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In order to create alloys with exceptional properties for orthopedic uses, this study focuses on the impact of zirconium (Zr) content on the structural, electrochemical, and tribological qualities of nanostructured Ti–25NbxZr [x = 5, 10, 15, 20, 25, and 30 atomic (at.) %] alloys. The structural evolution was investigated using XRD and SEM techniques. The mechanical characteristics of the produced alloys, including Vickers hardness and Young’s modulus, were measured. In addition, the corrosion tests were performed using the OCP, EIS, and PD methods in Ringer’s solution within the independent pH range at 37°C. A ball-on-disc tribometer was used to investigate the tribological behavior of the alloys under various loads and wet conditions using the Ringer solution. It has been verified that Zr content (at. %) in the alloys had an impact on their morphologies, structural evolution, and mechanical characteristics. According to the morphological analysis, the particle and crystallite size decreases with increasing Zr content. Young’s modulus and Vickers hardness show the same tendency. The EIS data demonstrated that a single passive film formed on the alloy surfaces, and the addition of Zr enhanced the corrosion resistance of the passive films. The polarization curves demonstrate that the alloys had low corrosion current densities and large passive areas without the passive films disintegrating. Likewise, the inclusion of Zr resulted in a reduction in the corrosion and passive current density values. All of these results suggested that the titanium alloys exhibit a more noble electrochemical activity caused by Zr. From the tribological perspective, it was found that the friction coefficient of the alloys reduced with increasing Zr content.
Infections with COVID-19 in enclosed public spaces, where virus-laden aerosol particles can accumulate over time, have significantly contributed to the rapid spread of the virus. It is therefore of great importance to understand the transport and dispersion process of aerosol particles in such spaces, especially against the background of future pandemics. In this work, we present a Lagrangian-Particle-Tracking experiment to assess the mixed convective flow in a classroom with different ventilation strategies. For this purpose, thermal plumes were created by heated dummies, and a collimated LED light-sheet with ~0.4 m thickness was used for illumination of helium filled soap bubbles (HFSB) acting as passive tracer particles. In this way, the Lagrangian trajectories of the particles were recorded at two approximately 4.2 m × 2.8 m large fields using the novel 2D-Shake-The-Box-Method. As a result, time-resolved trajectories of over 300,000 simultaneously tracked HFSB have been reconstructed, so that both small-scale and large-scale properties of the flow are visualized quantitatively across the entire cross-section of the room. The trajectories show that the thermal plumes create lengthwise circulating vortices, which cannot be destroyed across the entire cross-section of the room by opening or tilting a window. Furthermore, the mixing in the room through the operation of an air purifier is higher compared to opening a window, which suggests that this strategy in combination with its air filtering capability is the most effective strategy to prevent infections.
While urban life can be characterized by endeavors to settle stable and safe environments, for many people, urban space is rarely stable or safe; it is uncertain, troubled, imbued with challenges and perpetually under pressure. As the concept of unsettled appears to define the contemporary urban experience, this multidisciplinary book investigates the conflicts and possibilities of settling and unsettling through open and speculative analysis. The analytical prism of unsettled renders urban space an indeterminate ground unfolding through routines, temporalities and contestations in constant tension between settling and unsettling. Such contrasting experiences are contingent on how urban societies confront, undergo and overcome turbulence and difficulties in time and space. Contributions drawing on theoretical reflections and empirical accounts—from Argentina, Austria, Germany, Greece, Italy, the Netherlands, the UAE, the UK, the USA and Vietnam—give insights into plural occurrences of the unsettled, which might tie down or unleash transformative, liberatory and emancipatory potentials. This book is for students, professionals and researchers interested in the uncertainties, foundations, disturbances, inconsistencies, residuals and blind fields, which constitute the urban both as lived space and as social, cultural and political ideal.
