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Alloy modification and ultrasonic assisted milling of wear resistant alloys with defined surfaces
(2023)
The targets for reducing CO2 emissions are closely linked to the development of highly efficient and economical steel components in plant, process and power plant technology, which require wear protection coatings tailored to the application and steel material for high combined corrosive, tribological, thermal and mechanical stresses. In addition to increasing demands to replace conventional cobalt alloys with nickel alloys as a result of price and supply risks, there is a growing demand in industry for defined functional surfaces of high quality for these coatings. Milling is a standard process for finish machining. The desired properties of wear resistant alloys imply significant challenges for the milling process due to high tool wear and surface defects. Besides the hardness of the coating materials, especially due to the precipitations, inhomogeneous, anisotropic weld structures of the claddings lead to further deteriorations of milling processes due to unstable milling conditions and process forces.
A joint project of BAM and ISAF of TU Clausthal (Fosta P1550/IGF 21959 N) investigates the optimization of these challenging machining conditions by means of alloy modifications of the welding powder for plasma transferred arc cladding, without reducing the wear protection potential and using ultrasonic assisted milling process.
In this paper, the influence of the microstructure and precipitation morphology adjusted by means of alloy modification on machining is investigated. The alloy used is a NiCrMoSiFeB alloy (trade name: Colmonoy 56 PTA). Through metallurgical investigations and in-situ measurement of cutting forces and temperatures at the cutting edge during the milling process as well as the subsequent investigation of tool wear and surface integrity, a detailed analysis and correlation between microstructural properties and machinability is feasible. The findings allow recommendations for standards and processing guidelines, enabling safe and economical production of highly stressed steel components with non-critical, cost-reduced materials.
Alloy 36 (1.3912), also known as “Invar”, is an alloy with 36% nickel. It was developed in 1897 by Guillaume and stands out for its very low thermal expansion coefficient. It is classified as a difficult-to-cut material and is commonly used for the production of fiber-reinforced composites in the field of mold construction. Additive manufacturing (AM) offers many economic advantages regarding the repair, modification and manufacture of entire components. Subsequent machining of the AM components is necessary to account for complex structures, final contours or defined surfaces. This is usually done using a tool with a geometrically defined cutting edge, i.e., milling processes. Surface integrity is determined by metallurgical (e.g., microstructure of the subsurface), topological (e.g., surface defects, roughness) and mechanical (e.g., residual stresses) factors, which is crucial in terms of component safety and performance. Modern, hybrid cutting processes, such as ultrasonic-assisted milling (US), provide potentially improvement of the cutting situation of these components.
In part I of this investigation, the initial alloy 36 is modified with the elements Ti, Zr and Nb up to a maximum of 1 wt.-%. The influence of the modification elements on the microstructure as well as on the hardness of the AM components is examined. Part II focusses on the effect of the alloy modifications on machinability as well as on the surface integrity of plasma-transferred-arc-welded (PTA) and finish milled invar components.
The results show a significant positive influence of ultrasonic assistance on the resulting cutting force of both materials. The modification with 1% Ti shows a positive influence on the surface integrity, as the roughness of the conventional machining processes is lower compared to the initial alloy, which has to be confirmed in further experiments.
Alloy 36 (1.3912), also known as “Invar”, is an alloy with 36% nickel. It was developed in 1897 by Guillaume and stands out for its very low thermal expansion coefficient. It is classified as a difficult-to-cut material and is commonly used for the production of fiber-reinforced composites in the field of mold construction. Additive manufacturing (AM) offers many economic advantages regarding the repair, modification and manufacture of entire components. Subsequent machining of the AM components is necessary to account for complex structures, final contours or defined surfaces. In part I of this investigation, the initial alloy 36 is modified with the elements Ti, Zr and Hf up to a maximum of 0.33 wt.-%. The influence of the modification elements on the microstructure as well as on the hardness of the AM components is examined. Part II focusses on the effect of the alloy modifications on machinability as well as on the surface integrity of plasma-transferred-arc-welded (PTA) and finish milled invar components. Machining tests were carried out, to investigate the influence of ultrasonic assistance and the effects of modification elements Ti, Zr and Hf on the occurring cutting forces, temperatures and resulting surface integrity of the AM components made of alloy 36 and their modifications. The results show a significant positive influence of ultrasonic assistance on the resulting cutting force as well as on the roughness of all materials investigated.
