@misc{DoehringStollenwerkProserpioetal.2015, author = {D{\"o}hring, Thorsten and Stollenwerk, Manfred and Proserpio, Laura and Winter, Anita}, title = {Transfer of astronomical mirror technologies - Project INTRAAST}, year = {2015}, abstract = {Poster}, subject = {Optisches Glas}, language = {en} } @inproceedings{DoehringStollenwerkGongetal.2015, author = {D{\"o}hring, Thorsten and Stollenwerk, Manfred and Gong, Qingqing and Proserpio, Laura and Winter, Anita and Friedrich, Peter}, title = {The challenge of developing thin mirror shells for future X-ray telescopes}, series = {Proceedings of SPIE}, volume = {2015}, booktitle = {Proceedings of SPIE}, number = {9628}, organization = {Hochschule Aschaffenburg}, pages = {962809-1 -- 962809-8}, year = {2015}, abstract = {Previously used mirror technologies are not able to fulfil the requirements of future X-ray telescopes due to challenging requests from the scientific community. Consequently new technical approaches for X-ray mirror production are under development. In Europe the technical baseline for the planned X-ray observatory ATHENA is the radical new approach of silicon pore optics. NASA´s recently launched NuSTAR mission uses segmented mirrors shells made from thin bended glasses, successfully demonstrating the feasibility of the glass forming technology for X-ray mirrors. For risk mitigation also in Europe the hot slumping of thin glasses is being developed as an alternative technology for lightweight X-ray telescopes. The high precision mirror manufacturing requires challenging technical developments; several design trades and trend-setting decisions need to be made and are discussed within this paper. Some new technical and economic aspects of the intended glass mirror serial production are also studied within the recently started interdisciplinary project INTRAAST, an acronym for "industry transfer of astronomical mirror technologies". The goal of the project, embedded in a cooperation of the Max-Planck-Institute for extraterrestrial Physics and the University of Applied Sciences Aschaffenburg, is to master the challenge of producing thin mirror shells for future X-ray telescopes. As a first project task the development of low stress coatings for thin glass mirror substrates have been started, the corresponding technical approach and first results are presented.}, subject = {Astronomie}, language = {en} } @inproceedings{DoehringProbstStollenwerketal.2016, author = {D{\"o}hring, Thorsten and Probst, Anne-Catherine and Stollenwerk, Manfred and Wen, Mingwu and Proserpio, Laura}, title = {Development of low-stress Iridium coatings for astronomical x-ray mirrors}, series = {Proceedings of SPIE 9905, Space Telescopes and Instrumentation 2016: Ultraviolet to Gamma Ray}, volume = {2016}, booktitle = {Proceedings of SPIE 9905, Space Telescopes and Instrumentation 2016: Ultraviolet to Gamma Ray}, number = {9905}, editor = {den Herder, Jan-Willem A. and Takahashi, Tadayuki and Bautz, Marshall}, doi = {10.1117/12.2232074}, pages = {99056S-1 -- 99056S-7}, year = {2016}, abstract = {Previously used mirror technologies are not suitable for the challenging needs of future X-ray telescopes. This is why the required high precision mirror manufacturing triggers new technical developments around the world. Some aspects of X-ray mirrors production are studied within the interdisciplinary project INTRAAST, a German acronym for "industry transfer of astronomical mirror technologies". The project is embedded in a cooperation of Aschaffenburg University of Applied Sciences and the Max-Planck-Institute for extraterrestrial Physics. One important task is the development of low-stress Iridium coatings for X-ray mirrors based on slumped thin glass substrates. The surface figure of the glass substrates is measured before and after the coating process by optical methods. Correlating the surface shape deformation to the parameters of coating deposition, here especially to the Argon sputtering pressure, allows for an optimization of the process. The sputtering parameters also have an influence on the coating layer density and on the micro-roughness of the coatings, influencing their X-ray reflection properties. Unfortunately the optimum coating process parameters seem to be contrarious: low Argon pressure resulted in better micro-roughness and higher density, whereas higher pressure leads to lower coating stress. Therefore additional measures like intermediate coating layers and temperature treatment will be considered for further optimization. The technical approach for the low-stress Iridium coating development, the experimental equipment, and the obtained first experimental results are presented within this paper.