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Organisationseinheit der BAM
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Paper des Monats
- ja (1)
Prediction of fiber/matrix debonding kinetics in glass fibre reinforced polyoximethylene under creep
(2011)
A method for independent prediction of creep damage accumulation on the basis of damage at short term loading and long-term strength is verified for the case of fiber/matrix debonding of injection moulded short glass fibre reinforced polyoximethylene. Small angle Scattering X-ray refractometry is applied for damage registration. The method is applicable to materials which display delocalised damage prior to fracture. The predicted damage is compared with the experimental data for damage accumulation in creep.
Especially trace amounts of water vapour in gases can be reliably determined by coulometric trace humidity sensors. The principle of these sensors is based on water vapour absorption in a hygroscopic layer and its subsequent electrolytic decomposition. The calibration of sensors was performed in the humidity range, expressed as frost point temperature, from −30°C to −80°C . This range is equivalent to volume fractions smaller than 376 µL·L−1. Generated humidity was measured with coulometric sensors and a chilled dew point hygrometer that was used as reference. An empirical non-linear function was found between sensor signal and measured reference humidity. This function consists of two parameters with a measurement uncertainty. Both calibration parameters were checked by means of one-way analysis of variance. It showed that gas specific function can be used for humidity measurement in nitrogen, hydrogen, dinitrogen monoxide, compressed and synthetic air. It is possible to determine trace humidity in all tested gases with an expanded uncertainty less than 2.1 K (coverage factor k=2 ) regarding frost point temperature.
Bei der Brücke Altstädter Bahnhof handelte es sich um eine große Spannbetonkonstruktion, die einen elementaren Verkehrsknotenpunkt in der Stadt Brandenburg an der Havel bildete. Entgegen üblichen Spannbetonkonstruktionen mit kleinen Bündelspanngliedern kamen beim Haupttragwerk in Längsrichtung großformatige Spannblockspannglieder zum Einsatz. Im Fall der vorliegenden Brücke setzte sich das Spannglied aus 392 ovalen Einzeldrähten aus Hennigsdorfer Produktion zusammen, welche als spannungsrisskorrosionsgefährdet gelten. Bei Bauwerkserkundungen wurde ein hoher Versprödungsgrad der Spannstähle festgestellt, sodass die Brücke am 19.05.2021 gesprengt werden musste. Zuvor traten im Bereich detektierter Spanndrahtbrüche von außen erkennbare Längsrisse in den Stegen anstatt von üblicherweise quer gerichteten Biegerissen an der gezogenen Randfaser auf. Die abweichende Schadensäußerung im Falle einer Spannstahlschädigung brachte das Bundesministerium für Digitales und Verkehr (BMDV) dazu, weitergehende Untersuchungen durchzuführen. In Zusammenarbeit mit dem Landesbetrieb Straßenwesen Brandenburg, der Hochschule für Technik und Wirtschaft Dresden sowie der Bundesanstalt für Materialforschung und prüfung (BAM) wurden experimentelle Untersuchungen insitu konzipiert und durchgeführt. Im Konkreten wurde an zwei Messstellen eine gezielte Schädigung des großformatigen Spannglieds vorgenommen, um das zuvor vorgefundene Schadensbild nachzuvoll ziehen und validieren zu können. Konzept, Ergebnisse aus den Untersuchungen und Erkenntnisse für gleichartig ausgeführte Bauwerke sind Gegenstand des ersten Beitrags (Teil 1). Der zweite Teil [1] wird sich im Schwerpunkt den verwendeten Messverfahren und Monitoringsystemen widmen, welche die Durchführung des Versuchs begleiteten.
The paper provides a summary of safety characteristics of hydrogen and hydrogen fuel gases. The inves-tigations focus on water electrolysis, the feeding of hydrogen into the natural gas grid and the use ofhydrogen for the fermentation process in biogas plants. The safety characteristics of hydrogen such as avery low minimum ignition energy, very large explosion range and high flame velocity with the resultingrapid pressure increase of hydrogen explosions are of particular importance for explosion protection andthey differ strongly from those of natural gas. Explosion ranges of hydrogen-methane-carbon dioxidemixtures have been measured for the use of hydrogen in biomethane production. The paper also showsand discusses explosion ranges of hydrogen and hydrogen-natural gas mixtures. Pressure and tempera-ture dependencies of the explosion limits of mixtures were investigated. Furthermore, pressure rise rates(KGvalues) were measured with regard to constructive explosion protection. The maximum experimen-tal safe gaps were determined for the classification of the mixtures and assignment to explosion groupsaccording to the European ATEX directives. It was found that admixture of 10% hydrogen to natural gashas only a minor influence on the safety characteristics of gas explosions.
