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Organisationseinheit der BAM
- 8 Zerstörungsfreie Prüfung (491) (entfernen)
The porosity and the surface roughness are recently discussed problems for SLM parts. The influence of SLM process parameters on porosity is well studied for different materials. Nevertheless, the build angle (i.e. the angle between part orientation and build plate) needs to be understood as an additional SLM process parameter, as it has been shown, that the microstructure and hence the mechanical performance of various materials depend on the build angle. The inherent build angle of each strut as a part of a lattice structure is the motivation to investigate the influence of the build angle on the porosity and roughness on round-shaped (1 mm diameter) struts by means of CT. Conventional Coordinate Measuring Machine (CMM) has the limitation towards small and round shaped samples. The need for Computed Tomography (CT) regarding investigations of SLM parts will increase because no other non-destructive technique allows the assessment of complex geometries with inner laying surfaces. We used CT to assess the pores and the strut surface. Seven struts out of the nickel alloy Inconel 625 with build angles from 30° to 90° were studied. It was found that the number of pores is smaller, and the size of pores is larger for the 90° strut. In case of 30° strut, the number of pores is increased towards down-skin side, additionally, this strut orientation showed to have the largest number of attached powder particles. The elongated pores exist exclusively near the strut surface. While the roughness at the down-skin surface is highly depending of the biud angle, the roughness at the up-skin surface is the same for all struts. The mechanisms of pore and surface roughness formation is not mainly driven by gravity.
Strong coupling effects in magnetocaloric materials are the key factor to achieve a large magnetic entropy change. Combining insights from experiments and ab initio calculations, we review relevant coupling phenomena, including atomic coupling, stress coupling, and magnetostatic coupling. For the investigations on atomic coupling, we have used Heusler compounds as a flexible model system. Stress coupling occurs in first‐order magnetocaloric materials, which exhibit a structural transformation or volume change together with the magnetic transition. Magnetostatic coupling has been experimentally demonstrated in magnetocaloric particles and fragment ensembles. Based on the achieved insights, we have demonstrated that the materials properties can be tailored to achieve optimized magnetocaloric performance for cooling applications.
Additive manufacturing (AM) opens the route to a range of novel applications. However, the complexity of the manufacturing process poses a challenge to produce defect-free parts with a high reliability. Since process dynamics and resulting microstructures of AM parts are strongly influenced by the involved temperature fields and cooling rates, thermography is a valuable tool for process monitoring. Another approach to monitor the energy input into the part during process is the use of optical tomography.
Common visual camera systems reach much higher spatial resolution than infrared thermography cameras, whereas infrared thermography provides a much higher temperature dynamic. Therefore, the combined application increases the depth of information. Here, we present first measurement results using a laser beam melting setup that allows simultaneous acquisition of thermography and optical tomography from the same point of view using a beam splitter. A high-resolution CMOS camera operating in the visible spectral range is equipped with a near infrared bandpass filter and images of the build plate are recorded with long-term exposure during the whole layer exposing time. Thus, areas that reach higher maximum temperature or are at elevated temperature for an extended period of time appear brighter in the images. The used thermography camera is sensitive to the mid wavelength infrared range and records thermal videos of each layer exposure at an acquisition rate close to 1 kHz.
As a next step, we will use computer tomographic data of the built part as a reference for defect detection.
This research was funded by BAM within the focus area Materials.
The thermoelectric properties of Sr1-xBixTiO3-δ (0 ≤ x ≤ 0.07) have been investigated. Dense ceramics of Sr1-xBixTiO3-δ and Sr0.95TiO3-δ have been prepared by solid-state reaction and conventional sintering in air followed by annealing in a reducing atmosphere. XRD and SEM analyses show that the rutile TiO2 in Sr0.95TiO3 formed after sintering becomes Magnéli phase of TinO2n-1 after annealing. Moreover, Bi resolves from Sr1-xBixTiO3 after annealing, resulting in the formation of Sr1-xBixTiO3-δ/Bi/TinO2n-1 composites. With increasing Bi content in Sr1-xBixTiO3-δ, the electrical conductivity increases while the absolute values of the Seebeck coefficient decrease as a result of increasing carrier concentration. The thermal conductivity of SrTiO3-δ is reduced by doping Bi up to x = 0.07. Highest ZT ~ 0.13 is obtained in Sr0.93Bi0.07TiO3-δ at 1000 K.