Assessing alternative agricultural water management strategies requires long-term field trials or vast data collection for model calibration and simulation. This work aims to assess whether an uncalibrated agro-hydrological model using global input datasets for climate, soil and crop information can serve as a decision support tool for crop water management under data scarcity. This study employs the Cool Farm Tool Water (CFTW) at eight eddy covariance sites of the FLUXNET2015 dataset. CFTW is tested using global (CFTWglobal) and local (CFTWlocal) input datasets under current and alternative management scenarios. Results show that the use of global datasets for estimating daily evapotranspiration had little effect on the median Root Mean Square Error (RMSE) (CFTWglobal: 1.70 mm, CFTWlocal: 1.79 mm), while, however, the median model bias is much greater (CFTWglobal: - 18.6%, CFTWlocal: - 4.3%). Furthermore, the periods of water stress were little affected by the use of local or global data (median accuracy: 0.84), whereas the use of global data inputs led to a significant overestimation of irrigation water requirements (median difference: 110 mm). The model performance improves predominantly through the use of more representative local precipitation data, followed by local reference evapotranspiration and soil for some European growing seasons. We identify model outputs that can support decision-making when relying on global data, such as periods of water stress and the daily dynamics of water use. However, our findings also emphasize the difficulty of overcoming data scarcity in decision-making in agricultural water management. Furthermore, we provide recommendations for enhancing model performance and thus may increase the accessibility of reliable decision support tools in the future.
Die vorliegende Arbeit behandelt für eine breite Klasse zweidimensionaler Variationsprobleme eine Existenz- und Regularitätstheorie, die der Lösung von Randwertproblemen partieller Differentialgleichungssysteme dient. Dabei werden bekannte Ergebnisse gründlich untersucht und umfassend aufgearbeitet. Teilweise wird eine geeignete Anpassung der Voraussetzungen einiger Resultate vorgenommen. Speziell wird die Theorie auf das Plateausche Problem für Flächen vorgeschriebener mittlerer Krümmung im R3 angewendet. Eingangs wird das Konzept der direkten Methoden der Variationsrechnung erläutert. Über einen fundamentalen Satz zur schwachen Unterhalbstetigkeit von Funktionalen wird die Existenz eines Minimierers für eine breite Klasse von Variationsproblemen nachgewiesen. Da die Existenztheorie in Sobolev-Räumen agiert, sind Untersuchungen zur Regularität eines Minimierers notwendig. Im Rahmen der Regularitätstheorie wird das Dirichletsche Wachstumstheorem von Morrey gezeigt, welches ein hinreichendes Kriterium für die Hölder-Stetigkeit einer Funktion X ∈ W1,2(G) liefert. Zum Nachweis der Anwendbarkeit des Dirichletschen Wachstumstheorems auf einen Minimierer wird ein Wachstumslemma verwendet. Dabei werden eine Verknüpfung des Dirichlet-Integrals mit Fourierreihen sowie das Dirichlet- Integral der harmonischen Ersetzung einer Funktion mit L2-Randwerten genutzt. Infolgedessen ergibt sich die Hölder-Stetigkeit im Inneren für einen Minimierer. Zudem wird die Stetigkeit des Minimierers bis zum Rand gezeigt, sodass die Existenz eines stetigen Minimierers für eine breite Klasse von Variationsproblemen gesichert ist. Anschließend erfolgt die Berechnung der ersten Variation sowie die damit verbundene Herleitung der schwachen Euler-Lagrange-Gleichung, welche eine Beziehung zur Lösungstheorie von Differentialgleichungen im Sinne des Dirichletschen Prinzips herstellt.
