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Since the TEM has the capacity to observe the atomic structure of materials, in-situ TEM synthesis methods are uniquely suited to advance our fundamental understanding of the bottom-up dynamics that drive the formation of nanostructures. E-beam induced fragmentation (potentially identified as a manifestation of Coulomb explosion) and electron stimulated desorption (ESD) are phenomena that have received attention because they trigger chemical and physical reactions that can lead to the production of various nanostructures. Here we report a simple TEM protocol implemented on WO2.9 microparticles supported on thin amorphous carbon substrates. The method produces various nanostructures such as WC nanoparticles, WC supported films and others. Nevertheless, we focus on the gradual graphitization and gasification of the C substrate as it interacts with the material expelled from the WO2.9 microparticles. The progressive gasification transforms the substrate from amorphous C down to hybrid graphitic nanoribbons incorporating W nanoparticles. We think these observations open interesting possibilities for the synthesis of 2D nanomaterials in the TEM.
Gut kombiniert: Laser-Plasma-Auftragschweißen
Für den Schutz vor starkem abrasiven Verschleiß (Panzern) oder vor korrosiven Medien (Plattieren) sowie für das Auftragen einer Pufferlage können das Laser-Pulver-Auftragschweißen oder das Plasma-Pulver-Auftragschweißen zum Einsatz kommen. Während das Laser-Pulver-Auftragschweißen eine geringe thermische Belastung verspricht, ermöglicht das Plasma-Pulver-Auftragschweißen hohe Auftragraten. Wissenschaftler des Fraunhofer IPK erarbeiten neuartige Verfahrenskombinationen und Düsenkonzepte, die die jeweiligen Vorteile dieser bestehenden Verfahren vereinen und somit eine hohe Qualität und Effizienz garantieren. So kann beispielsweise die punktgenaue Energie der Laserstrahlung den Plasmalichtbogen stabilisieren und den Wärmeeintrag in das Bauteil besser kontrollieren.
Plasma-Transferred-Arc (PTA) welding is a process that enables high deposition rates, but also causes increased thermal load on the component. Laser metal deposition (LMD) welding, on the other hand, reaches a high level of precision and thus achieves comparatively low deposition rates, which can lead to high processing costs. Combining laser and arc energy aims to exploit the respective advantages of both technologies. In this study, a novel approach of this process combination is presented using a PTA system and a 2 kW disk laser. The energy sources are combined in a common process zone as a high-speed plasma laser cladding technology (HPLC), which achieves process speeds of 10 m/min at deposition rates of 6.6 kg/h and an energy per unit length of 39 J/mm.