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Eingeladener Vortrag
- nein (1030)
This study aims at improving the detection of near-surface defects in magnetizable and conductive specimens by combining the measurements of eddy current, magnetic flux leakage and thermography testing. Different signal processing methods for data normalization are proposed to enable data fusion at the pixel level. These methods are applied to a test specimen which contains 10 variably-sized defects. We quantitatively evaluate the performances of a total of 29 detection methods with respect to false alarm reduction at a fixed level of true positive rate. We report that false positive rate could be reduced from 1.65% down to 0.28% by the best multi-sensor method compared to the best single-sensor performance on the smallest defect, when 50% found flaw pixels are required for successful detection.
In the last years, new approaches for the evaluation of the corrosion resistance of martensitic stainless steels were developed, which allow nearly non-destructive as well as short-term corrosion testing. This work analyzes the sensitive influence of microstructure and surface treatment on the corrosion resistance. The effect of alloy composition and microstructure, which is always present in addition to the influence of various surface treatments will be evaluated and discussed. The corrosion behavior was investigated with conventional evaluation of the pitting potential, electrochemical potentiodynamic reactivation (EPR), electrochemical noise (EN), and the 'KorroPad' (KP) technique. EPR provided information about the passivation ability and the extent of chromium content reduction due to chromium carbide precipitation in the microstructure. The use of EN and KP aims to detect the influence of different surface treatment parameters on the corrosion resistance in a nearly non-destructive way. Furthermore the results shall demonstrate the functionality and convenience of the short-term corrosion test methods EN and KP in order to gain more acceptance within the scientific community. The results will allow the extraction of surface treatment effects on the corrosion behavior of the martensitic stainless steels 1.4116, 1.4034, and 1.4021.
ln den letzten Jahren hat sich gezeigt, dass die Ermittlung des Schwellenwertes DeltaKth nach den bestehenden Standardvorschriften für verschiedene Materialien zu nichtkonservativen Werten führt. Das ergibt sich im Vergleich mit Schwellenwerten, die man mit Anrissen erhält, die hinsichtlich der Ober- und der Unterlast komplett im Druckbereich erzeugt wurden. Dort, wo die Diskrepanz auftritt, verstärkt sie sich mit abnehmendem Spannungsverhältnis. ln der vorliegenden Studie wurden an einem mittel- und einem hochfesten Stahl bei unterschiedlichen Spannungsverhältnissen Schwellenwerte bestimmt. Anwendung fanden die konventionelle Lastabsenkungsmethode nach ASTM-Standard und ein Verfahren, bei dem der Langrissscbwellenwert als Endpunkt der sogenannten Zyklischen R-Kurve erhalten wird. Dieses folgt im Wesentlichen der von Pippan et al. entwickelten Methode, ergänzt diese jedoch durch eine eigene Verfahrensvariante.
In Deutschland fallen aktuell über 5 Mio. Tonnen Hausmüllverbrennungsaschen (HMVA) pro Jahr an. Aus diesen werden nur ca. 8 % Metalle (davon ca. 1 % NE-Metalle) zurückgewonnen. Zur Beurteilung des Wertstoffpotentials werden die HMVA nach standardisierten Vorschriften beprobt, für die Analytik vorbehandelt/vorbereitet/aufgearbeitet und auf ihre Inhaltsstoffe analysiert. Im nachfolgenden Beitrag wird der Schwerpunkt auf die Probenvorbehandlung und -vorbereitung gelegt, wobei der Merkmalstransfer von der Ausgangs-(Feld-)Probe über die Laborprobe und die Prüfprobe bis zur Mess-(Analysen-) Probe am Beispiel von NE-Metallen einer nassaufbereiteten HMVA untersucht wurde. Die Ergebnisse wurden mit Hilfe statistischer Methoden bewertet. Die Ergebnisse zeigen, dass die Verteilung der NE-Metalle in den einzelnen Schritten der Probenbehandlung elementspezifisch ist. Bei Blei ist ein Erhalt der Merkmalsverteilung über alle Behandlungsschritte erkennbar. Bei Kupfer nehmen die Konzentrationen in den aufeinander folgenden Behandlungsschritten deutlich ab. Die Ursache könnte das in der Feinfraktion enthaltene metallische Kupfer mit seinen spezifischen Eigenschaften sein. -------------------------------------------------------------------------------------------------------------------------------------------
More than 5 billion tons of municipal solid waste incineration bottom ashes (MSWI BA) are generated by incineration per year in Germany. Currently only 8 % of metals (of these 1 % are non-ferrous metals) are recovered from MSWI BA. For characterization of recovery potential, MSWI BA samples have to be taken, pre-treated and analyzed according to standardized methods. This manuscript focuses on sample pre-treatment and preparation of a MSWI BA sample aiming to investigate the characteristics transfer over the process of sub-sampling from the original (field) sample to the laboratory sample, test sample until the analytical sample. All results have been evaluated with statistical methods. The results show that influence of each single pre-treatment and preparation step on metal content differs for the individual metals. For lead a conservation of characteristics distribution can be observed, while for copper a continuous decline of solid concentration is observed over all preparation steps. One possible reason may be the fact that copper is mainly contained in the fine fraction as metallic copper with specific properties.
We report on the formation of polymer-stabilized superparamagnetic single-core and multi-core maghemite nanoparticles. The particle formation was carried out by coprecipitation of Fe(II) and Fe(III) sulfate in a continuous aqueous process using a micromixer system. Aggregates containing 50 primary particles with sizes of 2 nm were formed at a reaction temperature of 30 °C. These particles aggregated further with time and were not stable. In contrast, stable single-core particles with a diameter of 7 nm were formed at 80 °C as revealed by small-angle X-ray scattering (SAXS) coupled in-line with the micromixer for particle characterization. X-ray diffraction and TEM confirmed the SAXS results. X-ray absorption near-edge structure spectroscopy (XANES) identified the iron oxide phase as maghemite.
Particle size modality in bi-modal iron oxide suspensions was resolved by exploiting complex ac-susceptibility (ACS), small angle X-ray scattering (SAXS) and photon cross-correlation spectroscopy. To explain dynamic magnetic response of bi-modal suspensions, the Debye model was expanded to a linear superposition form allowing for the contribution of both particle fractions. This modified and adopted model is able to resolve the bi-modal particle size distributions. The SAXS curves of mono- and bi-modal suspensions were fitted well using a Monte Carlo simulation scheme, allowing the detection of bi-modal particle size distributions with high precision.