Ausgehend von der schwachen Euler-Lagrange-Gleichung wird die Hölder-Stetigkeit
der ersten Ableitungen eines Minimierers bewiesen. Für die Lösung von Randwertproblemen mit partiellen Differentialgleichungen zweiter Ordnung mithilfe der Variationsrechnung ist der Nachweis stetiger zweiter Ableitungen des Minimierers notwendig. Dabei wird der Fokus auf sogenannte Minimierer vom Poissonschen Typ gelegt. Eine C2,σ-Rekonstruktion, die auf der Schaudertheorie basiert, liefert in diesem Fall die gewünschte Regularität. In Anwendung dessen werden das Randwertproblem harmonischer Abbildungen in Riemannschen Räumen sowie das Dirichletproblem des H-Flächen-Systems behandelt, indem jeweils ein geeignetes Variationsproblem aufgestellt wird. Als Erweiterung des Dirichletproblems des H-Flächen-Systems wird das allgemeine
Plateausche Problem für Flächen vorgeschriebener mittlerer Krümmung mit den erarbeiteten Methoden der Variationsrechnung untersucht. Zudem wird das Plateausche Problem für Flächen vorgeschriebener mittlerer Krümmung in Kugeln, in Zylindern sowie insbesondere im Einheitskegel gelöst. Insgesamt wird eine ausführliche, in sich geschlossene und gut verständliche Existenzund Regularitätstheorie der zweidimensionalen Variationsrechnung zur Behandlung von Randwertproblemen partieller Differentialgleichungssysteme dargestellt, welche sich in besonderer Weise bei der Lösung des Plateauschen Problems für Flächen vorgeschriebener mittlerer Krümmung entfaltet.
This study describes the seasonal course of denitrifying and nitrate-reducing bacteria in a dimictic mesotrophic lake (Lake Scharmützelsee, Brandenburg, Germany) within a three-year period from 2011 to 2013. The bacterial cell numbers were quantified by the fluorescence microscopy, most probable number (MPN) and PCR-dependent quantification of the chromosomal 16S rDNA and of the nirS and nirK gene copy number. The highest seasonal differences (up to three orders of magnitudes) have been measured usingMPNin the epilimnion. This variation was not reflected by PCR-dependent approaches or direct microscopical enumeration. At adverse conditions (low temperature and/or low nitrate concentrations), the differences between MPN and gene copy numbers increased by up to five orders of magnitudes and decreased to one magnitude at favourable environmental conditions. These results can be explained best by an increasing ratio of viable but not cultivable (VBNC) cells or dead cells at impairing conditions. In the hypolimnion, the courses of MPN and nir gene copy numbers were similar. This can be explained by a higher feeding pressure and therefore smaller amounts of dormant cells. In the pelagial in general, the total cell numbers enumerated by either microscopical or molecular approaches were similar. In the sediment, more than 99% of the DNA was obviously not related to viable bacteria but was rather DNA in dead cells or adsorbed to particle surfaces.
Salvaging Buildings : reclaiming a livelihood from the excesses of Istanbul's mass urbanization
(2023)
Turkey’s demolition waste management is, to a great extent, dependent on çıkmacıs (reclaimers) who salvage condemned buildings for raw materials and architectural elements. Its urbanization history is full of key moments marked by building demolitions, which became a necessary material resource for informal urbanization. As early as the 1970s, the çıkmacıs helped the gecekondus [squatter houses] by supplying second-hand building materials and construction loans. They managed to turn a lack of infrastructure into an advantage and remain very adaptable to the ever-changing conditions of neo-liberalized urbanization. They depend on solidarity networks and other informal resources. Assemblage thinking helps to redefine the concept of informality, understand the relational dynamics between various actors, and focus on the agency of materials. The empirical data gained from ‘follow the thing’ ethnographic research in Turkey and Georgia reveals the double lives of çıkmacıs who move between village and city. Additionally, by following the example of a reclaimed window frame’s journey from Istanbul to Tbilisi, we can more clearly see the second-hand trade network in the context of urbanization and incremental architecture. In the context of waste’s materiality, the empirical part of the research shows the symbiotic relationship between çıkmacıs and the discarded demolition materials.