An increase in the thermal diffusivity of Fe2TiO5 is observed after only three cycles of measurement. X-ray refraction shows an increase in the mean specific surface. A segregation of Ca- and F-rich nanocrystals at grain boundaries is also observed by SEM and STEM-EDX. This emphasizes the importance of precursor purity and the influence of redistribution of impurities on thermoelectric properties.
Up to now THz-TDS-systems aren’t considered to be nondestructive testing facilities for large scale industrial applications, despite it was proven that they provide a comprehensive set of quality parameters. A practical approach to bring THz-TDS in addition to already existing testing systems into the industrial mainstream is systematic development of future test procedures and test facilities for dielectrics. For this purpose polyeth-ylene test specimen with introduced artefacts were designed, to evaluate the detection sensitivity of Time of Flight measurements based on dielectrics. SAFT reconstructed tomograms are presented which visualize the sizes and location of artificially introduced flaws.
In this paper we report on the characterization by X-ray computed tomography of calcium phosphate (CaP) and polycaprolactone (PCL) coatings on Ti-6Al-4V alloy scaffolds used as a material for medical implants. The cylindrical scaffold has greater porosity of the inner part than the external part, thus, mimicking trabecular and cortical bone, respectively. The prismatic scaffolds have uniform porosity. Surface of the scaffolds was modified with calcium phosphate (CaP) and polycaprolactone (PCL) by dip-coating to improve biocompatibility and mechanical properties. Computed tomography performed with X-ray and synchrotron radiation revealed the defects of structure and morphology of CaP and PCL coatings showing small platelet-like and spider-web-like structures, respectively.
Additive Manufacturing by Selective Laser Melting (SLM) offers an ample scope for producing geometrically complex parts as compared to the traditional subtractive manufacturing strategies. However, the residual stresses (RS) developed during the processing can reduce the load bearing capacity as well as induce unwanted distortion, limiting the life time and the application of SLM parts.
Die Untersuchung stellt eine Technologie einer Hochtemperatur-Ultraschallankopplung zwischen einem Lithiumniobat-Piezokristall und einer Elektrode aus rostfreiem Stahl dar. Die Ultraschallankopplung erfolgt durch das Diffusionslotprozess mit einem Aktivlot auf Silber-Kupfer-Basis.
Die beschriebene Technologie ermöglicht die Herstellung eines hochtemperaturbeständigen Ultraschallprüfkopf zum Dauereinsatz bis 600 °C.
Additive Manufacturing (AM) through the Selective Laser Melting (SLM) route offers ample scope for producing geometrically complex parts compared to the conventional subtractive manufacturing strategies. Nevertheless, the residual stresses which develop during the fabrication can limit application of the SLM components by reducing the load bearing capacity and by inducing unwanted distortion, depending on the boundary conditions specified during manufacturing.
The present study aims at characterizing the residual stress states in the SLM parts using different diffraction methods. The material used is the nickel based superalloy Inconel 718. Microstructure as well as the surface and bulk residual stresses were characterized. For the residual stress analysis, X-ray, synchrotron and neutron diffraction methods were used. The measurements were performed at BAM, at the EDDI beamline of -BESSY II synchrotron- and the E3 line -BER II neutron reactor- of the Helmholtz-Zentrum für Materialien und Energie (HZB) Berlin.
The results reveal significant differences in the residual stress states for the different characterization techniques employed, which indicates a dependence of the residual state on the penetration depth in the sample. For the surface residual stresses, longitudinal and transverse stress components from both X-ray and synchrotron agree well and the obtained values were around the yield strength of the material. Furthermore, synchrotron mapping disclosed gradients along the width and length of the sample for the longitudinal and transverse stress components. On the other hand, lower residual stresses were found in the bulk of the material measured using neutron diffraction. The longitudinal component was tensile and decreased towards the boundary of the sample. In contrast, the normal component was nearly constant and compressive in nature. The transversal component was almost negligible. The results indicate that a stress re-distribution takes place during the deposition of the consecutive layers. Further investigations are planned to study the phenomenon in detail.
