Ingenieurwissenschaften und zugeordnete Tätigkeiten
Filtern
Erscheinungsjahr
Dokumenttyp
- Beitrag zu einem Tagungsband (72) (entfernen)
Referierte Publikation
- ja (72) (entfernen)
Schlagworte
- Thermography (5)
- Additive manufacturing (4)
- Welding (4)
- Active thermography (3)
- Additive Manufacturing (3)
- FEM (3)
- Residual stress (3)
- Simulation (3)
- Ultrasound (3)
- Ageing (2)
Organisationseinheit der BAM
- 8 Zerstörungsfreie Prüfung (12)
- 8.0 Abteilungsleitung und andere (9)
- 9 Komponentensicherheit (7)
- 3 Gefahrgutumschließungen; Energiespeicher (4)
- 6 Materialchemie (4)
- 3.4 Sicherheit von Lagerbehältern (3)
- 8.5 Röntgenbildgebung (3)
- 9.4 Integrität von Schweißverbindungen (3)
- 5 Werkstofftechnik (2)
- 6.2 Material- und Oberflächentechnologien (2)
Nanotechnology is one of the key technologies of the 21st century. The exploitation of 'new' effects that arise from materials structured on the nano-scale has also been proposed successfully for flame retardancy of polymers since the end of the 90s. Of all of the approaches these include, at this time the use of nanocomposites offers the best potential for industrial application, also some other ideas are sketched, such as using electrospun nanofibers mats or layer-by-layer deposits as protection coatings, as well as sub-micrometer multilayer coatings as effective IR-mirrors. The general phenomena, inducing a flow limit in the pyrolysing melt and changing the fire residue, are identified in nanocomposites. Key experiments are performed such as quasi online investigation of the protection layer formation to understand what is going on in detail. The flame retardancy mechanisms are discussed and their impact on fire behaviour quantified. With the latter, the presentation pushes forward the state of the art. For instance, the heat shielding is experimentally quantified for a layered silicate epoxy resin nanocomposite proving that it is the only import mechanism controlling the reduction in peak heat release rate in the investigated system for different irradiations. The flame retardancy performance is assessed comprehensively illuminating not only the strengths but also the weak points of the concepts. Guidelines for materials development are deduced and discussed. Apart from inorganic fillers (layered silicate, boehmite, etc.) not only carbon nanoobjects such as multiwall carbon nanotubes, multilayer graphene and graphene are investigated, but also nanoparticles that are more reactive and harbor the potential for more beneficial interactions with the polymer matrix.
CONRAD-2 is an imaging instrument using low-energy (cold) neutrons. The instrument is installed at the end of a curved neutron guide which avoids the direct line of sight towards the reactor core. This ensures a very low background of high-energy neutrons and. photons at the sample position. The cold neutron beam provides a wavelength range which is suitable for phase-and diffraction-contrast imaging such as grating interferometry and Bragg edge mapping. The instrument is well suited for high resolution imaging due to the high efficiency of the very thin scintillators that can be used for the detection of cold neutrons. An instrument upgrade was performed recently as a part of an upgrade program for the cold neutron instrumentation at HZB. The parameters of the instrument as well as some research highlights will be presented.
In this paper we present results of our recent efforts to understand the mechanical interface behaviour of single-walled carbon nanotubes (CNTs) embedded in metal matrices. We conducted experimental pull-out tests of CNTs embedded in Pd or Au and found Maximum forces in the range 10 - 102 nN. These values are in good agreement with forces obtained from molecular Dynamics simulations taking into account surface functional Groups (SFGs) covalently linked to the CNT material. The dominant failure mode in experiment is a CNT rupture, which can be explained with the presence of SFGs. To qualify the existence of SFGs on our used CNT material, we pursue investigations by means of fluorescence labeling of surface species in combination with Raman imaging. We also report of a tensile test system to perform pull-out tests inside a transmission electron microscope to obtain in situ images of CNT-metal interfaces under mechanical loads at the atomic scale.
For pulse laser materials processing often optical step index and gradient index multimode fibers with core diameters ranging from 100 to 600 μm are used. The design of a high power fiber transmission system must take into account limitations resulting from both surface and volume damage effects. Especially, breakdown at the fiber end faces and self-focusing in the fiber volume critically influence the fiber performance. At least operation charts are desirable to select the appropriate fiber type for given laser parameters.
In industry-relevant studies the influence of fiber core diameter and end face preparation on laser-induced (surface) damage thresholds (LIDT) was investigated for frequently used all-silica fiber types (manufacturer LEONI). Experiments on preform material (initial fiber material) and compact specimens (models of the cladding and coating material) accompanied the tests performed in accordance with the relevant LIDT standards ISO 21254-1 and ISO 21254 2 for 1-on-1 and S-on-1 irradiation conditions, respectively. The relation beam diameter vs. LIDT was investigated for fused silica fibers. Additionally, laser-induced (bulk) damage thresholds of fused silica preform material F300 (manufacturer Heraeus) in dependence on external mechanical stress simulating fiber bending were measured. All experiments were performed with 10-ns laser pulses at 1064 and 532 nm wavelength with a Gaussian beam profile.
