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Organisationseinheit der BAM
- 4 Material und Umwelt (38)
- 7 Bauwerkssicherheit (29)
- 8 Zerstörungsfreie Prüfung (22)
- 4.5 Kunst- und Kulturgutanalyse (16)
- 3 Gefahrgutumschließungen; Energiespeicher (15)
- 6 Materialchemie (13)
- 7.5 Technische Eigenschaften von Polymerwerkstoffen (12)
- 5 Werkstofftechnik (11)
- 8.2 Zerstörungsfreie Prüfmethoden für das Bauwesen (10)
- 1 Analytische Chemie; Referenzmaterialien (9)
Methoden der Dauerüberwachung von Gebäuden des kulturellen Erbes im Rahmen der Denkmalkonservierung
(2012)
Infrared thermography
(2012)
Near-IR femtosecond (fs) (pulse duration = 150 fs, wavelength = 775 um, Repetition rate 1 kHz) and VUV nanosecond (ns) (pulse duration = 20 ns, wavelength = 157 nm, repetition rate 1 to 5 Hz) laser pulse ablation of single-crystalline TeO? (c-Te02) surfaces was performed in air using the direct focusing technique. A multi-method characterization using optical microscopy, atomic force microscopy and scanning electron microscopy revealed the surface morphology of the ablated craters. This allowed us at each irradiation site to characterize precisely the lateral and vertical dimensions of the laser-ablated craters for different laser pulse energies and number of laser pulses per spot. Based on the obtained information, we quantitatively determined the Ablation threshold fluence for the fs laser irradiation when different pulse numbers were applied to the same spot using two independent extrapolation techniques. We found that in the case of NIR fs laser pulse irradiation, the ablation threshold significantly depends on the number of laser pulses applied to the same spot indicating that incubation effects play an important role in this material. In the case of VUV ns laser pulses, the ablation rate is significantly higher due to the high photon energy and the predominantly linear absorption in the material. These results are discussed on the basis of recent models of the interaction of laser pulses with dielectrics. In the second part of this chapter, we use timeof-flight mass spectrometry (TOFMS) to analyze the elemental composltion of the ablation products generated upon laser irradiation of c-Te02 with single fs- (pulse duration ~ 200 fs, wavelength 398 nm) and ns-pulses (pulse duration 4 ns, wavelength 355 nm). Due to the three Order of magnitude different peak intensities of the ns- and fs laser pulses, significant differences were observed regarding the laser-induced species in the plasma plume. Positive singly, doubly and triply charged Te ions (Te+, Te2+, Te3+) in the form of many different isotopes were observed in case of both irradiations. In the case of the ns-laser ablation, the TeO+ formation was negligible compared to the fs case and there was no Te trimer (Te3+) formation observed. It was found that the amplitude of Te ion Signals strongly depends on the applied laser pulse energy. Singly charged Oxygen ions (0+) are always present as a byproduct in both kinds of laser ablation.
Near-IR femtosecond (fs) (pulse duration = 150 fs, wavelength = 775 nm, repetition
rate 1 kHz) and VUV nanosecond (ns) (pulse duration = 20 ns, wavelength = 157 nm,
repetition rate 1 to 5 Hz) laser pulse ablation of single-crystalline TeO2 (c-TeO2 ) surfaces
was performed in air using the direct focusing technique. A multi-method
characterization using optical microscopy, atomic force microscopy and scanning
electron microscopy revealed the surface morphology of the ablated craters. This allowed
us at each irradiation site to characterize precisely the lateral and vertical dimensions of
the laser-ablated craters for different laser pulse energies and number of laser pulses per
spot. Based on the obtained information, we quantitatively determined the ablation
threshold fluence for the fs laser irradiation when different pulse numbers were applied to
the same spot using two independent extrapolation techniques. We found that in the case
of NIR fs laser pulse irradiation, the ablation threshold significantly depends on the
number of laser pulses applied to the same spot indicating that incubation effects play an
important role in this material. In the case of VUV ns laser pulses, the ablation rate is
significantly higher due to the high photon energy and the predominantly linear
absorption in the material. These results are discussed on the basis of recent models of the
interaction of laser pulses with dielectrics. In the second part of this chapter, we use time-
of-flight mass spectrometry (TOFMS) to analyze the elemental composition of the
ablation products generated upon laser irradiation of c-TeO2 with single fs- (pulse
duration ~200 fs, wavelength 398 nm) and ns-pulses (pulse duration 4 ns, wavelength
355 nm). Due to the three order of magnitude different peak intensities of the ns- and fs
laser pulses, significant differences were observed regarding the laser-induced species in
the plasma plume. Positive singly, doubly and triply charged Te ions (Te+, Te2+, Te3+) in
the form of many different isotopes were observed in case of both irradiations. In the case
of the ns-laser ablation, the TeO+ formation was negligible compared to the fs case and
there was no Te trimer (Te3+) formation observed. It was found that the amplitude of Te
ion signals strongly depends on the applied laser pulse energy. Singly charged oxygen
ions (O+) are always present as a byproduct in both kinds of laser ablation.