In order to provide further evidence of damage mechanisms predicted by the solid-state transformation creep (SSTC) model, direct observation of damage accumulation during creep of Al–3.85Mg was made using synchrotron X-ray refraction (SXRR). X-ray refraction techniques capture the specific surface (i.e. surface per unit volume) with a field of view comparable to the specimen size but with microscopic sensitivity. A significant rise of the internal specific surface with increasing creep time was observed, providing evidence for the creation of a fine grain substructure, as predicted by the SSTC model.
We analyzed the results of high-energy X-ray CT scans for three 20×16×16 in. block samples of Indiana limestone from our recent radial acidizing experiments with HCl. CT scans were done for complete samples, and 3D images of internal dissolution patterns were built. Each 3D image consists of submillimeter-size voxels to capture fine details of individual wormholes.
The obtained 3D images of acidized blocks allow us to observe from various angles the details of the wormholes obtained in the three experiments, which demonstrated wide pore-volume-to-breakthrough (PVBT) range with three different injection rates. Also, variation of the CT number reveals the presence of depositional layers in all block samples, and the obtained CT images were used to interpret the effect that rock layers might have on wormhole penetration at different injection rates.
Further, the built voxel models were used to calculate the radial distributions of dissolved rock volume, which otherwise are not obvious for such complex branched structures as wormholes. We observed how varied experimental conditions affected those distributions. The radial distributions were found very similar across the samples, which suggested the way to detect the effective wormhole penetration depth.
THz-TDS Systeme können zeitaufgelöst die Amplitude der elektrischen Feldstärke E(t) detektieren. Der Vorteil des verwendeten Messprinzips besteht in dem gleichzeitigen Nachweis von Amplitude und Phase des zwischen der Antenne und dem Detektor sich ausbreitenden elektrischen Feldes eines Impulses. Befindet sich im Strahlengang dielektrisches Material, dann ändern sich die Laufzeit (Time of Flight) und Amplitude des Impulses im Vergleich zum freien Strahlengang.
Planare Fehlstellen, wie Risse oder delaminierte Schichten in Kompositen sowie mehrschichtig aufgebaute Dielektrika können als optische Mehrschichtsysteme aufgefasst werden, mit denen sich die beobachteten Transmissions- und Reflektionseigenschaften im THz-Bereich erklären lassen.
Bei Entwicklung eines optischen Schichtenmodells für das jeweilig ausgewählte Schichtensystem lassen sich zeitliche Impulsverläufe in Abhängigkeit von der Schichtenfolge- und deren –dicke berechnen.
Durch den Fit der experimentell gewonnener Daten mit den aus dem Schichtenmodell berechneten Impulssequenzen lassen sich unter Verwendung der Methode der kleinsten Quadrate Schichtdicken oder die Brechungsindizes der einzelnen Schichten im jeweiligen Testobjekt bestimmen. Anhand eines repräsentativen Beispiels wird die Entwicklung des Schichtenmodells erklärt und die erreichten Genauigkeiten zur Bestimmung der Schichtdicken und Brechungsindizes anhand selbst entwickelter Testkörper diskutiert.
During their life cycle, composite structures used in aircraft structures can be subjected to high- and low-velocity impact loading. High velocity impact damage is usually easy to detect as it creates visible external damage. Low-velocity impacts are more complex to assess because, although significant damage can be generated internally, there can be little indication of external damage on the impacted surface, leading to the term BVID. Impact damage, especially barely visible impact damage, is therefore of primary concern for design and maintenance of modern aircraft composite structures. As a result there is a concerted research effort to improve the damage resistance and tolerance of these materials.