}, subject = {R{\"o}ntgenspiegel}, language = {en} } @inproceedings{DoehringStollenwerkProserpioetal.2016, author = {D{\"o}hring, Thorsten and Stollenwerk, Manfred and Proserpio, Laura and Breunig, Elias and Friedrich, Peter}, title = {The challenging development of lightweight glass mirrors for future X-ray telescopes}, series = {DGaO Proceedings}, volume = {2016}, booktitle = {DGaO Proceedings}, publisher = {Deutsche Gesellschaft f{\"u}r angewandte Optik}, address = {Erlangen}, organization = {Hochschule Aschaffenburg}, issn = {1614-8436}, url = {http://nbn-resolving.de/nbn:de:0287-2016-B018-0}, pages = {2}, year = {2016}, abstract = {Previously used mirror technologies are not able to fulfill the challenging requirements of future X-ray telescopes. A promising new technology under development is the hot slumping of thin glasses. Challenges, design trades and first results are presented, including the thermal shaping process, the development of low stress coatings and the mirror segments integration concept.}, subject = {R{\"o}ntgenteleskop}, language = {en} } @inproceedings{ProbstDoehringStollenwerketal.2017, author = {Probst, Anne-Catherine and D{\"o}hring, Thorsten and Stollenwerk, Manfred and Mingwu, Wen and Proserpio, Laura}, title = {Iridium coatings for space based x-ray optics}, series = {Proceedings of SPIE}, volume = {2017}, booktitle = {Proceedings of SPIE}, number = {10562}, editor = {Cugny, Bruno and Karafolas, Nikos and Sodnik, Zoran}, doi = {10.1117/12.2296167}, pages = {105621E-01 -- 105621E-09}, year = {2017}, abstract = {Future investigations of astronomical X-ray sources require light weight telescope systems with large collecting areas and good angular resolution. The Wolter I type telescope design offers a suitable possibility for obtaining performant X-ray mirrors with high collecting areas. The technology based on replicated slumped glass optics using thin glasses thereby provides the opportunity to fulfil the light weight and mass production requirements. In NASA's telescope NuSTAR this technology has been proven as advantageous compared to previous systems. Coating thin glasses with iridium, gold or platinum enhances the reflectivity of X-ray mirrors.}, subject = {Iridium}, language = {en} } @article{BuettnerProbstEmmerichetal.2018, author = {B{\"u}ttner, Andre and Probst, Anne-Catherine and Emmerich, Florian and Damm, Christine and Rellinghaus, Bernd and D{\"o}hring, Thorsten and Stollenwerk, Manfred}, title = {Influence of Sputtering Pressure on the Microstructure and Layer Properties of Iridium Thin Films}, series = {Thin Solid Films}, volume = {2018}, journal = {Thin Solid Films}, number = {662}, issn = {0040-6090}, pages = {41 -- 46}, year = {2018}, abstract = {Iridium layers with low stress, high density, and low surface roughness find widespread use in different high-technology applications. This paper presents a study of the influence of the sputtering pressure on the properties of iridium thin films and of its effect on the substrate surface microstructure. We analysed the dependence of the microstructure, crystalline structure, electrical resistivity, and deposition rate on the sputtering pressure and surface defects of the substrate. For the latter, plasma etching of the substrate was performed for different processing times and its effect on the surface roughness of substrates and, subsequently, on the grown iridium films, was examined. The sputtering pressure and the substrate plasma etching time both had a strong influence on the microstructure and surface roughness. These microstructural changes are in good agreement with the tendency described in the Thornton Structure-Zone Model for different sputtering pressures and the microstructure phase map of Alvarez. The electrical resistivity, deposition rate, and crystalline structure were highly dependent on the sputtering pressure.}, subject = {Iridium}, language = {en} } @inproceedings{DoehringProbstStollenwerketal.2017, author = {D{\"o}hring, Thorsten and Probst, Anne-Catherine and Stollenwerk, Manfred and Emmerich, Florian and Stehl{\´i}kov{\´a}, Veronika and Inneman, Adolf}, title = {Prototyping iridium coated mirrors for X-ray astronomy}, series = {Proceedings of the International Society for Optics and Photonics}, volume = {2017}, booktitle = {Proceedings of the International Society for Optics and Photonics}, number = {10235}, editor = {Hudec, Ren{\´e} and Pina, Ladislav}, publisher = {SPIE International Society for Optics and Photonics}, address = {Bellingham WA}, organization = {Hochschule Aschaffenburg}, doi = {10.1117/12.2265931}, pages = {1023504-1 -- 1023504-8}, year = {2017}, abstract = {X-ray astronomy uses space-based telescopes to overcome the disturbing absorption of the Earth´s atmosphere. The telescope mirrors are operating at grazing incidence angles and are coated with thin metal films of high-Z materials to get sufficient reflectivity for the high-energy radiation to be observed. In addition the optical payload needs to be light-weighted for launcher mass constrains. Within the project JEUMICO, an acronym for "Joint European