Alloy 36 (1.3912) is an alloy with 36% nickel and 64% iron and is generally classified as a difficult-to-cut material. Increasingly complex structures and the optimization of resource efficiency are making additive manufacturing (AM) more and more attractive for the manufacture or repair of components. Subsequent machining of AM components is unavoidable for its final contour. By using modern, hybrid machining processes, e.g., ultrasonic-assisted milling (US), it is possible to improve the cutting situation regarding the resulting surface integrity as well as the cutting force. Part I deals with the influence of the alloying elements Ti, Zr, and Hf on the microstructure and the hardness of the initial alloy 36. Part II focusses on the effect of the alloy modifications and the ultrasonic assistance on machinability as well as on the surface integrity after finish-milling. The results show a highly significant influence of the ultrasonic assistance. The cutting force during the US is reduced by over 50% and the roughness of approx. 50% compared to conventional milling (CM) for all materials investigated. Moreover, the US causes a defect-free surface and induces near-surface compressive residual stresses. CM leads to a near-surface stress state of approx. 0 MPa.
Ni alloys are generally classified as difficult-to-cut materials and cost intensive. Additive manufacturing (AM) offers economic advantages. However, machining of these AM components is mandatory to create the final contour or surface. The inhomogeneous and anisotropic microstructure and properties of AM components causes an unstable cutting process. Moreover, undesirable tensile residual stresses are generated due to subsequent machining. In this investigation, the initial alloy 36 is modified with Ti and Nb up to 1.6 wt.-% and build-up welded via gas metal arc welding (GMAW) and plasma-transferred-arc (PTA). Then, finish-milling tests are carried out to investigate the influence of the modification as well as the cutting parameters on the resulting cutting force and the surface integrity. In addition, the conventional milling process (CM) is compared with the ultrasonic-assisted milling process (US), which has a significant influence on the machinability as well as on the surface integrity.
Ni alloys are generally classified as difficult-to-cut materials and cost intensive. Additive manufacturing (AM) offers economic advantages. However, machining of these AM components is mandatory to create the final contour or surface. The inhomogeneous and anisotropic microstructure and properties of AM components causes an unstable cutting process. Moreover, undesirable tensile residual stresses are generated due to subsequent machining. In this investigation, the initial alloy 36 is modified with Ti and Nb up to 1.6 wt.-% and build-up welded via gas metal arc welding (GMAW) and plasma-transferred-arc (PTA). Then, finish-milling tests are carried out to investigate the influence of the modification as well as the cutting parameters on the resulting cutting force and the surface integrity. In addition, the conventional milling process (CM) is compared with the ultrasonic-assisted milling process (US), which has a significant influence on the machinability as well as on the surface integrity.
This presentation summarizes the latest results on the BAM-Themenfeld project SURDIA on processing of high-entropy alloys (HEAs) at BAM. At first, the influence of machining by ultrasonic-assisted milling on the surface integrity is presented. Second, the weld processing by Tungsten Inert Gas (TIG) welding is presented and the results of the Friction Stir Welding (FSW), which is conducted at BAM for the first time.