One of the great strengths of X-ray computed tomography over conventional inspection methods (ultrasound, thermography, radiography) is that it can image damage in 3D. or inter-ply interfaces. An X-ray computed tomography (CT) data processing methodology is developed to extract the through-thickness distribution of damage in curved or deformed composite panels. The method is applied to [(0°/90°)2]s carbon fibre reinforced polymer (CFRP) panels subjected to low velocity impact damage (5 J up to 20 J) providing 3D ply-by-ply damage visualisation and analysis. Our distance transform approach allows slices to be taken that approximately follow the composite curvature allowing the impact damage to be separated, visualised and quantified in 3D on a ply-by-ply basis. In this way the interply delaminations have been mapped, showing characteristic peanut shaped delaminations with the major axis oriented with the fibres in the ply below the interface. This registry to the profile of the panel constitutes a significant improvement in our ability to characterise impact damage in composite laminates and extract relevant measurements from X-ray CT datasets.
Aktuell werden Prozessmonitoringsysteme in der additiven Fertigung (AM) zur Überwachung der Energiequelle, des Bauraums, des Schmelzbades und der Bauteilgeometrie zumindest im metallbasierten AM schon kommerziell angeboten. Weitere Verfahren aus den Bereichen der Optik, Spektroskopie und zerstörungsfreien Prüfung werden in der Literatur als geeignet für die in-situ Anwendung bezeichnet, es finden sich aber nur wenige Berichte über konkrete Umsetzungen in die Praxis.
Die Bundesanstalt für Materialforschung und -prüfung hat ein neues Projekt gestartet, dessen Ziel die Entwicklung von Verfahren des Prozessmonitorings zur in-situ Bewertung der Qualität additiv gefertigter Bauteile in AM-Prozessen mit Laser- bzw. Lichtbogenquellen ist. Verschiedene Verfahren der zerstörungsfreien Prüfung, wie Thermografie, optische Tomografie, optische Emissionsspektroskopie, Wirbelstromprüfung und Laminografie werden in verschiedenen AM-Prozessen zum Einsatz gebracht und die Ergebnisse fusioniert. Die evaluierten Ergebnisse werden mit Referenzverfahren wie Computertomografie und Ultraschall-Tauchtechnik verglichen. Ziel ist eine deutliche Reduzierung aufwändiger und zeitintensiver, zerstörender oder zerstörungsfreier Prüfungen nach der Fertigung des Bauteiles und zugleich eine Verringerung von Ausschussproduktion.
Hier wird das Projekt als Ganzes vorgestellt und der Fokus auf verschiedene Methoden der Temperaturmessung mit Hilfe der Thermografie gelegt. Anforderungen an die Messtechnik für verschiedene AM-Systeme werden diskutiert und erste experimentelle Ergebnisse werden präsentiert.
Modern and energy-efficient materials are essential for innovative designs for aerospace and automotive industries. Current technologies for rapid manufacturing such as additive manufacturing and liquid composite moulding by polymer Extrusion allow innovative ways of creating robust and lightweight constructions. Commercially available printing devices often use polylactide (PLA) or acrylonitrile butadiene styrene (ABS) as raw material. Therefore, parameters like the infill ratio, influencing the ability to resist mechanical stress, may have a beneficial impact on the lifetime of components.
These manufacturing technologies require a good knowledge about materials and even adapted non-destructive testing technologies and methods. Airborne ultrasonic testing has beneficial advantages for testing those lightweight constructions. It is a contact-free testing method, which does not require a liquid couplant. Therefore, it allows fast test cycles without any unwanted alternations of the material properties due to interactions with any coupling liquid. This contribution deals with the characterisation of printed specimens based on PLA by using airborne ultrasound and presents the current edge of non-destructive testing and evaluation using airborne ultrasonic transducers. The specimens, manufactured by polymer extrusion, are printed as thin plates. The infill ratio, as well as the material thickness, were varied to model density imperfections with different geometric shapes and properties. For better understanding of the limits of airborne ultrasonic testing in transmission, we compared own-developed transducers based on different physical principles: on ferroelectrets, on the thermoacoustic effect, as well as a new type of transducers based on gas discharges.
Es wird ein Verfahren zur Charakterisierung der Beständigkeit und
Langzeitstabilität von additiv gefertigten Kunststoff-Bauteilen vorgestellt. Dabei sollen die Prüfkörper über 2000 Stunden künstlich bewittert und währenddessen die Änderungen der Eigenschaften der Bauteile zerstörungsfrei untersucht werden.