Mirror Competence", the Aschaffenburg University of Applied Sciences and the Czech Technical University in Prague started a collaboration to develop mirrors for X-ray telescopes. The X-ray telescopes currently developed within this Bavarian- Czech project are of Lobster eye type optical design. Corresponding mirror segments use substrates of flat silicon wafers which are coated with thin iridium films, as this material is promising high reflectivity in the X-ray range of interest. The deposition of the iridium films is based on a magnetron sputtering process. Sputtering with different parameters, especially by variation of the argon gas pressure, leads to iridium films with different properties. In addition to investigations of the uncoated mirror substrates the achieved surface roughness has been studied. Occasional delamination of the iridium films due to high stress levels is prevented by chromium sublayers. Thereby the sputtering parameters are optimized in the context of the expected reflectivity of the coated X-ray mirrors. In near future measurements of the assembled mirror modules optical performances are planned at an X-ray test facility.}, subject = {Iridium}, language = {en} } @inproceedings{ProbstDoehringZeisingetal.2017, author = {Probst, Anne-Catherine and D{\"o}hring, Thorsten and Zeising, Sebastian and Salmaso, Bianca and Stollenwerk, Manfred and Proserpio, Laura}, title = {Challenges in metrology of mirror segments for X-ray telescopes}, series = {Proceedings of the 8th High Level Expert Meeting Asphere Metrology}, volume = {2017}, booktitle = {Proceedings of the 8th High Level Expert Meeting Asphere Metrology}, number = {8}, publisher = {UTOB e.V.}, address = {Braunschweig}, organization = {Hochschule Aschaffenburg}, pages = {4}, year = {2017}, abstract = {High angular resolution, large collecting area and reduced weight per unit area are required for astronomical X-ray telescopes of the next generation observatories. New technologies for processing X-ray mirrors are under development to fulfill these needs. One option is to realize a Wolter I type telescope constituted of several hundred nested thin and light-weight X-ray mirror segments. The individual mirror segments need to be coated with an about 100 nm thick film of a high-reflective material to enhance the reflectivity for X-rays. Thereby an accurate shape metrology of the segments is necessary to predict the angular resolution of the astronomical telescope as well as to control the development process of X-ray mirrors. We present the challenges in shape measurements of thin glasses used to control the coating process and first experimental results about the repeatability of the measurements.}, subject = {Spiegelteleskop}, language = {en} } @inproceedings{DoehringProbstEmmerichetal.2017, author = {D{\"o}hring, Thorsten and Probst, Anne-Catherine and Emmerich, Florian and Stollenwerk, Manfred and Stehlikova, Veronika and Friedrich, Peter and Damm, Christine}, title = {Development of iridium coated X-ray mirrors for astronomical applications}, series = {Proceedings of the International Society for Optics and Photonics (SPIE)}, volume = {2017}, booktitle = {Proceedings of the International Society for Optics and Photonics (SPIE)}, number = {10399}, publisher = {SPIE}, doi = {10.1117/12.2273988}, pages = {103991C-1 -- 103991C-8}, year = {2017}, abstract = {Future space-based X-ray observatories need to be very lightweight for launcher mass constraints. Therefore they will use a reduced mirror thickness, which results in the additional requirement of low coating stress to avoid deformation of the initial precisely shaped mirror substrates. Due to their excellent reflection properties iridium coatings are sometimes applied for grazing incidence mirrors in astronomical X-ray telescopes. At Aschaffenburg University of Applied Sciences the coating of thin iridium films by an RF-magnetron sputtering technique is under development. The work is embedded in collaborations with the Max-Planck-Institute for Extraterrestrial Physics in Germany, the Czech Technical University in Prague, the Osservatorio Astronomico di Brera in Italy, the German Leibniz Institute for Solid State and Materials Research in Dresden, and the French Institute Fresnel. Sputtering with different parameters leads to iridium films with different properties. The current work is focused on the microstructure of the iridium coatings to study the influence of the substrate and of the argon gas pressure on the thin film growing process. Correlations between coating density, surface micro-roughness, the crystalline structure of the iridium layers, and the expected reflectivity of the X-ray mirror as well as coating stress effects are presented and discussed. The final goal of the project is to integrate the produced prototype mirrors into an X-ray telescope module. On a longer timescale measurements of the mirror modules optical performance are planned at the X-ray test facility PANTER.