Messtechnik und Sensorik
(2011)
In a future energy supply system based on renewable sources hydrogen technology will play a key role. Because the amount of energy from renewable sources, such as wind or solar power, differs seasonally and regionally, an energy storage method is necessary.
Hydrogen, as an environmentally friendly energy carrier, can fill this gap in an ideal way, in particular for mobile applications (Wurster et al., 2009). Already today, in Germany the amount of hydrogen as a byproduct in chemical industry is enough for fuelling about 1 Mio passenger cars1. Excess electrical power can be used to produce hydrogen by electrolysis. On demand, this hydrogen can be used for mobile or stationary fuel cells. Beside this new developing technology, hydrogen is used as fuel for rocket engines and in chemical industry since a long time. Table 1 comprises some physical parameters of hydrogen. It can be seen that hydrogen gas has a very low density which makes storage at high pressure or in liquid form (LH2) necessary.
In aeronautic and space engineering, safety is a major aspect. Periodical inspections by different non-destructive testing (NDT) techniques are performed to assess the structural integrity. The accuracy of such inspection is high ly dependent on the skills of the technician. To be more efficient automated procedures independent of human decision are needed. The costs for such inspections are also significant as they require immobilisation of aircrafts. Alternative on-line structural health monitoring (SHM) procedure capable to detect, acquire, and identify damage should permit important cost reductions but also safety increase from real-time damage assessment. The increasing application of composite materials in modern aircrafts and spacecrafts permits the development of such procedure from the embedment of sensors and actuators in the structure during manufacturing.
The introduction of an innovative process for non-destructive testing is described in terms of its different phases and how the process is controlled in the Fraunhofer IZFP in order to obtain optimal results. Examples are discussed of applications by IZFP in various important and safety-relevant industrial sectors where the automated inspection systems were introduced. These case studies include the inspection of railway components such as the wheel sets of the German high-speed train and in-line pipe inspection by using intelligent pipeline inspection gauges. Complex inspection systems, both hardware and software, developed in partnership with the Federal Institute for Materials Research and Inspection (BAM), were applied to inspection tasks in civil engineering. Two automated systems based on a robot and on a flexible manipulation are presented. Both systems can be applied to diverse inspection technologies and to the data fusion of various types of non-destructive testing (NDT) data.
Globalisation of both science and trade has increased the relevance of the comparability of measurement data whether in research, industry or regulatory contexts. Reference materials (RMs) are essential tools in the quest for comparable and reliable measurement results, a quest which laboratories, worldwide, are tasked with every day. An explicit acknowledgement of the importance of RMs in todays measurement systems is found, for instance, in the laboratory accreditation standards, such as ISO/IEC 17025.
Schäden an Bauwerksoberflächen wie Risse, Ablösungen, Feuchte, Bewuchs (Moose, Flechten, Pilze usw.) und Krustenbildung werden zurzeit hauptsächlich durch konventionelle Verfahren, wie z.B. Sichtprüfung und manuelle Vermessung, erfasst. Zur Sicherung des kulturellen Erbes werden jedoch dringend moderne und effiziente Verfahren und Strategien für eine vorbeugende Instandhaltung benötigt, die mit geringeren Kosten häufigere Inspektionen ermöglichen. Auch Wachstum und Alterung des Gebäudebestands verschärfen die Situation zunehmend, Da eine detaillierte 3-D-Darstellung und wiederholte Beobachtung insbesondere von Rissen und Ablösungen u.a. auch für die sicherheitsrelevante Einschätzung der
Standsicherheit eines Gebäudes eine sehr große Rolle spielen, wurden in den letzten Jahren laserbasierte Messverfahren weiterentwickelt und eingesetzt, Diese ermöglichen eine schnelle und automatisierte Erfassung der Oberflächengeometrie und können zudem innerhalb vorgegebener Zeitintervalle wiederholt eingesetzt werden. Das Verfahren kann auch durch eine zusätzliche Aufnahmetechnik ergänzt werden, die eine Zuordnung von erfassten Farbwerten zu den 3-D-Messpunkten erlaubt.
Lehm ist ein seit Jahrtausenden bewährter, weit verbreiteter und heute ein moderner Baustoff. Für vordringliche Bauaufgaben in der Altbausanierung, dem energieeffizienten Neubau sowie dem Bauen in Entwicklungs- und Schwellenländern ist Lehm hervorragend geeignet. Der Baustoff Lehm ist zu einem Material für anspruchsvolle Bauvorhaben geworden. Seine Ästhetik und Ausstrahlung, seine Wirkung für Raumklima und Wohlbefinden werden von vielen Menschen geschätzt. Besonders zukunftsrelevant sind die umweltspezifischen Eigenschaften des Materials, z.B. die unerreichbar günstige Energiebilanz vieler Lehmbaustoffe. Lehmsteine werden im Neubau überwiegend für die Ausmauerung von Holzständerkonstruktionen verwendet (Bild 1). Die Anwendung für tragende Wände ist derzeit noch untergeordnet, gewinnt aber an Bedeutung.