Resovist® originally developed as a clinical liver contrast agent for Magnetic Resonance Imaging exhibits also an outstanding performance as a tracer in Magnetic Particle Imaging (MPI). In order to study the physical mechanism of the high MPI performance of Resovist®, we applied asymmetric flow fieldflow fractionation (A4F) and static magnetic fractionation (SMF) to separate Resovist® into a set of fractions with defined size classes. As A4F based on an elution method separates MNP according to their hydrodynamic size, SMF fractionates a particle distribution by its magnetic moment. The obtained fractions of both separation techniques were then magnetically characterized by magnetorelaxometry measurements to extract the corresponding effective magnetic anisotropy and hydrodynamic size distribution parameters. Additionally, the MPI performance of each fraction was assessed using magnetic particle spectroscopy. With both separation techniques fractions (normalized to their iron amount) an MPI signal gain of a factor of two could be obtained, even though the distribution of effective anisotropy and hydrodynamic size were significantly different. Relating these findings to the results from magnetic characterization allows for a better understanding of the underlying mechanisms of MPI performance of Resovist®. This knowledge may help to improve the design of novel MPI tracers and development of separation methods.
Shedding light onto the spectra of lime: Raman and luminescence bands of CaO, Ca(OH)2 and CaCO3
(2015)
In microscopy studies of 19th-century cement stone, we found free lime in the form of darkened spherical structures, as they were described in the literature already. When trying to determine their phase composition by Raman spectroscopy, we encountered contradictive assignments in literature spectra of the lime phases CaO, Ca(OH)2 and CaCO3 and observed strong spectral features that have been ignored or erroneously assigned so far. In this study we present Raman spectra of pure lime phases and of a naturally grown calcite crystal, burnt limestone (quick lime, mainly CaO), aged slaked lime putty (mainly Ca(OH)2), and carbonated lime putty (mainly CaCO3). Based on the results, we shed light mainly onto these two questions: (1) Does CaO have a Raman spectrum? (2) Which features in the spectra are luminescence bands that could be (and already have been) misinterpreted as Raman bands? We proof our assignment of luminescence bands in lime phases by using three different laser wavelengths for excitation, and give hypotheses on the origin of the luminescence as well as practical advices on how to identify these misleading features in Raman spectra. This article is mainly addressed to users of Raman spectroscopy in different fields of material analysis who might not be aware of the presence of interfering bands in their spectra.
Thermal ionisation, also known as surface ionisation, was one of the first ionisation techniques developed for mass spectrometry, having been invented as early as 1918. The ionization process, described by the empirically derived “fractionation laws”, is widely understood. Isotope ratio measurements can be achieved with high precision and accuracy. Due to this, thermal ionisation has paved the way for great scientific achievements including: the discovery of new isotopes, the determination of radioactive half-lives and atomic weights of the elements, the accurate determination of the age of the earth and investigations on human society in the past such as mobility and trade. TIMS is still regarded as ‘golden standard’ in isotope ratio measurements. Thus the method is a reference technique that remains at the forefront of isotopic analysis particularly in the fields of metrology. A concise overview is given here of the technical background of thermal ionisation as well as the numerous applications of this technique in earth sciences, industry, metrology, and nuclear forensics.
This paper indicates that the tribological behavior under dry sliding of a Fe3Al-niobium carbide (NbC) composite prepared by pyrometallurgical synthesis was compared to NbC-based hard metals bonded by cobalt or Fe3Al. The dry sliding wear resistance (0,1-7/10 m/s) of the present Fe3Al-NbC with ∼60% NbC was close to those known of NbC-based hard metals. No grain pull-outs or fragmentations of the NbC grains were seen in the wear tracks, as a metallurgical interphase was formed between matrix and NbC grains.
Measurement strategies
(2015)
Designing an appropriate measurement strategy for a particular analytical question is not always obvious, since a number of factors have to be considered, whereby some of them might be difficult to define. A set of key questions generally precede the experimental design in analytical measurements and help to choose the measurement strategy, which is fit for the intended use – in the particular case of the content of this book – either for quantification, elemental ratio or isotope ratio analyses, accordingly.
Maintenance, Repair and Overhaul (MRO) is acquiring increasing commercial and socio-economic significance. For products and goods with high investment costs and a long lifespan, especially in the sectors of energy and transportation, a considerable portion of commercial profits are generated by after-sales services. In the field of research and development, not enough attention has been paid so far to tasks and approaches involving MRO. The field thus has a limited scientific background, despite a high potential in the business sector for technological and scientific optimization. The challenges and chances of MRO for sustainable enterprises will be explained with reference to the Fraunhofer Innovation Cluster Maintenance, Repair and Overhaul in Energy and Transport. The developments and project results of the four fields of innovation »Cleaning«, »Repair and Overhaul«, »Condition Monitoring and Diagnosis«, as well as »MRO Planning and Digital Assistance« will be explained.
In- and quasielastic neutron scattering is employed to investigate both the vibrational density of states and the molecular dynamics of two homologous discotic liquid crystals (DLC) with different length of the alkyl side chain based on a triphenylene derivate. For both compounds characteristic low frequency excess contributions to the vibrational density of states are found. Therefore it is concluded that these liquid crystals show a glass-like behaviour. Elastic scans further show that in these materials a rich molecular dynamics takes place.
The application of high-strength fine-grained structural steels with yield strengths greater than or equal to 690 MPa expands because of present light weight design trends. The requirements regarding the welded components safety increased due to high loading capacity. This determines a sustainable and economic application as well. However, high welding residual stresses could diminish the components safety, especially due to high restraint conditions in component or repair welds. Therefore, this work is concerned with global and local welding stresses, especially crack-critical welding stresses in the HAZ and while root welding due to the restraint conditions. Restraint intensities of real components were analysed and realised with two different weld tests, alongside two different plate dimensions and steel grades. A comparison of the test results showed several significant effects for heat control and restraint intensity regarding restraint forces and local welding stresses. Among these effects, substantial influences were found for the filler metal selection with partially altered results for root and filler beads. Local stresses of weld seam and HAZ were affected differently.
For the description of (single) crystal orientations, e.g. as measured by electron backscatter diffraction (EBSD) & X-ray diffraction (XRD), Euler angles are still generally used to import and export data. However, because of the lack of standard definitions for the unit cell reference settings and specimen axes, several transformation descriptions exist which produce different sets of Euler angles for the same orientation. There is also no recommended region within the minimal Euler orientation space into which orientations should be placed. This is the reason why different sets of Euler angles for the same orientation are generated by the available software packages for indexing EBSD patterns. These issues are reviewed and addressed.