}, subject = {Iridium}, language = {en} } @article{ProbstStollenwerkEmmerichetal.2017, author = {Probst, Anne-Catherine and Stollenwerk, Manfred and Emmerich, Florian and B{\"u}ttner, Andre and Zeising, Sebastian and Stadtm{\"u}ller, Johannes and Riethm{\"u}ller, Franziska and Stehlikova, Veronika and Mingwu, Wen and Proserpio, Laura and Damm, Christine and Rellinghaus, Bernd and D{\"o}hring, Thorsten}, title = {Influence of sputtering pressure on the nanostructure and the X-ray reflectivity of iridium coatings}, series = {Surface and Coatings Technology}, volume = {2017}, journal = {Surface and Coatings Technology}, number = {343}, issn = {0257-8972}, pages = {101 -- 107}, year = {2017}, abstract = {Reflective mirror coatings made of iridium are used in X-ray telescopes of the Chandra X-ray Observatory (CXO) launched in 1999 by the National Aeronautics and Space Administration (NASA) to investigate astronomical sources at photon energies below 10. keV. These coatings were produced in a DC magnetron sputtering process and have so far proven their suitability for space-based applications. We are considering in the present paper the processing of thin iridium films for lightweight telescopes using the radio frequency magnetron sputtering technique with an oblique angle deposition. The coating development presented here is focused on the influence of total sputtering pressure on film properties as well as on its impact on the mirror's performance. Characterisation methods such as X-ray diffractometry, X-ray reflectometry, atomic force microscopy and transmission electron microscopy have been used. Correlations between morphology, density, surface micro-roughness, crystal structure of the iridium layer and the expected reflectivity of the X-ray mirror are described and discussed.}, subject = {Iridium}, language = {en} } @misc{DoehringProbullaKomziketal.2018, author = {D{\"o}hring, Thorsten and Probulla, Theodor and Komzik, Richard and Mann, Michael and Sivanic, Peter and Stollenwerk, Manfred}, title = {Slovak-Bavarian collaboration on the development of telescope instrumentation}, editor = {Hambalek, Lubomir}, organization = {Hochschule Aschaffenburg}, pages = {1}, year = {2018}, abstract = {Within the project SLOBATCO (Slovak-Bavarian Telescope Collaboration) the Astronomical Institute of the Slovak Academy of Sciences and Aschaffenburg University of Applied Sciences collaborate in the development and commissioning of the new {\O}1.3 m astronomical telescope and the corresponding scientific instrumentation. The project is funded by the Bavarian Academic Center for Central, Eastern and Southeastern Europe (BAYHOST). Technical work packages are targeting filter wheel software for the VIS camera, additional IR filters, and an upgrade of the mirror coating facility by additional sputtering equipment.}, subject = {Spiegelteleskop}, language = {en} } @article{ProbstBegouDoehringetal.2018, author = {Probst, Anne-Catherine and Begou, Thomas and D{\"o}hring, Thorsten and Zeising, Sebastian and Stollenwerk, Manfred and Stadtm{\"u}ller, Johannes and Emmerich, Florian and Lumeau, Julien}, title = {Coating stress analysis and compensation for iridium-based x-ray mirrors}, series = {Applied Optics}, volume = {2018}, journal = {Applied Optics}, number = {57 (29)}, editor = {Publishing OSA,}, pages = {8775 -- 8779}, year = {2018}, abstract = {Iridium-based coatings for mirrors of x-ray telescopes are studied. In particular, stress-induced deformation is characterized and shown to be compressive and equal to -1786  MPa. Two methods for stress compensation are then studied. One relies on the deposition of silica on the back surface of the substrate and a second one relies on the deposition of a chromium sublayer. Advantages and drawbacks of each of these techniques are presented.}, subject = {R{\"o}ntgenteleskop}, language = {en} } @inproceedings{DoehringStollenwerkSchmittetal.2022, author = {D{\"o}hring, Thorsten and Stollenwerk, Manfred and Schmitt, Paul and Szeghalmi, Andrea}, title = {Umweltbest{\"a}ndige Spiegelbeschichtungen aus Iridium f{\"u}r den infraroten Spektralbereich}, series = {DGaO Proceedings}, volume = {2022}, booktitle = {DGaO Proceedings}, number = {123}, publisher = {DGaO}, organization = {TH Aschaffenburg}, issn = {1614-8436}, pages = {1 -- 2}, year = {2022}, abstract = {Das Edelmetall Iridium ist hart; extrem dicht; thermisch, mechanisch und chemisch stabil; weist eine hohe Reflektivit{\"a}t im mittleren und fernen Infrarot auf und hat eine hohe Best{\"a}ndigkeit gegen{\"u}ber Umwelteinfl{\"u}ssen - auch ohne weitere Schutzschichten. Es wurden die komplexen Brechungsindizes f{\"u}r Iridium-Spiegelbeschichtungen bestimmt, welche vorhandene Literaturwerte erg{\"a}nzen.