High-strength structural steels are used in machine, steel, and crane construction with yield strength up to 960 MPa. However, welding of these steels requires profound knowledge of three factors in terms of avoidance of hydrogen-assisted cracking (HAC): the interaction of microstructure, local stress/strain, and local hydrogen concentration. In addition to the three main factors, the used arc process is also important for the performance of the welded joint. In the past, the conventional transitional arc process (Conv. A) was mainly used for welding of high-strength steel grades. In the past decade, the so-called modified spray arc process (Mod. SA) has been increasingly used for welding production. This modified process enables reduced seam opening angles with increased deposition rates compared with the Conv. A. Economic benefits of using this arc type are a reduction of necessary weld beads and required filler material. In the present study, the susceptibility to HAC in the heat-affected zone (HAZ) of the high-strength structural steel S960QL was investigated with the externally loaded implant test. For that purpose, both Conv. A and Mod. SA were used with same heat input at different deposition rates. Both conducted test series showed same embrittlement index “EI” of 0.21 at diffusible hydrogen concentrations of 1.3 to 1.6 ml/100 g of arc weld metal. The fracture occurred in the HAZ or in the weld metal (WM). However, the test series withMod. SA showed a significant extension of the time to failure of several hours compared with tests carried out with Conv. A.
Thermo Analytic Investigation of Hydrogen Effusion Behavior - Sensor Evaluation and Calibration
(2011)
The well established carrier gas analysis (CGA) method was used to test different hydrogen detectors comprising a thermal conductivity detector (TCD) and a metal oxide semiconducting (MOx) sensor. The MOx sensor provides high hydrogen sensitivity and selectivity, whereas the TCD exhibits a much shorter response time and a linear hydrogen concentration dependency. Therefore, the TCD was used for quantitative hydrogen concentration measurements above 50?µmol/mol. The respective calibration was made using N2/H2 gas mixtures. Furthermore, the hydrogen content and degassing behaviour of titanium hydride (TiH2-x) was studied. This material turned out to be a potential candidate for a solid sample calibration. Vacuum hot extraction (VHE) coupled with a mass spectrometer (MS) was then calibrated with TiH2-x as transfer standard. The calibration was applied for the evaluation of the hydrogen content of austenitic steel samples (1.4301) and the comparison of CGA-TCD and VHE-MS.
Martensitic 9% Cr steels like P91 and P92 show susceptibility to delayed hydrogen assisted cracking depending on their microstructure. In that connection, effective hydrogen diffusion coefficients are used to assess the possible time-delay. Limited data on room temperature diffusion coefficients reported in literature vary widely by several orders of magnitude (mostly attributed to variation in microstructure). Especially P91 weld metal diffusion coefficients are rare so far. For that reason, electrochemical permeation experiments had been conducted using P92 base metal and P91 weld metal (in as-welded and heat-treated condition) with different thicknesses. From the results obtained, diffusion coefficients were calculated using to different methods, time-lag, and inflection point. Results show that, despite microstructural effects, the sample thickness must be considered as it influences the calculated diffusion coefficients. Finally, the comparison of calculated and measured hydrogen concentrations (determined by carrier gas hot extraction) enables the identification of realistic diffusion coefficients.
Welded components of P91 9% Cr steel demand for careful welding fabrication with necessary post weld heat treatment (PWHT). Before the PWHT, a hydrogen removal heat treatment is necessary for avoidance of hydrogen assisted cracking (HAC). In this context, the microstructure and temperature-dependent hydrogen diffusion is important, and reliable diffusion coefficients of P91 weld metal are rare. For that reason, the diffusion behavior of P91 multi-layer weld metal was investigated for as-welded (AW) and PWHT condition by electrochemical permeation experiments at room temperature and carrier gas hot extraction (CGHE) from 100 to 400 °C. Hydrogen diffusion coefficients were calculated, and the corresponding hydrogen
concentration was measured. It was ascertained that both heat treatment conditions show significant differences. At room
temperature the AW condition showed significant hydrogen trapping expressed by to seven times lower diffusion coefficients. A preferred diffusion direction was found in perpendicular direction expressed by high permeability. The CGHE experiments
revealed lower diffusion coefficients for the AW condition up to 400 °C. In this context, a hydrogen concentration of approximately 21 ml/100 g was still trapped at 100 °C. For that reason, a certain HAC susceptibility of as-welded P91 weld metal cannot
be excluded, and hydrogen removal should be done before PWHT.