THz and mid IR spectroscopy of high-molecular PE (HMW) and ultra high-molecular PE (UHMW) reveals modifications of the molecular structure. Characteristic absorption bands are changed if the two materials are exposed by -Co60 radiation up to 600 kGy and subsequently stored at an annealing temperature of 398 K until for 729 days. UHMW-PE and HMW-PE behave differently during the ageing process because of their molecular weight and inherent structure distinctions. The spectroscopic data offer characteristic absorption bands, which have been used to describe the complete ageing process in more detail. For instance, the integral absorption in the B1u THz-region can be used to describe quantitatively the reduction of crystallinity. The formation of trans vinylene unsaturation and the decay of vinyl during ageing can be observed in detail in the mid IR range.
Absorption edge tomography, also known as differential tomography at absorption edges, is a method which exploits the sudden change of the attenuation coefficient, when the photon energy crosses the absorption edge of an element. Synchrotron radiation is the best source for absorption edge tomography, because of its small bandwidth, high intensity and easily adjustable photon energy. The synchrotron beamline BAMline at the synchrotron radiation facility BESSY II in Berlin, which is operated by the Bundesanstalt für Materialforschung und -prüfung (BAM), provides a monochromatized beam in a photon energy range from 5 keV up to 80 keV with a bandwidth of 2%, when the double multilayer monochromator is used. Together with the microtomography setup, this enables differential tomography with submicron resolution at the K edge of the elements from chromium up to the lanthanides, and up to uranium, when the L edges are used as well.
In this work, metal organic frameworks (MOFs) embedded in polymer are characterized using differential tomography. MOFs are microporous structures of metal ions, coordinated by organic linker molecules, that can be used in a broad field of applications, especially in gas storage and catalysis. In this work, polymer embedded MOFs were extruded into filaments, which could be used for 3d-printing to profit from the specific properties of the MOFs in polymeric materials combined with the arbitrary shapes provided by 3d-printing. For the extrusion, different polymer classes like ABS, polyester- and polyetherurethanes, as well as different MOFs (ZIF-8, ZIF-67, HKUST-1) were used to create MOF containing filaments with a nominal diameter of 3.0 mm. Differential tomography at the edges of the Zn, Co, and Cu was then used to find the distribution of the corresponding MOF in the filament and to analyze the shape of the inclusions.
Absorption edge tomography, also known as differential tomography at absorption edges, is a method which exploits the sudden change of the attenuation coefficient, when the photon energy crosses the absorption edge of an element. Synchrotron radiation is the best source for absorption edge tomography, because of its small bandwidth, high intensity and easily adjustable photon energy. The synchrotron beamline BAMline at the synchrotron radiation facility BESSY II in Berlin, which is operated by the BundesanstaltfürMaterialforschung und -prüfung (BAM), provides a monochromatized beam in a photon energy range from 5 keV up to 80 keV with a bandwidth of 2%, when the double multilayer monochromator is used. Together with the microtomography setup, this enables differential tomography at the K edge of the elements from chromium up to the lanthanides, and up to uranium, when the L edges are used as well.
In this work, the absorption edge tomography is employed to perform a non-destructive, three-dimensional characterization of the microstructure of metallic alloys. As an example, a high strength Mg-Y-Zn alloy containing long period stacking ordered (LPSO) phases is analysed. The alloy with a nominal composition of Mg97Y2Zn1 was synthesized by melting highly pure magnesium, zinc and a Mg-22%Y master alloy and casting an ingot, which was homogenised at 350 °C and then extruded using an extrusion ratio of 18:1.
The results demonstrate that synchrotron based absorption edge tomography is a promising technique to perform a 3D characterization of the microstructure of metallic alloys.
Die Scaled Boundary Finite Elemente Methode (SBFEM) ist eine semi-analytische Methode, die vielversprechende Ergebnisse bei der Modellierung geführter Ultraschallwellen zeigt. Effizienz und niedriger Rechenaufwand der Methode werden durch Diskretisierung des Randes der Rechendomäne erreicht, während für die Domäne selbst die analytische Lösung verwendet wird. Mittels der SBFEM können verschiedene Arten von Fehlern können modelliert werden, z. Risse, Poren, Delamination, Korrosion, die in eine Struktur aus anisotropen und isotropen Materialien integriert sind.