The influence of crystal symmetry in form of chiral (enantiomorphic) groups is discussed, as well as how multiple, but symmetry-equivalent sets of Euler angles can be reduced in order to deliver a unique orientation description. The Euler coloring algorithms applied to EBSD map data is critically discussed. The specific case of cubic symmetry, especially the effect of the three-fold rotation on the Euler space is investigated in more detail for the highest-symmetric chiral group 432. Recommendations for standard settings of the unit cell to orthogonal coordinate system transformation are given which exploit inherent symmetry.
The formation of laser-induced periodic surface structures (LIPSS) on different materials (silicon, fused silica, quartz) with linearly polarized fs-laser irradiation is studied experimentally. In dielectrics, the importance of transient excitation stages in the LIPSS formation is demonstrated by using (multiple) cross-polarized double-fs-laser-pulse irradiation sequences. A characteristic decrease of the spatial LIPSS periods is observed for double-pulse delays of less than 2 ps along with a characteristic 90°-rotation of the LIPSS orientation.
Polyglycerol (PG) coated polypropylene (PP) films were synthesized in a two-step approach that involved plasma bromination and subsequently grafting hyperbranched polyglycerols with very few amino functionalities. The influence of different molecular weights and density of reactive linkers were investigated for the grafted PGs. Longer bromination times and higher amounts of linkers on the surface afforded long-term stability. The protein adsorption and bacteria attachment of the PP-PG films were studied. Their extremely low amine content proved to be beneficial for preventing bacteria attachment.
A two-step separation procedure for the quantification of Pd and Pt in automotive exhaust emissions using isotope dilution mass spectrometry was established using a combination of cation and anion exchange chemistry. AG 50W-X12 was used as cation exchange resin and DGA as weakly basic anion exchange resin. This procedure enabled the effective separation of Pd and Pt from the matrix and from interfering elements. Additionally Pd and Pt were collected in separate chromatographic fractions, which increased the precision of the isotope ratio determination by separate measurements using single collector sector field ICPMS. The analytical procedure was validated by analysing the synthetically prepared samples and the certified reference materials BCR-723 (road dust) and IAEA-450 (algae). For the SI-traceable results complete uncertainty budgets were calculated yielding relatively expanded uncertainties (k = 2) of ≈1% for analyte masses in the ng range. Procedure blanks of 55 pg Pd and 3 pg Pt were obtained. The detection limits were calculated as 12 pg for Pd and 7 pg for Pt. Additionally, Pd and Pt blank levels of different filter materials are presented as well as the first results for automotive exhaust particles collected on cellulose filters.
Beim Abreißen von Flaschenventilen an Atemluftflaschen wird schlagartig sehr viel Energie frei. Im Beitrag wird auf Unfälle im Zusammenhang mit Atemschutzgeräten, welche gerade nicht im Einsatz verwendet werden, eingegangen. Es wird beschrieben, welche die häufigsten Fehler bei der Handhabung solcher Geräte sind, was im schlimmsten Fall passieren kann und an welchen Stellen welche Maßnahmen ergriffen werden sollten, um die Unfallfolgen zu begrenzen bzw. den Unfall zu vermeiden.
Effective cleanup of groundwater contaminated with radionuclides using permeable reactive barriers
(2015)
The mining of natural resources always causes environmental impacts such as land use, large quantities of waste, destruction of habitat, impairment of groundwater regime, and quite possibly contamination of soil, water, or air (Dudka and Adriano 1997). The environmental impact of mining cannot be estimated easily. The concept of total material requirement (TMR) is an attempt to quantify the environmental impact of materials. TMR is the sum of domestic and imported primary natural resources and their hidden flows (Adriaanse et al. 1997). Hidden flows are often not considered in environmental analyses because they are attributed with no cost. However, overburden from mining, earth moving for construction, and soil erosion are major sources of ecological damage. From the mining of minerals to the final products, a number of process steps take place (exploration, mine site development, extraction, milling, washing, concentration, smelting, refining, fabrication), each step being connected to other input flows such as energy or other resources. The hidden flows for metals related to metal ore mining have been investigated by Halada et al. (2001). Table 9.1 lists the data for some metals, together with the data for some other minerals and fuels. The TMR in the United States in the 1990s was between 80 and 100 tonnes per capita; in the European Union (EU-15) approximately 50 tonnes per capita (Bringezu 2002).
In order to assess the anisotropy-related uncertainties of relatively determined photoluminescence quantum yields (ΦPL) of molecular emitters and luminescent nanomaterials, we compared ΦPL values measured without and with polarizers using magic angle conditions and studied systematically the dependence of the detected emission intensity on the polarizer settings for samples of varying anisotropy. This includes a dispersion of a spherical quantum dot (QD) with an ideally isotropic emission, a solution of a common small organic dye in a fluid solvent as well as dispersions of elongated quantum dot rods (QDR) with an anisotropic luminescence and a small organic dye in a rigid polymeric matrix, as ideally anisotropic emitter. Our results show that for instruments lacking polarizers, anisotropy-related measurement uncertainties of relative photoluminescence quantum yields can amount to more than 40%, with the size of these systematic errors depending on the difference in emission anisotropy between the sample and the standard.
Mit einer neuartigen analytischen Zentrifuge können Klebverbindungen, Beschichtungen und Kompositwerkstoffe untersucht werden. Die Idee der Wissenschaftler an der BAM Bundesanstalt für Materialforschung und -prüfung: Die Proben müssen nicht mehr eingespannt, sondern nur noch eingesteckt werden. Durch das einfache Einstecken der Prüfkörper ist eine sehr schnelle Beladung möglich. Zudem können bis zu acht Proben gleichzeitig unter identischen Bedingungen geprüft werden. Konventionelle Zugprüfmaschinen waren und sind nur in der Lage, einen (eingespannten) Probekörper zu testen. Das von BAM-Forschern bereits 2004 zum Patent angemeldete Funktionsprinzip wurde seitdem von der Berliner LUM GmbH als Lizenznehmer zum marktreifen Produkt weiterentwickelt.
Radiologic evaluation techniques are nondestructive testing (NDT) used to detect the bulk of explosives and contraband materials in large objects. As compared to conventional low-energy (<450 key) X-ray imaging, high-energy (>1 MeV) digital X-ray radiography is required for the NOT of large containers because of the need for high penetration through thick materials, sensitivity, and the ability to distinguish between low-and high-Z materials. Mobile, high-energy, and high-resolution radiologic techniques are useful to detect contraband and threat materials in digital radiographic images of containers with complex packing. This paper presents a mobile, high-energy X-ray radiographic technique for the in-field nondestructive inspection of cargo containers. The developed experimental technique consisted of a betatron as a high-energy (7.5 MeV) X-ray source and a high-resolution (400 mu m) matrix detector for the digital X-ray imaging. In order to evaluate the detection efficiency and image quality of the measurement technique, a test specimen was proposed that was made of a 3 mm thick steel container with an inner dimension of 60 x 30 x 40 cm(3) comprising different low-and high-Z materials. Image quality indicators were used to assess the essential image quality parameters such as image basic spatial resolution, effective attenuation coefficient, and signal-to-noise ratio (SNR). Experimental investigations were performed on a 6.1 m sea freight container with mockup dangerous materials in complex packing. Preliminary experimental results showed that the proposed technique was able to distinguish between liquids and solids, as well as detect contraband materials. Furthermore, a remarkable SNR of 400 was achieved in the measured digital X-ray images. The influence of temperature on X-ray radiation dose rate at different X-ray energies was also investigated. Finally, important applications of the proposed technique in the context of maritime security are discussed.
