TY - CHAP A1 - Rivolta, Giacomo A1 - Basso, Stefano A1 - Civitani, Marta Maria A1 - Cotroneo, Vincenzo A1 - Döhring, Thorsten A1 - Michler, Willy-Leopold A1 - Pareschi, Giovanni A1 - Spiga, Daniele A1 - Stollenwerk, Manfred T1 - Upgrade of a laboratory X-ray diffractometer to extend its operating range towards soft energies T2 - Proceedings of SPIE N2 - The optical properties of X-ray mirror samples are commonly measured using diffractometers based on laboratory sources; like the Bede D1 diffractometer operating at INAF-OAB. This instrument can generate a collimated X-ray beam up to 60 keV, even though the most interesting energy region for x-ray astronomy applications is usually below 10 keV. In the softest part of this range (below 6 keV), high X-ray absorption in air hinders a full and precise characterization of optical components. In this work, we present an upgrade of the Bede D1 diffractometer that extends the operative range of the instrument below 6 keV; this is done by maximizing the flux at lowest energies and by reducing absorption by means of a helium-rich atmosphere. The upgraded instrument will be used for the tests of X-ray mirrors with innovative soft X-ray coatings, with potential application to the next generation X-ray telescopes (such as ATHENA and eXTP). KW - X-ray KW - mirror KW - reflectivity KW - refractometer KW - ATHENA KW - Röntgenspiegel KW - Diffraktometer Y1 - 2022 UR - https://www.spiedigitallibrary.org/conference-proceedings-of-spie/12181/121814S/Upgrade-of-a-laboratory-x-ray-diffractometer-to-extend-its/10.1117/12.2629940.short U6 - https://doi.org/doi: 10.1117/12.2629940 SN - 0277-786X VL - 2022 IS - 12181 SP - 121814S-1 EP - 121814s-7 PB - SPIE ER - TY - JOUR A1 - Cotroneo, Vicenzo A1 - Basso, Stefano A1 - Civitani, Marta A1 - Döhring, Thorsten A1 - Gibertini, Eugenio A1 - Iovenitti, Simone A1 - Magagnin, Luca A1 - Pareschi, Giovanni A1 - Sironi, Giorgia A1 - Spiga, Daniele A1 - Tagliaferri, Gianpiero A1 - Valsecchi, Giuseppe T1 - Polydopamine Coatings for Enhanced Soft X-Ray Reflectivity in Space Telescope Mirrors JF - ECS Meeting Abstracts N2 - It has been known for years that sputtered low-density coatings deposited under vacuum (e.g. carbon or B4C), applied on top of high-density metallic coatings, can enhance their reflectivity in the soft X-ray band (below ~5 keV). However, the physical deposition techniques, as vacuum-based sputtering, to produce B4C or amorphous coatings are usually difficult and highly costing. Polydopamine (PDA), a bio-polymer inspired by mussels, exhibits exceptional surface binding and it’s nowadays a popular material used in surface engineering for multipurpose applications (Ryu, 2018). PDA thin film are typically produced in aqueous solution by the oxidative polymerization of dopamine, commonly known as one of the “hormones of happiness”, resulting in nanometric PDA coating with tunable thickness and morphology. In recent years, we have introduced and investigated a novel and scalable strategy for enhancing the soft X-ray reflectivity of telescope mirrors used in space missions based on dip-liquid deposition of PDA thin films as carbon-rich coating (carbon 62.7 %wt. in DA monomer) (Cotroneo, 2022). This method is very versatile and quick and offers a low-cost alternative to conventional carbon-like coating, while maintaining or even exceeding performance in the energy range below ~5 keV. Experimental tests across three X-ray beamlines—including two synchrotron facilities—demonstrated consistent reflectivity enhancement, especially in the 1–4 keV energy range and with a good match between theoretical predictions and experimental reflectivity profiles. When applied over traditional coatings (e.g Au, Ir), the dip-liquid overcoats produced improvements of up to 100% in effective area for some specific X-ray bands compared to conventional single-metal films. These results are particularly compelling for nickel-replicated mirrors with gold coatings, a common architecture in cost-sensitive space missions. Bibliography Cotroneo, V., 2022. Dopamine dip-liquid overcoatings for soft x-ray reflectivity enhancement. SPIE Proceedings. Ryu, J. H., 2018. Polydopamine Surface Chemistry: A Decade of Discovery. ACS Applied Materials & Interfaces. KW - Röntgenteleskop KW - Röntgenspiegel Y1 - 2025 U6 - https://doi.org/10.1149/MA2025-02673247mtgabs SN - 2151-2043 VL - MA2025-02 IS - 67 SP - 3247 EP - 3247 PB - The Electrochemical Society ER -