzhou, China}, booktitle = {2015 28th International Vacuum Nanoelectronics Conference (IVNC), 13-17 July 2015, Guangzhou, China}, publisher = {IEEE}, doi = {10.1109/IVNC.2015.7225584}, pages = {204 -- 205}, abstract = {Electron sources based on silicon field emitter arrays, produced in processes based on semiconductor technology, are good candidates for a miniaturized X-ray source. A key parameter for this application is the stability of the X-ray photon flux and, thus, the emission current. In the present work we have investigated the influence of the residual gas pressure and a resistor in series on the emission stability of a high aspect ratio n-type silicon emitter array with hybrid extraction electrode. An increase of current fluctuations was found for pressures above 10-6 mbar. High resistances in series to the emitter array alter the emission characteristics, but greatly suppress spikes in the emission current and improve its stability. This, however, strongly depends on the bias point. The field enhancement factor is not affected by the resistance. In a long term measurement the emission current was found to be constant after an initial phase of degradation.}, language = {en} } @inproceedings{SerbunNavitskiMuelleretal., author = {Serbun, Pavel and Navitski, Aliaksandr and M{\"u}ller, G{\"u}nter and Schreiner, Rupert and Prommesberger, Christian and Langer, Christoph and Dams, Florian}, title = {Scaling of the field emission current from B-doped Si-tip arrays}, series = {25th International Vacuum Nanoelectronics Conference (IVNC) ; Jeju, Korea (South), 09.07.2012 - 13.07.2012}, booktitle = {25th International Vacuum Nanoelectronics Conference (IVNC) ; Jeju, Korea (South), 09.07.2012 - 13.07.2012}, publisher = {IEEE}, address = {Piscataway, N.J.}, isbn = {978-1-4673-1984-3}, issn = {2380-6311}, doi = {10.1109/IVNC.2012.6316965}, pages = {1 -- 2}, abstract = {We have fabricated a test chip with various hexagonal arrays of B-doped Si tips (height ~ 3 μm, apex radius <; 30 nm, number 1-4447, resistivity 4 Ωcm, 100 orientation) in triangular arrangement (pitch 10 μm, density 1.16×10 6 cm -2 ) in order to systematically investigate the field emission current scaling with the number N of tips. Regulated voltage scans for 1 nA revealed rather efficient emission from nearly all tips of the arrays at an average field of 15 V/μm. The expected current plateau was always obtained at fields around 20 V/μm, but its width strongly increased with N. In this carrier depletion range, the single tip provided a much higher stability (<; 5\%) of the current (2-3 nA) than at lower (>; 50 \%) and higher currents (>; 30\%). Integral current measurements of the hexagonal arrays resulted in a statistically improved current stability (<; 1\%) but only a weak increase of the total current with N 0.28 yet. These results will be discussed with respect to the remaining inhomogeneity of the tips.}, language = {en} } @article{KleshchSerbunLuetzenkirchenHechtetal., author = {Kleshch, Victor I. and Serbun, Pavel and L{\"u}tzenkirchen-Hecht, Dirk and Orekhov, Anton and Ivanov, Victor E. and Prommesberger, Christian and Langer, Christoph and Schreiner, Rupert and Obraztsov, Alexander N.}, title = {A Comparative Study of Field Emission from Pristine, Ion-treated and Tungsten Nanoparticle-decorated p-type Silicon Tips}, series = {Physica Status Solidi B}, volume = {256}, journal = {Physica Status Solidi B}, number = {9}, publisher = {Wiley}, doi = {10.1002/pssb.201800646}, abstract = {The field electron emission characteristics of individual tips of a silicon field emitter array are analyzed. The array of conical-shaped tips is fabricated on a p-type silicon wafer by using reactive ion etching and sharpening oxidation. The tips are decorated with single tungsten nanoparticles at their apexes. Furthermore, the focused ion beam is also used to increase surface conductivity of some of the tips. Comparative measurements of field emission are performed by using the scanning anode probe field emission microscopy technique. All types of tips demonstrated emission activation consisting of a sudden current increase at a certain value of the applied voltage. Compared to the pristine tips, a noticeable reduction of the saturation effect in the current-voltage characteristics and a smaller light sensitivity for the decorated tips is found. For ion-treated tips, saturation effects and light sensitivity are completely suppressed. Scanning electron microscopy observations reveal the formation of single nanoscale protrusions extending from the metal particles and from the apexes of bare ion-treated tips after exposure under strong electric fields during the field emission measurements. The influence of protrusions growth on characteristics of silicon field emitter arrays is discussed.}, language = {en} }