In den Untersuchungen zum Zündvermögen von Filmeffektzündern wurde nachgewiesen, dass diese einen Plastiksprengstoff auf Basis von PETN nicht zu einer detonativen Umsetzung anregen können. Die Erfüllung der grundlegenden Sicherheitsanforderung (ESR) des Anhanges 1 der Richtlinie 2013/29/EG und die Kategorisierung als pyrotechnischer Gegenstand für Theater (T2) kann somit als gegeben angesehen werden, da der verwendete Explosivstoff zur Gruppe der sensibelsten Sprengstoffe (Initiierung mit geringen Zündenergien) gehört. Es wurde weiterhin nachgewiesen, dass der Untemassertest nach DIN EN 13763 Teil 15 aussagekräftige Ergebnisse liefert, welche die Fähigkeit von Filmeffektzündern und vergleichbaren pyrotechnischen Gegenständen bestätigen respektive widerlegen, einen Sekundärsprengstoff zu zünden (eine Detonation zu initiieren).
Für eine allgemeine Einschätzung des Zündvermögens von Filmeffektzündern und vergleichbaren pyrotechnischen Gegenständen ist ein Grenzbereich für ein äquivalentes Zündvermögen in g PETN auf Basis der Experimente mit dem o. g. Unterwassertest bestimmt worden. Filmeffektzünder und vergleichbare pyrotechnische Gegenstände sind nicht in der Lage, einen Sekundärsprengstoff zur Detonation anzuregen, wenn das aus dem Unterwassertest ermittelte äquivalente Zündvermögen unter 0,25 g PETN liegt.
Auswirkungen von Ermüdungsbeanspruchungen auf Struktur und Eigenschaften von Fahrbahndeckenbeton
(2015)
Ausgehend von der Zielsetzung der DFG-Forschergruppe 1498, die Einflüsse auf den AKR-Schädigungsprozess in Fahrbahndecken aus Beton grundlegend zu klären, sind zwei aufeinander aufbauende Untersuchungsschwerpunkte Gegenstand dieses Beitrags. Im ersten Schwerpunkt wurden die prüftechnischen Voraussetzungen für die Charakterisierung der Degradation und damit der Rissbildung im Fahrbahndeckenbeton durch die Vorschädigung infolge von Ermüdungsbeanspruchungen geschaffen. Realisiert wurde dies durch die Implementierung und Optimierung eines Monitoringsystems im zyklischen 4-Punkt-Biegeversuch zur simultanen Erfassung der Rissbildung im großformatigen Schwingbalken. Zusätzlich wurde die Röntgen-3D-Computertomografie für die hochauflösende räumliche quantitative Rissanalyse in den Bohrkernen aus den Schwingbalken ohne und mit Vorschädigung weiterentwickelt. Im zweiten Untersuchungsschwerpunkt wurde mittels vielfältiger Experimente an kleinformatigen Probekörpern aus dem Schwingbalken gezeigt, dass durch die Ermüdungsbeanspruchung die bruchmechanischen Materialkennwerte des Betons zum Teil eine signifikante Veränderung erfahren. Based on the objective of the DFG (German research foundation) funded research group 1498 to clarify the influences on the ASR damage process, this paper deals with two focuses of investigation. In the first focus the technical requirements for the characterisation concerning the degradation and the formation of cracks in concrete pavements by the pre-damage as a result of fatigue loading were created. This was realized by the implementation and the optimisation of a monitoring system in the cyclic four point bending test to capture simultaneously the formation of cracks in the beam under sinusoidal bending load. In addition, the X-ray 3D-computed tomography was enhanced for the high-resolution quantitative spatial crack analysis in the drilling cores extracted of the beam under sinusoidal bending load without and with a pre-damage. Building on the first focus, in the second focus of investigation a significant change of the fracture-mechanical properties of the concrete as a result of fatigue loading has been demonstrated in numerous experiments using small specimens extracted from the beam under sinusoidal bending load.
This paper presents a new X-ray backscatter technique (XBT) for non-destructive imaging of aerospace materials with only a single-sided access. It uses a special twisted slit collimator to inspect the whole object by changing the viewing direction of the X-ray backscatter camera. For the first time, the X-ray backscatter measurements were conducted using high-energy (>500 keV) X-ray sources. Experiments were performed on thick complex structured aluminium components, stringers and honeycomb structures to validate the applicability of the present technique to image small changes in the material properties and also to detect low-density material inclusions. In order to reduce the inspection time from hours to several seconds and to improve the image quality of the X-ray backscatter image, the backscattered signals were measured using a digital detector array with high spatial resolution (200 µm). The influence of the energy of the X-ray source and the slit width of the camera on the X-ray backscatter image were also investigated. In the proposed technique, the whole object is irradiated by an un-collimated X-ray beam resulting in a low image acquisition time of 3 min that facilitates the use of XBT for the real time NDT&E of aerospace materials.
Sicherstellung des Korrosionsschutzes durch werkstoffgerechte Verarbeitung nichtrostender Stähle
(2015)
The ground vibrations, which are generated by trains on different tracks, have been calculated by finite-element boundary-element models. The ballasted track is modelled in detail by the finite element method. The infinite soil is modelled by the boundary element method as a homogeneous or layered half-space. The track-soil system is coupled to a simple rigid mass model of the vehicle so that the vehicle-track interaction is completely included. Transfer functions are calculated in frequency domain without and with vehicle-track interaction, the compliance of the track and the mobilities of the soil at different distances from the track. Finally, the ratios between the ground vibration amplitudes with and without mitigation measures are calculated to quantify the effectiveness of the mitigation measures.
Tracks with under-sleeper pads have been investigated in a wide parameter study for the RIVAS project. The main parameters that influence the reduction of ground vibration are the stiffness of the under-sleeper pad, the mass and the width of the sleeper. The softest sleeper pad yields the best reduction of the ground vibration. The influence of the sleeper mass is not so strong, as the characteristic frequency is ruled by the mass of the sleeper and the mass of the wheelset as well.