Co-Cr alloys are frequently used for highly stressed components, especially in turbine and plant construction, due to their high resistance to thermal and mechanical stress, as well as to corrosive and abrasive loads. Furthermore, they are classified as difficult-to-cut materials because of their high strength and toughness as well as their low thermal conductivity. However, for Co, an increased cost and supply risk can be observed in recent years. Therefore, additive manufacturing (AM) offers significant economic advantages due to higher material efficiency regarding repair, modification, and manufacturing of such components. Concerning inhomogeneity and anisotropy of the microstructure and properties as well as manufacturing-related stresses, a lot of knowledge is still necessary for the economic use of additive welding processes in SMEs. In addition, subsequent machining, particularly contour milling, is essential to generate the required complex contours and surfaces. Hence, additive and machining manufacturing processes need to be coordinated in a complementary way, especially due to additional challenges arising in milling of heterogeneous hard-to-cut microstructures. Recently, it has been shown that modern, hybrid cutting processes, such as ultrasonic-assisted milling (US), can improve the cutting situation. In this investigation, the Co-Cr initial alloy is additionally modified with Ti and Zr up to 1 wt.-% with the aim to enhance the homogeneity of the microstructure and, thus, the machinability. Hence the investigation includes finish milling tests of the AM components and the comparison of US and conventional machining. Both the modifications and the ultrasonic assistance exhibit a significant effect on the machining situation, e.g., US causes a higher surface integrity of the finish milled surfaces compared to conventional milling.
Co-Cr alloys are frequently used for highly stressed components, especially in turbine and plant construction, due to their high resistance to thermal and mechanical stress, as well as to corrosive and abrasive loads. Furthermore, they are classified as difficult-to-cut materials because of their high strength and toughness as well as their low thermal conductivity. However, for Co, an increased cost and supply risk can be observed in recent years. Therefore, additive manufacturing (AM) offers significant economic advantages due to higher material efficiency regarding repair, modification, and manufacturing of such components. Concerning inhomogeneity and anisotropy of the microstructure and properties as well as manufacturing-related stresses, a lot of knowledge is still necessary for the economic use of additive welding processes in SMEs. In addition, subsequent machining, particularly contour milling, is essential to generate the required complex contours and surfaces. Hence, additive and machining manufacturing processes need to be coordinated in a complementary way, especially due to additional challenges arising in milling of heterogeneous hard-to-cut microstructures. Recently, it has been shown that modern, hybrid cutting processes, such as ultrasonic-assisted milling (US), can improve the cutting situation. In this investigation, the Co-Cr initial alloy is additionally modified with Ti and Zr up to 1 wt% with the aim to enhance the homogeneity of the microstructure and, thus, the machinability. Hence the investigation includes finish milling tests of the AM components and the comparison of US and conventional machining. Both the modifications and the ultrasonic assistance exhibit a significant effect on the machining situation; for example US causes a higher surface integrity of the finish milled surfaces compared to conventional milling.
The long-term global goals of achieving almost net zero carbon emissions in the next decades are closely linked to the development of highly efficient components in plant, process and energy engineering, and their sustainable and resource-saving production. Plant components must increasingly withstand tribological loads in addition to high thermal, mechanical, and corrosive stresses. Such combined stresses demand high-performance alloys economically tailored to the application for wear protection and components produced as semi-finished products, via additive manufacturing (AM) or claddings via deposition welding. For instance, the protection of special components made of less cost-intensive materials, e.g., steel in process engineering for screw machines or exhaust gas separation, is feasible applying cost-intensive Ni- or Co-based hard-phase claddings.
Today an increasing number of above-mentioned applications demand precise finishing machining of components to ensure defined compact surfaces with a high integrity and complex contours. Contour milling is standard process for finishing machining of metals. Especially, the desired properties of wear resistant materials (e.g., high strength, hard precipitations) imply significant challenges for milling processes and tools, leading frequently to uneconomic milling conditions due to intolerable high tool wear and surface defects. Inhomogeneous, anisotropic weld structures due to cladding or AM of wear resistance alloys lead to further deteriorations of milling processes due to unstable milling conditions and process forces during chip removal.
To tackle these challenges, already several approaches exist, (1) to enhance machinability of the claddings by alloy modifications to specifically influence solidification and hard phases morphology (precipitation shape, size, distribution) and (2) to achieve significant improvements of the machining situation (e.g., increase of tool life and surfaces integrity) by means of modern hybrid machining processes such as ultrasonic-assisted milling. This contribution shows a comprehensive overview of recent results with these promising approaches for additively welded Ni- CoCr-alloys.