TY - CHAP A1 - Döhring, Thorsten A1 - Probst, Anne-Catherine A1 - Stollenwerk, Manfred A1 - Wen, Mingwu A1 - Proserpio, Laura ED - den Herder, Jan-Willem A. ED - Takahashi, Tadayuki ED - Bautz, Marshall T1 - Development of low-stress Iridium coatings for astronomical x-ray mirrors T2 - Proceedings of SPIE 9905, Space Telescopes and Instrumentation 2016: Ultraviolet to Gamma Ray N2 - Previously used mirror technologies are not suitable for the challenging needs of future X-ray telescopes. This is why the required high precision mirror manufacturing triggers new technical developments around the world. Some aspects of X-ray mirrors production are studied within the interdisciplinary project INTRAAST, a German acronym for "industry transfer of astronomical mirror technologies". The project is embedded in a cooperation of Aschaffenburg University of Applied Sciences and the Max-Planck-Institute for extraterrestrial Physics. One important task is the development of low-stress Iridium coatings for X-ray mirrors based on slumped thin glass substrates. The surface figure of the glass substrates is measured before and after the coating process by optical methods. Correlating the surface shape deformation to the parameters of coating deposition, here especially to the Argon sputtering pressure, allows for an optimization of the process. The sputtering parameters also have an influence on the coating layer density and on the micro-roughness of the coatings, influencing their X-ray reflection properties. Unfortunately the optimum coating process parameters seem to be contrarious: low Argon pressure resulted in better micro-roughness and higher density, whereas higher pressure leads to lower coating stress. Therefore additional measures like intermediate coating layers and temperature treatment will be considered for further optimization. The technical approach for the low-stress Iridium coating development, the experimental equipment, and the obtained first experimental results are presented within this paper. KW - telescope KW - mirror KW - coating KW - iridium KW - astronomy KW - Röntgenspiegel KW - Iridium KW - Beschichtung Y1 - 2016 U6 - https://doi.org/10.1117/12.2232074 VL - 2016 IS - 9905 SP - 99056S-1 EP - 99056S-7 ER - TY - CHAP A1 - Probst, Anne-Catherine A1 - Döhring, Thorsten A1 - Stollenwerk, Manfred A1 - Mingwu, Wen A1 - Proserpio, Laura ED - Cugny, Bruno ED - Karafolas, Nikos ED - Sodnik, Zoran T1 - Iridium coatings for space based x-ray optics T2 - Proceedings of SPIE N2 - Future investigations of astronomical X-ray sources require light weight telescope systems with large collecting areas and good angular resolution. The Wolter I type telescope design offers a suitable possibility for obtaining performant X-ray mirrors with high collecting areas. The technology based on replicated slumped glass optics using thin glasses thereby provides the opportunity to fulfil the light weight and mass production requirements. In NASA's telescope NuSTAR this technology has been proven as advantageous compared to previous systems. Coating thin glasses with iridium, gold or platinum enhances the reflectivity of X-ray mirrors. KW - Iridium KW - coating KW - X-ray KW - astronomy KW - mirror KW - Iridium KW - Spiegelteleskop KW - Röntgenastronomie Y1 - 2017 U6 - https://doi.org/10.1117/12.2296167 VL - 2017 IS - 10562 SP - 105621E-01 EP - 105621E-09 ER - TY - JOUR A1 - Probst, Anne-Catherine A1 - Stollenwerk, Manfred A1 - Emmerich, Florian A1 - Büttner, Andre A1 - Zeising, Sebastian A1 - Stadtmüller, Johannes A1 - Riethmüller, Franziska A1 - Stehlikova, Veronika A1 - Mingwu, Wen A1 - Proserpio, Laura A1 - Damm, Christine A1 - Rellinghaus, Bernd A1 - Döhring, Thorsten T1 - Influence of sputtering pressure on the nanostructure and the X-ray reflectivity of iridium coatings JF - Surface and Coatings Technology N2 - Reflective mirror coatings made of iridium are used in X-ray telescopes of the Chandra X-ray Observatory (CXO) launched in 1999 by the National Aeronautics and Space Administration (NASA) to investigate astronomical sources at photon energies below 10. keV. These coatings were produced in a DC magnetron sputtering process and have so far proven their suitability for space-based applications. We are considering in the present paper the processing of thin iridium films for lightweight telescopes using the radio frequency magnetron sputtering technique with an oblique angle deposition. The coating development presented here is focused on the influence of total sputtering pressure on film properties as well as on its impact on the mirror's performance. Characterisation methods such as X-ray diffractometry, X-ray reflectometry, atomic force microscopy and transmission electron microscopy have been used. Correlations between morphology, density, surface micro-roughness, crystal structure of the iridium layer and the expected reflectivity of the X-ray mirror are described and discussed. KW - Iridium KW - sputtering KW - microstructure KW - coating KW - X-ray KW - Iridium KW - Röntgenteleskop Y1 - 2017 UR - https://doi.org/10.1016/j.surfcoat.2017.10.062 SN - 0257-8972 VL - 2017 IS - 343 SP - 101 EP - 107 ER -