}, subject = {Iridium}, language = {de} } @article{SchmittFeldeDoehringetal.2022, author = {Schmitt, Paul and Felde, Nadja and D{\"o}hring, Thorsten and Stollenwerk, Manfred and Uschmann, Ingo and Hanemann, Kevin and Siegler, Marie and Klemm, Georg and Gratzke, Nancy and T{\"u}nnermann, Andreas and Schwinde, Stefan and Schr{\"o}der, Sven and Szeghalmi, Adriana}, title = {Optical, structural, and functional properties of highly reflective and stable iridium mirror coatings for infrared applications}, series = {Optical Materials Express}, volume = {2022}, journal = {Optical Materials Express}, number = {12 / 2}, doi = {10.1364/OME.447306}, pages = {545 -- 559}, year = {2022}, abstract = {Metallic coatings are essential for numerous optical systems due to their high and broadband refl ectivity in the infrared spectral range. In contrast to well-established (protected)silver and gold mirror coatings, iridium is environmentally durable, referring to ISO 9211-3 and thermally stable up to 600 °C even without protective layers, as demonstrated. Additionally,the optical and related structural properties of atomic layer deposited (ALD) and magnetron sputtered (MS) Ir coatings were investigated using spectrophotometry, FTIR, ellipsometry, WLI,AFM, XRR, XRD, SEM, and electrical resistivity measurements. The properties of Ir ALD and Ir MS coatings diff er due to their topography and microstructure.}, subject = {Iridium}, language = {en} } @article{SchmittFeldeDoehringetal.2022, author = {Schmitt, Paul and Felde, Nadja and D{\"o}hring, Thorsten and Stollenwerk, Manfred and Uschmann, Ingo and Hanemann, Kevin and Siegler, Marie and Klemm, Georg and Gratzke, Nancy and T{\"u}nnermann, Andreas and Schwinde, Stefan and Schr{\"o}der, Sven and Szeghalmi, Adriana}, title = {Optical, structural, and functional properties of highly reflective and stable iridium mirrorcoatings for infrared applications: supplement}, series = {Optical Materials Express}, volume = {2022}, journal = {Optical Materials Express}, number = {12/2}, doi = {10.6084/m9.figshare.17121509}, pages = {545 -- 559}, year = {2022}, abstract = {Metallic coatings are essential for numerous optical systems due to their high and broadband refl ectivity in the infrared spectral range. In contrast to well-established (protected)silver and gold mirror coatings, iridium is environmentally durable, referring to ISO 9211-3 and thermally stable up to 600 °C even without protective layers, as demonstrated. Additionally,the optical and related structural properties of atomic layer deposited (ALD) and magnetron sputtered (MS) Ir coatings were investigated using spectrophotometry, FTIR, ellipsometry, WLI, AFM, XRR, XRD, SEM, and electrical resistivity measurements. The properties of Ir ALD and Ir MS coatings diff er due to their topography and microstructure.}, subject = {Iridium}, language = {en} } @misc{DoehringStollenwerkSchmittetal.2022, author = {D{\"o}hring, Thorsten and Stollenwerk, Manfred and Schmitt, Paul and Szeghalmi, Adriana}, title = {Umweltbest{\"a}ndige Spiegelbeschichtungen aus Iridium f{\"u}r den infraroten Spektralbereich}, publisher = {DGaO}, organization = {TH Aschaffenburg}, pages = {1 -- 1}, year = {2022}, abstract = {Hochreflektierende Metallbeschichtungen sind essenziell f{\"u}r zahlreiche optische Elemente. Bew{\"a}hrte Spiegelbeschichtungen aus Silber und Gold bieten eine hohe und breitbandige Eigenreflexion im infraroten Spektralbereich, sind ohne geeignete Schutzschichten jedoch anf{\"a}llig gegen{\"u}ber Umwelteinfl{\"u}ssen und mechanischer Beanspruchung. Insbesondere im langwelligen Spektralbereich verringern die Absorptionsbanden dieser Schutzschichten teilweise die hohe Spiegelreflektivit{\"a}t wieder. Das Edelmetall Iridium (Ir) ist hart; extrem dicht; thermisch, mechanisch und chemisch stabil; weist eine {\"a}hnlich hohe Reflektivit{\"a}t im mittleren und fernen Infrarot, wie Silber und Gold, auf und hat zus{\"a}tzlich eine hohe Best{\"a}ndigkeit gegen{\"u}ber Umwelteinfl{\"u}ssen - auch ohne Schutzschichten. In diesem Beitrag werden die optischen und strukturellen Eigenschaften von Iridium-Spiegelbeschichtungen, welche mittels Atomlagenabscheidung (ALD) und DC-Magnetron-Sputtern hergestellt wurden, vorgestellt und miteinander verglichen. Die komplexen Brechungsindizes f{\"u}r ALD-erzeugte und gesputterte Iridium-Spiegelbeschichtungen wurden f{\"u}r Wellenl{\"a}ngen von 200 nm bis 20 μm bestimmt, welche nun bereits vorhandene Literaturwerte erg{\"a}nzen.