Behavior of dust/air mixtures is very complex and difficult to predict since it depends on material properties as well as boundary conditions. Without other influences airborne particles deposit due to gravity but the time it takes for total deposition as well as easiness of resurrection depends very much on the specific dust sample and the boundary conditions. It still lacks a complete understanding of all interacting reasons and one approach is using experimentally determined characteristics, one is named dustiness.
Dustiness is the tendency of dust to form clouds and to stay airborne. Dustiness is determined with two basic principles, which are light attenuation and ratio of filled-in and measured mass. Assessment of dustiness of industrial powders has been done for a long time regarding work place safety. Dustiness is used there to determine inhalable fraction and to evaluate health risks. Lately it became interesting in dust explosion protection as well. Dustiness could be used to optimize determination of zones, adaption of venting area and/or for positioning of suppression systems.
Dustiness can be useful in many ways but is not a physical property of dusts, therefore it depends on material properties such as density, particle size distribution, shape and water content as well as boundary conditions or determination method. This makes it very difficult to compare dustiness for different techniques and apparatuses and determination method as well as results should be considered carefully. This work gives an overview of existing standards, recent research and suggests improvements to the new dustiness as proposed for dust explosion protection.
Pd/TiO2 coatings with template-controlled mesopore structure as highly active hydrogenation catalyst
(2015)
Micro-structured reactors offer excellent mass and heat transport capabilities and can therefore sustain very high reaction rates and space–time-yields also for highly exothermic catalytic reactions. However, such high rates cannot be reached when the reactors are coated or filled with conventional catalysts powders. We present a strategy for the direct synthesis of highly active wall-coated supported catalysts via co-deposition of a pore template (here micelles formed from PEO-b-PPO-b-PEO) and a precursors for the metal oxide (TiCl4) along with a compatible precursor for the active metal (PdCl2). The obtained catalytic coatings possess a template-controlled open pore structure and excellent mechanical stability. Moreover, the active metal is highly dispersed and well-distributed across the coating also at high Pd loadings. The corresponding high activity along with rapid mass transfer enabled by the open pore system results in the best space–time-yields in the gas-phase hydrogenation of butadiene reported so far in literature for a supported catalyst.
The hepatotoxin phomopsin A (PHO-A), a secondary metabolite mainly produced by the fungus Diaporthe toxica, occurs predominantly on sweet lupins. Along with the growing interest in sweet lupins for food and feed commodities, concerns have been raised about fungal infestations, and consequently, about the determination of PHO-A.
High performance liquid chromatography coupled to tandem mass spectrometry (LC-MS/MS) represents the most suitable analytical technique for sensitive and selective detection of mycotoxins including PHO-A. However, isotopic labeled substances are needed as internal standards for a reliable and convenient quantification.
As no isotope standard for PHO-A is currently available, a biosynthesis of fully 15N6-labeled PHO-A was established by cultivation of D. toxica on defined media containing Na15NO3 and 15N-labeled yeast extract as the only nitrogen sources. The identity of 15N6-PHO-A was confirmed by high resolution mass spectrometry.
The new 15N6-labeled standard will facilitate the method development for PHO-A including a more accurate quantification by LC-MS/MS.
Für Spannstähle muss im Rahmen der Überwachung die Beständigkeit gegenüber Spannungsrisskorrosion nach DIN EN ISO 15630-3 nachgewiesen werden. Die Stähle werden hierbei entweder einer konzentrierten Ammoniumthiocyanatlösung oder einer verdünnten Lösung, die eher die Verhältnisse in der Baupraxis wiedergibt, ausgesetzt. In den vergangenen Jahren gab es an Spannstäben der Festigkeitsklasse St 950/1050 immer wieder Probleme mit dem Erreichen der erforderlichen Standzeiten in der konzentrierten Lösung. Der Ringversuch sollte nun klären, inwieweit Unsicherheiten hinsichtlich der Zuverlässigkeit und Aussagekraft der Ergebnisse von Spannungsrisskorrosionsprüfungen bestehen. Außerdem sollten die Prüfanweisungen, die Prüfeinrichtungen sowie die Vor-Ort-Inspektion der Prüfstände kritisch beurteilt werden, um eventuell vorhandene versuchstechnische Probleme zu identifizieren und ggf. zu beheben.
Basics of statistic
(2015)
Austenitic stainless steels provide a beneficial combination of chemical and mechanical properties and have been used in a wide field of applications for over 100 years. Further improvement of the chemical and mechanical properties was achieved by alloying nitrogen. But the solubility of N within the melt is limited and can be increased in substituting Ni by Mn and melting under increased pressure. In order to avoid melting under pressure and decrease production costs, a part of N can also be substituted by C. This leads to austenitic high interstitial steels (AHIS). Within the solution annealed state strength and ductility of AHIS is comparable or even higher of those of AHNS and can be further improved by cold working. Unfortunately the endurance limit does not follow this trend as it is known from cold-worked austenitic CrNi steels. This is due to the differences of the slip behavior which is governed by the stacking fault energy as well as other near field effects. Construction components operating under cyclic loads over long periods of time cannot be considered being free of voids or even cracks. Thus the crack propagation behavior is of strong interest as well. This contribution presents the tensile, fatigue, crack propagation and fracture toughness properties of AHNS and AHIS in comparison to those of CrNi-steels. The differences are discussed in relation to microstructural characteristic as well as their alterations under cyclic loading.
In Betonbauteilen unter gleichzeitiger zyklischer Beanspruchung und externer Alkalizufuhr ist die Gefahr von Schäden infolge oder unter Mitwirkung einer Alkali-Kieselsäure-Reaktion (AKR) besonders hoch. Dies betrifft insbesondere Fahrbahndecken, bedingt durch den zunehmenden Schwerlastverkehr und den winterlichen Auftrag des Enteisungsmittels NaCl. Speziell die Rolle einer mechanischen Vorschädigung des Betons infolge der Verkehrsbeanspruchungen auf den Ablauf einer AKR ist dabei aber noch nicht in ausreichendem Umfang geklärt. Ein Teil der dazu seit 2012 durchgeführten Untersuchungen im Rahmen der DFG-Forschergruppe 1498 soll im Folgenden vorgestellt werden. Es zeigte sich, dass eine AKR in definiert mechanisch vorgeschädigten Betonprobekörpern mit alkalireaktiven Gesteinskörnungen und unter äußerer Alkalizufuhr vor allem früher beginnt als in äquivalenten Probekörpern ohne Vorschädigung. Grund dafür ist das schnellere und tiefere Eindringen von Wasser und insbesondere gelöstem NaCl in den Beton, wodurch Na-Ionen als Reaktionspartner für eine AKR früher und langfristig auch in größerer Menge verfügbar sind.------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------
In concrete elements, simultaneously subjected to cyclic loadings and external alkalis, the risk for damages caused by or under participation of an alkali-silica reaction (ASR) is particularly high. This concerns especially concrete pavements due to the increasing heavy load traffic and the wintry application of NaCl deicer. Notably the role of a mechanical pre-damage of concrete caused by traffic loadings on the course of the ASR is largely unclear. A part of the investigations that has been conducted since 2012 into this issue within the scope of the DFG (German research foundation) funded research group 1498 shall be introduced in the following. It was evident that an ASR in defined mechanically pre-damaged concrete prisms with alkali-reactive aggregates and under an external supply of alkalis started earlier than in equal prisms without a pre-damage. The reason for this is the faster and deeper ingress of water and particularly of dissolved NaCl into the concrete, by what Na ions as reaction partner for an ASR are available earlier and, in the long-term, in greater amounts too.