In der Altbausanierung und Denkmalpflege wird Lehm als historisch authentischer Baustoff und aufgrund seiner bauphysikalischen Qualitäten vielfältig eingesetzt.
Plasmapolymerisation
(2010)
Fallbeispiele für die Anwendung der 3D-Messtechnik und der aktiven Thermografie in der Denkmalpflege
(2010)
Solar energy has been transformed into useful redox differences or disequilibria within the Earth´s crust since the onset of anoxygenic and oxygenic photosynthesis in the Precambrian. Inorganic oxidized carbon is transformed into reduced carbon compounds by capturing and storing solar energy. During this process, many different organic compounds are formed including carbohydrates, proteins, hydrocarbons, and various other complex organic metabolic products and their diagenetic polymerization products (melanin, humic substances, petroleum, coal, and kerogen). Many of these solar energy-enriched compounds, however, are oxidized immediately or during the diagenetic transformation of sediments. The oxidation agents are oxygen, sulfate, iron, and other oxidized compounds, which in turn are partly enriched with the original solar energy. On a global biogeochemical scale, however, sulfur and iron are the most important elements. Geological evidence shows that biogeochemical cycles tend to yield stable ratios between the most oxidized forms of carbon (carbon dioxide and calcium/magnesium carbonate) and the most reduced forms (diamond, coal, methane, and hydrocarbons). Throughout the Earths history and evolution, this equilibrium ratio is around 1:4, maximally 1:5. When too much carbon is stored in the crust in the form of reduced compounds or vice versa, climatic and biogeomorphogenetic consequences upset the equilibrium. The biosphere reacts in a way to return to the optimal ratio. Excellent examples for this fluctuating equilibrium are the Carboniferous (too much organic carbon stored), the Permian (too little organic carbon stored), and the Tertiary with a generally equivalent production of hydrocarbons and carbonates. At present, we are in a period in which there is a global biogeochemical need to oxidize reduced carbon compounds as fast as possible in order to avoid even more dramatic global climate shifts. The highly evolved human genome seems to be the tool for this shift. Enormous amounts of reduced carbon are turned into the oxidized form as carbon dioxide, which by various biogeochemical pathways is quickly transformed into carbonate, another oxidized form of carbon that can be stabilized and stored in the sedimentary record. Fast recycling of excessively stored solar energy may enable the survival of a global biosphere under highly stressed conditions.
This chapter provides an overview of methods that are commonly used for the analysis of the original water content of fresh and hardened concrete. The methods consist of direct methods, which detect the water content or the water/cement ratio primarily, as well as indirect methods, which measure other material characteristics related to the water content.
Die Verträglichkeit von metallischen Behälterwerkstoffen und wassergefährdenden Flüssigkeiten
(1991)
Safety measures
(1995)
Zuverlässige Bestimmung von Chloridgehalten bei der Instandsetzung tausalzgeschädigter Bauwerke
(2010)
Pigmentveränderung
(2009)
The construction process of the New Berlin Main Station, the former Lehrter Bahnhof, has been monitored from the beginning. In this station, the main European east-western railway connection crosses the northsouth railway lines. Four east-western bridges, built in the first construction phase, carry the platforms for international lines and suburban train tracks. The outer two bridges carry the supports of the relatively flat glass roof, too. Since the glass roof is very sensitive to vertical displacements, the authorities required a complex monitoring system. This case study describes long-term measurements with classical and enhanced innovative sensors to monitor vertical displacements of neighboring glass roof supports. Additionally, traditional strain gauges were embedded parallel to long-gauge length fiber-optic strain sensors in the near-surface concrete of the partial prestressed bridges to reliably survey possible changes.
The measurements on site go along with long-term laboratory tests on prestressed concrete beams. Researchers study load effects and long-term environmental influences on two large-scale model beams, inside and outside the laboratory.
The monitoring system has been working stable as an early warning system for any changes of the structural conditions since 2002. All data are available on line for both the project team and the owner.
Catalyst characterization
(2009)
JATROPHA - The Seed of Energy - CO2-Neutral Fuels and Lubricants Based on Sustainable Non-Food Oils
(2009)
Verfahrensvalidierung und Ergebnisunsicherheit am Beispiel der Spannkraftermittlung in Spannstählen
(2008)
Fiber Optic Sensors
(2006)
Meßtechnik und Sensorik
(2007)
Messtechnik
(2001)
Prüfung
(1979)
Ergebnisse der Tintenanalyse
(2005)
Baustoffe
(2002)
Smart technical textiles are by definition textiles that can interact with their environment.
They can sense and react to environmental conditions and external stimuli from mechanical, thermal, chemical or other sources. Such textiles are multifunctional or even “intelligent” which is fulfilled by a number of sensors incorporated in the textiles. The embedded sensors are sensitive to various parameters such as temperature, strain, chemical, biological and other substances.