}, subject = {Iridium}, language = {de} } @inproceedings{DoehringStollenwerkSchmittetal.2022, author = {D{\"o}hring, Thorsten and Stollenwerk, Manfred and Schmitt, Paul and Szeghalmi, Adriana}, title = {Environmentally stable iridium mirror coatings for the infrared spectral range}, series = {Proceedings of SPIE}, volume = {2022}, booktitle = {Proceedings of SPIE}, number = {12298}, publisher = {SPIE}, organization = {TH Aschaffenburg}, doi = {https://doi.org/10.1117/12.2632057}, pages = {122980A-1 -- 122980A-08}, year = {2022}, abstract = {Highly reflective metal coatings are essential for numerous optical elements. Established mirror coatings made of silver (Ag) and gold (Au) offer high and broadband self-reflection in the infrared (IR) spectral range but are susceptible to environmental influences and mechanical stress without suitable protective layers. In the long-wavelength spectral range, in particular, the absorption bands of these protective layers partially reduce the high mirror reflectivity again. However, the noble metal iridium (Ir) is hard, extremely dense, and thermally, mechanically, and chemically stable. Iridium provides a similarly high reflectivity in the mid (MIR) and far-infrared (FIR) spectral range, as silver and gold, and high resistance to environmental influences - even without protective layers. In this paper, the different deposition processes, as well as the optical and structural properties of iridium mirror coatings fabricated by atomic layer deposition (ALD) and by magnetron sputtering (MS), are presented and compared with each other. The complex refractive indices for ALD and MS deposited iridium mirror coatings were determined for wavelengths from 200 nm to 20 μm, complementing the existing literature values. We demonstrate that iridium mirror coatings offer a high and broadband reflectivity from the mid to far-infrared spectral range. In contrast to established - protected - silver and gold mirror coatings, the iridium coatings are environmentally durable and thermally stable up to 600 °C, even without protective layers. Therefore, as an interesting mirror coating material, iridium has the potential for special applications in infrared astronomy and probably also for industrial instruments.}, subject = {Iridium}, language = {en} } @misc{DoehringRoedlingKimmeletal.2021, author = {D{\"o}hring, Thorsten and R{\"o}dling, Claudius and Kimmel, Kevin and Zeising, Sebastian and Stadtm{\"u}ller, Johannes and Stollenwerk, Manfred and Verma, Shruti and Rees, Paul}, title = {Optical characterization of reflective coatings for astronomical telescope mirrors}, series = {DGaO Jahrestagung}, volume = {2021}, journal = {DGaO Jahrestagung}, organization = {TH Aschaffenburg}, pages = {1 -- 1}, year = {2021}, abstract = {With ground based optical telescopes astronomers observe celestial objects over a wide spectral range. As usually three or even more reflections at telescope mirrors are involved, good reflection properties of the mirror coatings are important. The aluminum evaporation technique has been - and is still - the standard solution for the reflective coatings of large astronomical mirrors. Such coatings have excellent reflectivity in the ultraviolet and in the visible, but perform poorly in the infrared. Silver is the metal having highest reflectivity for wavelengths longward of 400 nm, but isn´t the best choice for reflectivity in the ultraviolet and for blue light. To avoid degradation by oxidation, durable silver coatings need to be protected by transmitting overcoating layers. In the presented study, different metallic coatings - including unusual ones like sputtered iridium - are characterized to identify a coating that is most suitable for the spectral range from ultraviolet to infrared. Experimental results are compared to simulations based on the complex refractive indices of these materials. Thereby dependence of incidence angle and polarization is also considered.}, subject = {Spiegelteleskop}, language = {en} } @inproceedings{FreudenmannStollenwerkDoehringetal.2021, author = {Freudenmann, Dominic and Stollenwerk, Manfred and D{\"o}hring, Thorsten and Stadtm{\"u}ller, Johannes and Negri, Michele and Lauck, Felix}, title = {Combustion efficiency of iridium coated pellets for environmentally friendly space propulsion}, series = {14th Pico- and Nanosatellite Workshop, W{\"u}rzburg, Germany}, booktitle = {14th Pico- and Nanosatellite Workshop, W{\"u}rzburg, Germany}, year = {2021}, abstract = {Most of the satellite engines still uses critical fuels such as hydrazine, which is chemically aggressive, toxic and carcinogenic. New developments for satellite engines try to avoid such critical propellants. One promising approach is the usage of rocket-grade hydrogen peroxide [H2O2] in mono- and bipropellant driven rocket engines. Catalysts in the rocket engines convert the hydrogen peroxide by an exothermic catalytic reaction; the resulting hot gases oxygen and water vapor provide the thrust. Currently used catalysts are, for example, Al2O3 pellets impregnated with platinum. Within a joint research project of Aschaffenburg University and the German Aerospace Center new catalysts are developed. They consist of ceramic pellets coated with iridium using the magnetron sputtering process. Thereby the surface structure of the iridium layers strongly depends on the used sputtering process conditions [1]. After optimization of