In diesem Beitrag wird das SBFEM verwendet, um die Ausbreitung von geführten Wellen in einer Struktur zu analysieren, die aus einem isotropen Metall besteht, das an anisotropes Kohlefaserverstärktes Material gebunden ist. Das Verfahren ermöglicht die Identifizierung geeigneter Wellentypen (Modi) und die Analyse ihrer Interaktion mit verschiedenen Defekten. Die erzielten Ergebnisse werden zur Entwicklung eines Zustandsüberwachungssystems für Composite-Druckbehälter verwendet, die in der Automobil- und Luftfahrtindustrie benutzt werden.
Water Migration in One-Side Heated Concrete: 4D In-Situ CT Monitoring of the Moisture-Clog-Effect
(2018)
In order to study damage in concrete exposed to fire, a series of continuous X-ray computed tomography (CT) measurements were performed on a concrete sample heated, in-situ, on one side. The water migration relative to time and 3D space and, in particular, the dynamic condensation and vaporization of water droplets in the pores was quantified. This approach shows significant potential for further investigation of fire-related concrete damage.
Impact damages and delaminations in fibre-reinforced composites (FRC) might not be visible at the surface, but could have an influence on the resistance and on the long-term behaviour of the component. Therefore, and especially for safety relevant structures, non-destructive methods are required for the assessment of such damages.
Active thermography methods are suitable to characterize damages after loading using different kind of excitation techniques and various configurations of infrared (IR) camera and heating sources. Here, flash lamps, impulse excitation with infrared radiator and lock-in technique with halogen lamps or widened laser beams are suited. In addition, non-optical sources like sonotrodes (requiring direct contact to the structure) or induction generators (only suited for carbon fibre reinforced polymer (CFRP) structures) could be applied as well. For the investigation of the evolution of the damage during the impact, passive thermography can be applied in-situ. Elastic and plastic deformations alter the temperature of the structure and thus the temperature on the surface.
In this contribution, at first the general principles of quantitative defect characterisation in FRC using active thermography with flash, impulse and lock-in excitation are described. Optical and thermal properties of the FRC material and its anisotropy are considered. Results of phase differences obtained at flat bottom holes with flash and lock-in thermography are compared for qualifying both methods for quantitative defect characterization. Secondly, the damage evolution of CFRP and GFRP structures under impact load and static tensile loading is described. The spatial and temporal evolution of the surface temperature enables us to distinguish matrix cracks or fibre-matrix separation from delaminations between the layers. Afterwards, all results for loading defects, obtained by passive and active thermography, are compared with each other. Fig. 1 and 2 show the difference of passive and flash thermography obtained at impact and tensile loaded CFRP plates, respectively. As one purpose of these investigations is the development of standards within national (DIN) and European (CEN) standardisation bodies, new draft and final standards are presented and further needs are discussed at the end of the presentation.
Acoustic Emission
(2018)
Das Phänomen Schallemission (eng. Acoustic Emission, AE) ist eine Begleiterscheinung bei aktiven Mechanismen und Prozessen wie sie in Werkstoffen auftreten, die einer Belastung durch Krafteinwirkung oder durch Änderung der Umgebungsbedingungen ausgesetzt sind. Plastische Verformung, Risswachstum, Korrosion oder der Übergang zu einer anderen Phase generieren u.a. transiente elastische Wellen, die sich im Werkstoff und an der Materialoberfläche ausbreiten. Auftretende Auslenkungen von wenigen hundert Pikometern sind mit piezo-elektrischen AE Sensoren detektierbar. Aufzeichnungsraten von bis zu 40 MHz ermöglichen dabei zeitliche Auflösungen von einigen Nano- bis Mikrosekunden. Die Dechiffrierung der detektierten Informationen ist für die Material- und Versagenscharakterisierung sowie für Anwendungen in der Struktur- oder Prozessüberwachung ein zentraler Forschungsschwerpunkt.