Earth, timber, fibre boards and insulation materials based on wooden and other natural fibres offer a variety of properties beneficial for eco innovative constructions that are able to improve the energy and resource efficiency of buildings.
Due to their porosity, natural building materials are vapour active and are able to buffer moisture. In combination with highly insulated and airtight but vapour permeable building envelopes, modern earth-timber constructions provide stable indoor humidity levels and can therefore be naturally ventilated while achieving highest energy efficiency standards. Experimental evidence suggests that monitored pilot buildings in Berlin do show healthy indoor air humidity levels (around 50%) in wintertime, while mechanically ventilated buildings demonstrate significantly lower values (around 25%), which have to be considered as uncomfortable and unhealthy.
The application of building materials being poor in chemical emissions, particularly volatile organic compounds (VOC) and radon, improves the indoor air quality further, so that intermittent ventilation twice a day will be sufficient to provide healthy indoor air quality. The air quality in critical rooms (e.g. small bedrooms), demonstrating a smaller air volume, should be monitored if appropriate ratios of room size to occupancy level cannot be realised.
Through night time ventilation in summer, vapour active earth-timber constructions provide evaporative cooling (humidity adsorption at night time and desorption during the day). As a result, indoor temperatures of earth-timber buildings range around 8 °C below the outside temperature peak, when an appropriate glazing ratio is reflected. The EU funded research project H-house is investigating various construction materials regarding water vapour adsorption as well as emission and absorption of harmful substances. Based on this investigation new wall constructions are designed to provide a healthier indoor environment.
The phenomenon of creep of structural steel in fire engineering is gaining more and more interest. Due to shortcomings of the EC3 constitutive model and other approaches based on classical creep theory an alternative approach mainly based on the ideas of Krempl is proposed. Due to this so-called operator approach the material as well as the constitutive model is looked upon as an operator. The application of this view serves as a guide through the analysis of the relationship between experimental facts and constitutive theory especially in the context of transient creep.
A fracture mechanics model which shall be applied to the fatigue strength determination of weldments has to focus on various aspects such as: (a) the description of mechanical and physical short fatigue crack extension which is characterised by yielding conditions which do not permit the application of the common ΔK concept and by the gradual build-up of the crack closure effect, (b) a consistent methodology for determining the initial crack size, (c) based on this, the determination of a fatigue limit, (d) the treatment of multiple crack propagation at load levels above this limit, (e) the variation of the local geometry along the weld toe, and (f) statistical effects.The paper gives alimited overview of the work the authors did in this field during the last years within the German project cluster IBESS. A model is presented and briefly discussed which covers the questions above.
Self-compacting concrete typically contains a higher content of powder materials than normal concrete. Furthermore it is assumed that the use of superplasticizers yields a more homogenous microstructure in the hardened paste. Both aspects generate a very dense microstructure, which can be assumed to cause material behaviour that differs from than normal concrete when it is exposed to elevated temperatures. However, the paste volumes in SCC can vary significantly based on the mixture composition. At a low paste volumes SCC can be very similar to normal concrete at hardened state while it can vary greatly at higher paste volumes. Since the high temperature behaviour of concrete is strongly affected by the different physical behaviour of the paste and the aggregates, it is likely that the high temperature behaviour is consequently strongly affected by the ratio of these mixture components. In the present study different SCC mixtures were observed with similar mechanical properties, but with significantly differing paste to aggregate ratios. Based on observations of the heat evolution at the fire exposed surface and at different depths inside the specimens as well as based on photogrammetric observations of the spalled dimensions, the results indicate that with increasing paste volumes the heat conductivity is reduced and as a result concrete with higher paste to aggregate ratios shows less spalling.
This work presents the use of limited experimental measurements to develop a set of calibrated Simulation parameters that can then be used for reliable simulation of subsea pipeline inspections. The modelling software aRTist is used as the simulation tool, and the calibration is through comparison with experimental images of a well characterised sample in a water tank. Image Quality parameters such as signal-to-noise ratio, contrast and basic spatial resolution are compared with the aim of matching simulated values to experimental results. Currently the model is partially calibrated, with signal-to-noise ratio successfully matched while differences are still found in contrast-to-noise ratio comparisons. This means that measurements depending on absolute intensity are not accurate enough in the simulation at this stage. However, the simulation is found to be accurate for wall thickness measurements in tangential images, which are not based on absolute intensity, with simulated and experimental cases producing similar results.
The method of movable cellular automata (MCA) and method of molecular dynamics (MD) were applied to simulate the friction and sliding behavior of model-tribofilms formed from a nanocomposite consisting of an epoxy matrix, 10 vol % micron-sized carbon fibers and 5 vol. % silica nanoparticles. Whereas MCA considered the tribofilm as an agglomerate of silica nanoparticles released from the composite and mixed with graphite particles, MD simulated the sliding behavior of an amorphous silica layer supported by stiff crystalline substrates on both sides. The MCA model provided reasonable quantitative results which corroborate experimental findings at moderate stressing conditions. The very low coefficient of friction observed experimentally under severe stressing conditions was not explained by this model. This could be attributed to the lack of mechanical data at the high temperature expected under these conditions. Although based on a simpler assumption of the tribofilm composition, MD-modelling could be easily applied to the expected high flash temperature and was able to predict friction reduction and smooth sliding under these conditions.