the sputtering parameters, it was demonstrated in laboratory experiments that the catalytic effect (measured by the volume of released gas) can be increased by a factor of four compared to platinum impregnated pellets [2]. In first hot firing tests at the test bench complex M11 at the DLR- Institute of Space Propulsion, these new, iridium-based catalysts have been used in a model combustion chamber for hydrogen peroxide decomposition. For this purpose, the reaction chamber was filled with iridium pellets in the high-altitude simulation chamber of the M11.2 test bench. The model chamber was equipped with numerous measuring devices like temperature and pressure sensors (e.g. Tcat, pcat). With the help of the mass flow and the herein obtained data, performance characteristics of the propellant system were accessible. High-concentrated hydrogen peroxide was used in the experiments as monopropellant (~ 87-wt.\% H2O2). During the experiments, the combustion chamber was operated in pulse mode and in continuous mode. Aim of this campaign called MoCa ("Monopropellant Catalytic Demonstrator") is the demonstration of functionality and the performance evaluation of this iridium-based monopropellant system. Recent experimental results will be presented. References: [1] A. B{\"u}ttner et al., Thin Solid Films 2018, 662: 41-46 [2] M. Stollenwerk et al., Journal of Materials Science 2021, 56(16), 9974-9984}, subject = {Satellitentechnik}, language = {de} } @inproceedings{DoehringStadtmuellerStollenwerketal.2021, author = {D{\"o}hring, Thorsten and Stadtm{\"u}ller, Johannes and Stollenwerk, Manfred and Cotroneo, Vincenzo and Pareschi, Giovanni and Gibertini, Eugenio and Magagnin, Luca}, title = {Low-density coatings for enhanced X-ray reflectivity of astronomical telescope mirrors}, series = {DGaO Proceedings}, volume = {2021}, booktitle = {DGaO Proceedings}, number = {122}, publisher = {DGaO}, organization = {TH Aschaffenburg}, issn = {1614-8436}, pages = {1 -- 2}, year = {2021}, abstract = {High reflectivity grazing incidence mirrors of astronomical X-ray telescopes are usually coated with thin layers of iridium, gold, or platinum. Due to a series of absorption edges, these noble metals have low reflectivity in the 2 - 4 keV band. We present the development of innovative material combinations using chromium and an additional layer of polydopamine for enhanced reflectivity X-ray coatings.}, subject = {R{\"o}ntgenteleskop}, language = {en} } @inproceedings{DoehringRoedlingKimmeletal.2021, author = {D{\"o}hring, Thorsten and R{\"o}dling, Claudius and Kimmel, Kevin and Zeising, Sebastian and Stadtm{\"u}ller, Johannes and Stollenwerk, Manfred and Verma, Shruti and Rees, Paul}, title = {Optical characterization of reflective coatings for astronomical telescope mirrors}, series = {DGaO Proceedings}, volume = {2021}, booktitle = {DGaO Proceedings}, number = {122}, publisher = {DGaO}, organization = {TH Aschaffenburg}, issn = {1614-8436}, pages = {1 -- 1}, year = {2021}, abstract = {Aluminium evaporation is still the standard solution for reflective coatings of large astronomical mirrors. Silver and gold are also used in specific cases depending on the targeted wavelength. This study characterized different metallic coatings - including unusual ones like sputtered iridium - to identify the most suitable mirror coating for the spectral range from ultraviolet to infrared wavelengths.}, subject = {Spiegelteleskop}, language = {en} } @misc{DoehringStadtmuellerStollenwerketal.2021, author = {D{\"o}hring, Thorsten and Stadtm{\"u}ller, Johannes and Stollenwerk, Manfred and Cotroneo, Vincenzo and Pareschi, Giovanni and Gibertini, Eugenio and Magagnin, Luca}, title = {Low-density coatings for enhanced X-ray reflectivity of astronomical telescope mirrors}, series = {DGaO Jahrestagung}, volume = {2021}, journal = {DGaO Jahrestagung}, organization = {TH Aschaffenburg}, pages = {1 -- 1}, year = {2021}, abstract = {X-ray telescopes usually operate in space and are quite different from astronomical telescopes for visible light. For normal angles of incidence, optical light is reflected on the mirror surface, whereas X-rays are either transmitted or absorbed. However, also high reflectivity X-rays mirrors are possible, when the incident rays direction is almost parallel to the mirror surface. Such grazing incidence mirrors are usually coated with thin layers of precious metals like iridium, gold or platinum, as this result in high X-ray reflectivity. These noble metals offer a wide range of reflection up to high photon energies, but, due to a series of absorption edges, have low reflectivity in the 2 - 4 keV band and below. This contribution presents the development of innovative material combinations based on thin layers of iridium and chromium, followed by an additional layer of carbon-based materials. We also discuss corresponding production methods (like dip coating) for enhanced reflectivity mirror coatings of future X-ray telescopes.