Nach einem kurzen Überblick zu den Grundlagen werden ausgewählte Ansätze der AE Methode vorgestellt und diskutiert:
1) AE Monitoring von Pipelines als Referenzmessung für die Entwicklung eines akustischen faseroptischen Monitorings (AGIFAMOR)
2) Schwellwertfreie AE Messung im 4-Punkt-Rohrbiegeprüfstand BAM_9.1 (AGIFAMOR)
3) Kombination von AE mit Röntgen-Mikrotomografie und die Anwendung der frequenzbasierten Mustererkennung ermöglichen eine Zuordnung von AE und Mechanismen (Ergebnisse aus dem SNSF Projekt Nr. 127'134, Baensch 2014, Diss. ETH No. 22372)
3D imaging techniques have an enormous potential to understand the microstructure, its evolution, and its link to mechanical, thermal, and transport properties. In this conference paper we report the use of a powerful, yet not so wide-spread, set of X-ray techniques based on refraction effects. X-ray refraction allows determining internal specific surface (surface per unit volume) in a non-destructive fashion, position and orientation sensitive, and with a nanometric detectability. We demonstrate showcases of ceramics and composite materials, where microstructural parameters could be achieved in a way unrivalled even by high-resolution techniques such as electron microscopy or computed tomography. We present in situ analysis of the damage evolution in a carbon fibre reinforced polymer and a Al/Al2O3metal matrix composite during tensile load, the direct observation of damage accumulation during creep of Al-3.85Mg and the identification of void formation (different kinds of defects, particularly unsintered powder hidden in pores, and small inhomogeneity’s like cracks) in Ti64 parts produced by selective laser melting using synchrotron X-ray refraction radiography tomography.
The CLEAN ENERGY Flagship is an initiative designed to utilize recent game changing developments in digital, materials and manufacturing technologies to catalyze a radical paradigm shift towards clean, reliable, efficient and cost-optimal energy.
Unifying and drastically accelerating radically new energy material design, processing and integration across the entire value chain addressing energy production, conversion, storage and systems.
CLEAN ENERGY participants are all distinguished research organisations that each benefit from their own industry networks and contacts with regions and state-level activities and have a long history of collaborating with each other (for 10 years now under the umbrella of EERA) within a European collaborative framework.
Through EERA, CLEAN ENERGY aims to become a crucial partner in the SET-Plan, supporting long-lasting approaches through its established networks and internal collaborations.
Im Fokus dieser Arbeit steht die computertomographische (CT) Untersuchung (Synchrotron- und Labor-CT) von IN625-Pulver und den daraus gefertigten Streben, welche wiederum zu Gitterstrukturen zusammengesetzt werden. Aufgrund der Filigranität wurde zur Fertigung dieser Proben das pulverbettbasierte selektive Laserschmelzen verwendet.
Porositätsanalysen und Größenverteilungen wurden für das Pulver bei einer rekonstruierten Voxelgröße von 0,5µm ermittelt. 6,0mm lange Streben variierten im Aufbauwinkel von 30° bis 90° zur Bauplattform und zeigten so den Unterschied zwischen Up- und Down-Skin hinsichtlich der Rauigkeit und Porenverteilung. Die Gitterstrukturen konnten in-situ mit bis zu 5,0kN belastet werden, um deren Verformung computertomographisch zu erfassen.
Near eutectic cast Al–Si alloys are the basis of all Al-alloys used for pistons due to their high fluidity and relatively high strength-to-weight ratio. Their microstructure is characterized by the presence of eutectic-Si embedded in an age hardenable -Al matrix. During solution heat treatment, the eutectic Si network undergoes a process of gradual disintegration, reducing the load bearing capability and the strength of the alloy. The improvement of the high temperature strength is achieved by addition of transition elements such as Cu, Mg or Ni through the formation of stiff intermetallic (IM) phases.