The adsorption of porphyrin derivatives on a Au(111) surface was studied by scanning tunneling microscopy and spectroscopy at low temperatures in combination with density functional theory calculations. Different molecular appearances were found and could be assigned to the presence of single gold adatoms bonded by a coordination bond underneath the molecular monolayer, causing a characteristic change of the electronic structure of the molecules. Moreover, this interpretation could be confirmed by manipulation experiments of individual molecules on and off a single gold atom. This study provides a detailed understanding of the role of metal adatoms in surface–molecule bonding and anchoring and of the appearance of single molecules, and it should prove relevant for the imaging of related molecule–metal systems.
Die "Empfehlungen für die Beförderung gefährlicher Güter, Handbuch über Prüfungen und Kriterien" ergänzen die "Empfehlungen für die Beförderung gefährlicher Güter, Modellvorschriften" und das "Global harmonisierte System zur Einstufung und Kennzeichnung von Chemikalien (GHS)". Sie enthalten Kriterien, Prüfmethoden und –verfahren, die angewendet werden sowohl für die Einstufung gefährlicher Güter nach den Vorschriften der Teile 2 und 3 der Modellvorschriften als auch für Chemikalien, von denen nach dem GHS physikalische Gefahren ausgehen.
Bright emitters with photoluminescence in the spectral region of 800–1600 nm are increasingly important as optical reporters for molecular imaging, sensing, and telecommunication and as active components in electrooptical and photovoltaic devices. Their rational design is directly linked to suitable methods for the characterization of their signal-relevant properties, especially their photoluminescence quantum yield (Φf). Aiming at the development of bright semiconductor nanocrystals with emission >1000 nm, we designed a new NIR/IR integrating sphere setup for the wavelength region of 600–1600 nm. We assessed the performance of this setup by acquiring the corrected emission spectra and Φf of the organic dyes Itrybe, IR140, and IR26 and several infrared (IR)-emissive Cd1-xHgxTe and PbS semiconductor nanocrystals and comparing them to data obtained with two independently calibrated fluorescence instruments absolutely or relative to previously evaluated reference dyes. Our results highlight special challenges of photoluminescence studies in the IR ranging from solvent absorption to the lack of spectral and intensity standards together with quantum dot-specific challenges like photobrightening and photodarkening and the size-dependent air stability and photostability of differently sized oleate-capped PbS colloids. These effects can be representative of lead chalcogenides. Moreover, we redetermined the Φf of IR26, the most frequently used IR reference dye, to 1.1 × 10-3 in 1,2-dichloroethane DCE with a thorough sample reabsorption and solvent absorption correction. Our results indicate the need for a critical reevaluation of Φf values of IR-emissive nanomaterials and offer guidelines for improved Φf measurements.
We present a systematic study on the effect of surface ligands on the luminescence properties and colloidal stability of β-NaYF4:Yb3+,Er3+ upconversion nanoparticles (UCNPs), comparing nine different surface coatings to render these UCNPs water-dispersible and bioconjugatable. A prerequisite for this study was a large-scale synthetic method that yields ~2 g per batch of monodisperse oleate-capped UCNPs providing identical core particles. These ~23 nm sized UCNPs display an upconversion quantum yield of ~0.35% when dispersed in cyclohexane and excited with a power density of 150 W cm-2, underlining their high quality. A comparison of the colloidal stability and luminescence properties of these UCNPs, subsequently surface modified with ligand exchange or encapsulation protocols, revealed that the ratio of the green (545 nm) and red (658 nm) emission bands determined at a constant excitation power density clearly depends on the surface chemistry. Modifications relying on the deposition of additional (amphiphilic) layer coatings, where the initial oleate coating is retained, show reduced non-radiative quenching by water as compared to UCNPs that are rendered water-dispersible via ligand exchange. Moreover, we could demonstrate that the brightness of the upconversion luminescence of the UCNPs is strongly affected by the type of surface modification, i.e., ligand exchange or encapsulation, yet hardly by the chemical nature of the ligand.
Critical review of the determination of photoluminescence quantum yields of luminescent reporters
(2015)
A crucial variable for methodical performance evaluation and comparison of luminescent reporters is the photoluminescence quantum yield (Φ pl). This quantity, defined as the number of emitted photons per number of absorbed photons, is the direct measure of the efficiency of the conversion of absorbed photons into emitted light for small organic dyes, fluorescent proteins, metal–ligand complexes, metal clusters, polymeric nanoparticles, and semiconductor and up-conversion nanocrystals. Φ pl determines the sensitivity for the detection of a specific analyte from the chromophore perspective, together with its molar-absorption coefficient at the excitation wavelength. In this review we discuss different optical and photothermal methods for measuring Φ pl of transparent and scattering systems for the most common classes of luminescent reporters, and critically evaluate their potential and limitations. In addition, reporter-specific effects and sources of uncertainty are addressed. The ultimate objective is to provide users of fluorescence techniques with validated tools for the determination of Φ pl, including a series of Φ pl standards for the ultraviolet, visible, and near-infrared regions, and to enable better judgment of the reliability of literature data.
Two-color double-fs-pulse experiments were performed on silicon wafers to study the temporally distributed energy deposition in the formation of laser-induced periodic surface structures (LIPSS). A Mach-Zehnder interferometer generated parallel or cross-polarized double-pulse sequences at 400 and 800 nm wavelength, with inter-pulse delays up to a few picoseconds between the sub-ablation 50-fs-pulses. Multiple two-color double-pulse sequences were collinearly focused by a spherical mirror to the sample. The resulting LIPSS characteristics (periods, areas) were analyzed by scanning electron microscopy. A wavelength-dependent plasmonic mechanism is proposed to explain the delay-dependence of the LIPSS. These two-color experiments extend previous single-color studies and prove the importance of the ultrafast energy deposition for LIPSS formation.