}, subject = {R{\"o}ntgenstrahlung}, language = {en} } @inproceedings{StehlikovaDoehringSchaeferetal.2019, author = {Stehlikova, Veronika and D{\"o}hring, Thorsten and Sch{\"a}fer, Tobias and Stollenwerk, Manfred and Friedrich, Peter and Burwitz, Vadim and Hartner, Gisela and Bradshaw, Miranda and Liao, Yingyu and Pelliciari, Carlo}, title = {X-ray reflectivity measurements at chromium-iridium tri-layer coatings}, series = {Proceedings of SPIE}, volume = {2019}, booktitle = {Proceedings of SPIE}, number = {11119}, organization = {Max-Planck-Institut f{\"u}r Extraterrestrische Physik}, doi = {http://dx.doi.org/10.1117/12.2530439}, pages = {111191L-1 -- 111191L-6}, year = {2019}, abstract = {Studying astronomical objects in the X-ray regime, iridium-based layer systems are highly effective reflective materials for telescopes mirrors. Aschaffenburg University and the Czech Technical University in Prague jointly developed stress compensated chromium-iridium coatings. To overcome the disturbing reflectivity reduction of the iridium absorption edge around 2 keV photon energy and improve general reflectivity at lower incident energies, thin overcoat layers of chromium have been applied in addition. Corresponding measurements at several X-ray lines have been performed on these samples at the PANTER test facility of the Max-Planck Institute for extraterrestrial Physics. A part of the experimental results and their comparison with theoretical simulations are presented in this contribution.}, subject = {R{\"o}ntgenastronomie}, language = {en} } @inproceedings{WitteStollenwerk2008, author = {Witte, Gerd and Stollenwerk, Manfred}, title = {Energy saving of cooling water pumps for power plants using adjustable propeller blades}, series = {International Rotating Equipment Conference 2008, D{\"u}sseldorf}, booktitle = {International Rotating Equipment Conference 2008, D{\"u}sseldorf}, year = {2008}, subject = {K{\"u}hlwasseranlage}, language = {en} } @inproceedings{Stollenwerk2005, author = {Stollenwerk, Manfred}, title = {DVD/R 16x high quality mass production - Vortrag auf der Conference Replication Expo, September 2005, Shanghai, China}, year = {2005}, abstract = {Vortrag auf der Conference Replication Expo September 2005, Shanghai, China}, subject = {DVD-R}, language = {en} } @article{MustorphStollenwerkBressau2006, author = {Mustorph, Heinz and Stollenwerk, Manfred and Bressau, Volker}, title = {Current Developments in Optical Data Storage with Organic Dyes}, series = {Angewandte Chemie}, volume = {45}, journal = {Angewandte Chemie}, number = {13}, pages = {2016 -- 2035}, year = {2006}, abstract = {The main motivation for the development of digital data storage has been the improvement in play-back quality and the increase in storage capacity. In 1982 Philips and Sony introduced the first technically and economically successful system based on this—the compact disc (CD) and a compatible player. A very broad diversity of optical data recording formats are available today, and a difference is drawn between prerecorded, recordable, and rewritable media. This Review gives an overview of the systems used, the main features of production, and then concentrates on the properties of the organic dyes that are used in recordable systems. Dyestuffs chemistry has gained the reputation of having become a mature field of activity. Is this prejudice or a justified swan song for dyestuffs chemistry? When applications in optical data storage are considered, it is evident that even today progresses such as CD-R and DVD/R would not be feasible without functional dyes.}, subject = {Optischer Speicher}, language = {en} } @article{DoehringPribullaKomziketal.2019, author = {D{\"o}hring, Thorsten and Pribulla, Theodor and Komzik, Richard and Mann, Michael and Sivanic, Peter and Stollenwerk, Manfred}, title = {Slovak-Bavarian collaboration on the development of telescope instrumentation}, series = {Contributions of the Astronomical Observatory Skalnate Pleso}, volume = {2019}, journal = {Contributions of the Astronomical Observatory Skalnate Pleso}, number = {49 / 2}, pages = {154 -- 158}, year = {2019}, abstract = {Within the project SLOBATCO (Slovak-Bavarian Telescope Collaboration) the Astronomical Institute of the Slovak Academy of Sciences and Aschaffenburg University of Applied Sciences collaborate in the development and commissioning of scientific instrumentation for the new {\O}1.3 m astronomical telescope at the Skalnat{\´e} Pleso observatory. The joint project is funded by the Bavarian Academic Center for Central, Eastern and Southeastern Europe (BAYHOST). Planned technical work packages are targeting the filter wheel software for the VIS camera, additional IR filters, and an upgrade of the mirror coating facility by additional sputtering equipment.}, subject = {Spiegelteleskop}, language = {en} }