High-resolution imaging of buried metal interconnect structures in advanced microelectronic products with full-field X-ray microscopy is demonstrated in the hard X-ray regime, i.e., at photon energies > 10 keV. The combination of two multilayer optics—a side-by-side Montel (or nested Kirkpatrick–Baez) condenser optic and a high aspect-ratio multilayer Laue lens—results in an asymmetric optical path in the transmission X-ray microscope. This optics arrangement allows the imaging of 3D nanostructures in opaque objects at a photon energy of 24.2 keV (In-Kα X-ray line). Using a Siemens star test pattern with a minimal feature size of 150 nm, it was proven that features < 150 nm can be resolved. In-Kα radiation is generated from a Ga-In alloy target using a laboratory X-ray source that employs the liquid-metal-jet technology. Since the penetration depth of X-rays into the samples is significantly larger compared to 8 keV photons used in state-of-the-art laboratory X-ray microscopes (Cu-Kα radiation), 3D-nanopattered materials and structures can be imaged nondestructively in mm to cm thick samples. This means that destructive de-processing, thinning or cross-sectioning of the samples are not needed for the visualization of interconnect structures in microelectronic products manufactured using advanced packaging technologies. The application of laboratory transmission X-ray microscopy in the hard X-ray regime is demonstrated for Cu/Cu6Sn5/Cu microbump interconnects fabricated using solid–liquid interdiffusion (SLID) bonding.
Comparing hybrid urbanisms in the global south : water delivery configurations in Peru and Ghana
(2023)
Urban development processes in the Global South (and North) are often described as characterized by formal and informal practices of different actors and their respective material realities. In critical urban studies, the disposition for this binary conception of formal and informal urbanisms has been discussed for many years. To a certain extent, these sometimes align rather problematically with contrasting notions of the “structural” versus the “everyday.” In this article, we explore an understanding of formal and informal urban practices (and respectively “structure” and “everyday”) as always interrelated, and we develop a methodology for a comparative examination of such hybrid urbanisms. In doing so, we address a missing link in the surging theoretical debate on comparative/southern urbanisms, which has rarely been substantiated by methodological explorations. The adapted concept of “delivery configurations” combines analyses of actor networks, material realities, rules and regulations, discourses, and heterogenous arrays of urban practices of negotiating these. However, bringing together local particularities and structural commonalities and exploring their interrelation only provides a basis for understanding case‐specific complexities. We argue that embedding the analysis in a multi‐scalar comparative framework can further its analytical rather than descriptive attributes and provide deeper insights into issues such as social inequality. To illustrate our methodological contribution, we provide first insights from a comparative research
project of water delivery in different neighbourhoods in the secondary cities of Sunyani (Ghana) and Arequipa (Peru). We highlight the practical challenges of comparing diverse urban contexts and examining the rather complex relationships between infrastructure delivery, urban development, and social inequality.
Biomass and bioenergy perspectives of a coal region : status quo, potential and scenarios in Lusatia
(2023)
Coal has been one of the main fuels used in Europe. Its decreasing role due to the ongoing transformation of the energy system will create significant socio-economic challenges. The switch into renewable energy systems could be an alternative to maintain jobs and economic activities within the affected regions. Biomass use and bioenergy can play an important role in the energy transition. Instead of energy crops, forest and agricultural residues should be used as biogenic energy sources in the future to avoid impacts on land use and food security. The main objective of this article is to investigate the biomass potential of a coal region and to provide scenarios for the future development of bioenergy production. Due to the changing framework conditions and, as a result, the different biomass focuses, previous bioenergy potential estimates must be reviewed. The methods for determining the potential of biomass for energy production was used for Lusatia (in German: Lausitz), the second largest coal region in Germany. These methods can also be applied in other regions. As a first step, the regional status quo assessment of cultivated areas and yields had decisive relevance for calculating biomass potential ranges. In a second step, the current bioenergy facilities in the region were identified, with a focus on power and heat production. The third step was the estimation of future regional bioenergy use. Therefore, the regional potential was gathered with the generally supra-regional framework conditions. For this purpose, national scenario studies were used, which contain the relevant target values and framework conditions. Two scenarios were developed for future bioenergy estimations: a conservative path based on the current policies and a progressive path, derived from the goal of climate neutrality by 2045. The results show a qualitative comparison among both scenarios and the previously determined potential ranges. Bioenergy can probably contribute to achieving climate neutrality with an increase in wood-fired systems, while agricultural bioenergy potential is likely to decline. In the discussion section, however, the uncertainty of these results is pointed out, as future use of bioenergy will be heavily influenced by the regulatory framework, competition with material use and the influences of climate change.