Development of a multi-VOC reference material for quality assurance in materials emission testing
(2015)
Emission test chamber measurement is necessary to proof building materials as sources of volatile organic compounds (VOCs). The results of such measurements are used to evaluate materials and label them according to their potential to emit harmful substances, polluting indoor air. If only labelled materials were installed indoors, this would improve indoor air quality and prevent negative impacts on human health. Because of the complex testing procedure, reference materials for the quality assurance are mandatory. Currently, there is a lack of such materials because most building products show a broad variation of emissions even within one batch. A previous study indicates lacquers, mixed with volatile organic pollutants, as reproducible emission source for a wide range of substances. In the present study, the curing of the lacquer-VOC mixture inside micro-chambers was optimised. Therefore, the humidity and the chamber flow were varied. Typical indoor air pollutants with a wide range of volatilities, for example, styrene, n-hexadecane, dimethyl and dibutyl phthalate were selected. It turned out that, under optimised curing parameters inside the micro-chamber, their emission can be reproduced with variations of less than 10 %. With this, a next important step towards a reference material for emission testing was achieved.
Fukuda et al. published a paper (Scripta Mater. 68 (2013) 984–987) in which they claimed to be able to determine the isothermal nature of the martensitic transformation in a Ti–Ni alloy. They analyzed the evolution of electrical resistance during isothermal holding stages and concluded that the variations were a consequence of the isothermal transition between austenite and martensite. In the following we will demonstrate that the discussed data do not allow the interpretation presented and that the isothermal nature is not proved.
Sulphurous additives for polystyrene: Influencing decomposition behavior in the condensed phase
(2015)
The thermal decomposition behaviour of polystyrene (PS) containing sulphur and phosphorus additives was investigated, using thermogravimetry coupled with Fourier transform infrared spectroscopy (TGA-FTIR). It was found that the additives influence the decomposition process of the polymer in the condensed phase, resulting in a decrease in styrene monomer formation and an increase in styrene oligmer derivatives. Via reference measurements with binary mixtures it was found that the presence of sulphur additives influences the radicalic decomposition process of PS. In combination with quantum chemical calculations it was concluded that this is due to the formation of radicals that abstract hydrogen from the polymer matrix at lower temperatures, disfavouring the radicalic decomposition pathway leading to styrene.
The effect of structural constriction on molecular mobility is investigated by broadband dielectric spectroscopy (BDS) within three types of molecular arrangements: monomers, oligomers and self-assembled monolayers (SAMs). While disordered monomers exhibit a variety of cooperative and local relaxation processes, the constrained nanodomains of oligomers and highly ordered structure of monolayers exhibit much hindered local molecular fluctuations. Particularly, in SAMs, motions of the silane headgroups are totally prevented whereas the polar endgroups forming the monolayer canopy show only one cooperative relaxation process. This latter molecular fluctuation is, for the first time, observed independently from other overlapping dielectric signals. Numerous electrostatic interactions among those dipolar endgroups are responsible for the strong cooperativity and heterogeneity of the canopy relaxation process. Our data analyses also revealed that the bulkiness of dipolar endgroups can disrupt the organization of the monolayer canopy thus increasing their ability to fluctuate as temperature is increased.
An approach is presented to model elastic waveguides of arbitrary cross-section coupled to infinite solid media. The formulation is based on the scaled boundary-finite element method. The surrounding medium is approximately accounted for by a dashpot boundary condition derived from the acoustic impedances of the infinite medium. It is discussed under which circumstances this approximation leads to sufficiently accurate results. Computational costs are very low, since the surrounding medium does not require discretization and the number of degrees of freedom on the cross-section is significantly reduced by utilizing higher-order spectral elements.
Epoxy carbon-fibre prepreg, Hexcel Type 6376 HTS, was investigated using Dynamic Mechanical Analysis (DMA). The DMA characteristic parameters are storage modulus E', loss modulus E' and loss factor tanδ. These parameters are ideally suited to observe the vitrification, referred to as glass transition, resulting from the cross-linking reaction. Detection of the cure state may also be achieved by determining the momentary glass transition temperature of partially cured samples. The consequent use of a multi-frequency measuring regime was used to derive the apparent activation energy for the glass transition process. Different temperature programs were also applied to monitor the curing process directly, as well as to investigate the different states of incomplete cure reached in preceding curing steps. The intention was to provide better understanding of the consequences of an interrupted autoclave curing process and to use DMA to detect the cure state achieved. With DMA, the continuation of an incomplete curing process also can be monitored. DMA measurements up to 300 °C showed, furthermore, that the final glass transition temperature was reduced by thermal degradation at high temperatures.
The objects of this investigation were sculptures taken from a ca. three hundred years old baroque epitaph of a church in Tonning, a town in Northern Germany. Around 1900 it was found in a disastrous state heavily damaged by wood-worm. At that time, the whole artwork was treated with the tar extract carbolineum as a remedy. Nowadays, this substance has been identified as carcinogenic, and its presence can be perceived by its stench and visually at certain spots on the surface where it has penetrated the covering paint.
A gold-painted sculpture of a massive wooden skull was interrogated with X-rays and fast neutrons to investigate the internal distribution of the carbolineum. The X-ray tomography, with its excellent spatial resolution revealed galleries left over from the worm infestation in the outer areas and cracks in the central region. The golden color coating appeared as a thick and dense layer. In comparison the tomography with fast neutrons, though being of lower resolution and yet unresolved artefacts revealed sections of slightly different densities in the bulk of the wood. These differences we attribute to the differences in the distribution of the impregnant in the wood, visible due to its higher hydrogen content making it less transparent for neutrons.
ISO standards for gas cylinders made from aluminum alloys generally require heat treatment after the forming process. Such heat treatment is a costly part of the manufacturing process. Particularly due to increasing international trade, market-surveillance authorities need simple and reliable methods to field-test cylinders for proper heat treating. By the present contribution the difference in strength of heat-treated and non-heat-treated gas cylinders is exemplarily shown and several material analysis methods are investigated for their suitability as field tests.
This article presents an analytical approach for simulation of ultrasonic diffracted wave signals from cracks in two-dimensional geometries based on a novel Huygens–Fresnel Diffraction Model (HFDM). The model employs the frequency domain far-field displacement expressions derived by Miller and Pursey in 2D for a line source located on the free surface boundary of a semi-infinite elastic medium. At each frequency in the bandwidth of a pulsed excitation, the complex diffracted field is obtained by summation of displacements due to the unblocked virtual sources located in the section containing a vertical crack. The time-domain diffracted wave signal amplitudes in a general isotropic solid are obtained by standard Fast Fourier Transform (FFT) procedures. The wedge based finite aperture transducer refracted beam profiles were modelled by treating the finite dimension transducer as an array of line sources. The proposed model is able to evaluate back-wall signal amplitude and lateral wave signal amplitude, quantitatively. The model predicted range-dependent diffracted amplitudes from the edge of a bottom surface-breaking crack in the isotropic steel specimen were compared with Geometrical Theory of Diffraction (GTD) results. The good agreement confirms the validity of the HFDM method. The simulated ultrasonic time-of-flight diffraction (TOFD) A-scan signals for surface-breaking crack lengths 2 mm and 4 mm in a 10 mm thick aluminium specimen were compared quantitatively with the experimental results. Finally, important applications of HFDM method to the ultrasonic quantitative non-destructive evaluation are discussed.
A software prototype is developed for assessing and updating the reliability of single-cell prestressed concrete box girders subjected to chloride-induced reinforcement corrosion. The underlying system model consists of two integrated sub-models: a condition model for predicting the deterioration state of the box girder and a structural model for evaluating the overall system reliability. The condition model is based on a dynamic Bayesian network (DBN) model which considers the spatial variation of the corrosion process. Inspection data are included in the calculation of the system reliability through Bayesian updating on the basis of the DBN model. To demonstrate the effect of partial inspections, the software prototype is applied to a case study of a typical highway bridge with six spans. The case study illustrates that it is possible to infer the condition of uninspected parts of the structure due to the spatial correlation of the corrosion process.
First developments of a new test to evaluate the fire behavior of photovoltaic modules on roofs
(2015)
A new test for photovoltaic (PV) modules exposed to an external fire source on roofs is proposed, and first results are presented. This is a simplification of the standards commonly in use for testing PV modules as roofing parts, roofing components or building components. Most of the tests required different fire scenarios and the use of burning brands such as wood cribs. In our study we proposed replacing wooden burning brands with a propane burner, the output of which is close to the one that can be observed in the burning of wooden cribs 500 g and 2 kg in size. The fire behavior was assessed by measuring smoke evolution, burning drips, flaming debris, and the time to burn-through of monocrystalline, polycrystalline and amorphous silicon panels. Two different configurations of the burner were tested, with the fire source on the top of the module or under the tilted module, respectively. The fire behavior of the modules was dependent on the burner output (16 to 46 kW), but also on the construction type of the panel (glass/glass or glass/plastic sheet) and on the position of the fire source (top or bottom). These preliminary tests for further development of the procedure yielded encouraging results for the evaluation of PV panels on roofs.
The aim of this study was the development of a low volume air sampling strategy for biocides and polychlorinated biphenyls (PCB) at low air change rates in modern, air-tight showcases as they are present in museums. Lindane, pentachlorophenol, dichlofluanid, tolyfluanid, isodrin, p,p-dichlorodiphenyl trichloroethane and permethrin were the biocides and PCB 28 and PCB 153 were the PCBs studied, all of which are semi volatile organic compounds (SVOC). Their occurrences in the museum environment originate from various sources e.g. preventive treatment of organic exhibits or organic building materials. Exhibits are long-term exposed to these pollutants due to storing in showcases or other storage equipment at low air change rates. To achieve air sampling under the aforementioned conditions the influences of temperature, air circulation, air change rate and relative humidity on the emission behavior of the selected biocides and PCBs had to be determined. This was carried out with pre-soaked wood samples in low volume air sampling experiments using 27 L test showcases and 23 L and 24 L emission test chambers and also diffusive sampling with glass as the sampling material.
The pore structure of lightweight granules made from masonry rubble was studied in order to better understand their engineering properties. Thermally and hydrothermally hardened granules were tested. Analysis by ESEM, mercury porosimetry and sorption methods yield important insight into their microstructure. The thermal granules are characterised by partly melted vitreous areas and large internal macropores that are connected via narrow throats. They show a marginal specific surface area along with a hydrophobic behaviour. In contrast, the hydrothermal granules have an accessible mesoporous system containing plate-like and ink-bottle pores. The shape of their water isotherms depending on the granules CaO content is sensitive to the morphology of calcium silicate hydrate phases (CSH). The hysteresis changes from a narrow loop that closes at low pressures, which can be attributed to coarser more crystalline CSH, to a large triangular-shaped loop along with a low pressure hysteresis, which is characteristic for fine fibre-like CSH with ink-bottle and plate-like pore morphologies. Granules with fibre-like CSH have the higher specific surfaces areas but those with more crystalline CSH show stronger physisorption of water molecules.
The aim of the joint project ViPQuali (Virtual Product Qualification) was to describe a components ageing behaviour in a given environment, by numerical simulation.
Having chosen polypropylene (PP) as the material, which does not show sensitivity to moisture, the relevant weathering parameters of the doseresponse functions could be limited to spectral irradiance and temperature.
In artificial irradiation tests, for PP plates of varied stabiliser content, spectral sensitivity as well as temperature dependence of irradiation-caused crack formation was quantified. For that purpose, samples were exposed both to artificial weathering tests at various constant temperatures and to spectrally resolved irradiation. The temperature dependence could be modelled by an Arrhenius fit. For fitting the spectral sensitivity, a plateau function was chosen. Subsequently, the stabiliser content was parameterised and extrapolated.
The formed dose–response functions were incorporated into a Computational Fluid Dynamics (CFD) software program, simulating the environment of a sample within a Phoenix-exposed IP/DP (Instrument Panel/Door Panel box) box, based on sun position and weather conditions, including radiation interactions. Observed local effects as well as the general ageing advance of PP hats are compared with respect to simulation and experiment.
Resulting from this project, for this most simple example of PP of varied stabiliser content, the time to failure can be estimated for each weathering exposure environment with known time-resolved irradiance and temperature conditions.
NbC has a relatively high hardness (19.6 GPa) and melting temperature (3600 °C) and is usually applied as a grain growth inhibitor in WC–Co hardmetals. The current study reports on the influence of the sintering technology and overall chemical composition on the microstructure and mechanical properties of NbC-based hardmetals, using Co as a binder. The partial replacement of NbC by 5 wt.% WC, Mo2C, VC or TiC allows one to significantly improve the hardness and toughness of the NbC–Co materials. The influence of different binders, i.e., Co, 316L stainless steel and Fe3Al on the microstructure and mechanical properties of NbC-based hardmetals was also investigated. The powder mixtures were sintered in the solid state by PECS and liquid state by conventional vacuum sintering. Detailed microstructural analysis was conducted by EPMA elemental mapping and WDS point analysis. Mechanical properties, including Vickers hardness and indentation toughness were assessed.