In present study a near-eutectic AlSi12CuMgNi alloy produced by squeeze casting was investigated in as-cast condition. The in-situ neutron diffraction compression tests revealed the stress partitioning mechanism between phases of the alloy. Large stresses were found in IMs, showing their significant role as a reinforcement elements. After the failure of IM and Si phases the load is transferred back to the Al matrix, inducing further plastic deformation in it, yet without creating microcracking. The neutron diffraction experiments were coupled with assessment of internal damage after ex-situ compression tests by synchrotron radiation computed tomography. The quantitative analysis of CT data revealed that local tensile stresses in IM and Si phases induce microcracks with preferential orientation, parallel to the axis of applied load.
Altogether, present experimental data was used as an input for the developed micromechanical model based on Maxwell homogenization scheme. In contrast to the neutron diffraction experiment, which can only determine stress differences between the axial and radial sample directions, the model allows predicting the principal stresses in each phase of the alloy.
We investigated lattice structure manufactured by laser beam melting with computed tomography on difference scales, such as powder scale, strut scale and lattice scale.
The raw powder has been evaluated by means of synchrotron computed tomography (CT) at the BAM-Line (HZB Bessy II, Berlin). Therefore, the particle size distribution and even the pore size distribution was investigated and compared with results received by the producer by means of sieving. Studies with laboratory X-ray CT of porosity and roughness of manufactured struts in dependence of the build angle exhibited the tendency that elongated pores appear solely in a certain range near the edge. The integrity and load-bearing capacity of a lattice structure was investigated by means of in-situ CT during compression. The lattice structure was compressed by 10 % in height with an applied maximum force of 5 kN. We applied digital volume correlation algorithm on volumes of different load steps to quantifies the displacement within the structure.
Having been introduced almost two decades ago, Additive Manufacturing (AM) of metals has become industrially viable for a large variety of applications, including aerospace, automotive and medicine. Powder bed techniques such as Selective Laser Melting (SLM) based on layer-by-layer deposition and laser melt enable numerous degrees of freedom for the geometrical design. Developing during the manufacturing process, residual stresses may limit the application of SLM parts by reducing the load bearing capacity as well as induce unwanted distortion depending on the boundary conditions specified in manufacturing.
The residual stress distribution in IN718 elongated prisms produced by SLM was studied non-destructively by means of neutron (bulk) and laboratory X-ray (surface) diffraction. The samples with different scanning strategies, i.e. hatching length, were measured in as-built condition (on a build plate) and after removal from the build plate.
While surface stress fields seem constant for AB condition, X-ray diffraction shows stress gradients along the hatch direction in the RE condition. The stress profiles correlate with the distortion maps obtained by tactile probe measurements.
Neutron diffraction shows bulk stress gradients for all principal components along the main sample directions. We correlate the observed stress patterns with the hatch length, i.e. with its effect on temperature gradients and heat flow. The bulk stress gradients partially disappear after removal from the baseplate.
Together with surface scan utilizing a coordinate-measuring machine (CMM), it is possible to link the stress release to the sample distortion.
We finally propose an explanation of those stress profiles based on the deposition strategy.
Additive Manufacturing (AM) through the Selective Laser Melting (SLM) route offers ample scope for producing geometrically complex parts compared to the conventional subtractive manufacturing strategies. Nevertheless, the residual stresses which develop during the fabrication can limit application of the SLM components by reducing the load bearing capacity and by inducing unwanted distortion, depending on the boundary conditions specified during manufacturing. The present study aims at characterizing the residual stress states in the SLM parts using different diffraction methods. The material used is the nickel based superalloy Inconel 718. Microstructure as well as the surface and bulk residual stresses were characterized.
For the residual stress analysis, X-ray, synchrotron and neutron diffraction methods were used. The measurements were performed at BAM, at the EDDI beamline of -BESSY II synchrotronand the E3 line -BER II neutron reactor- of the Helmholtz-Zentrum für Materialien und Energie (HZB) Berlin. The results reveal significant differences in the residual stress states for the different characterization techniques employed, which indicates the dependence of the residual state on the penetration depth in the sample. For the surface residual stresses, longitudinal and transverse stress components from X-ray and synchrotron agree well and the obtained values were around the yield strength of the material. Furthermore, synchrotron mapping disclosed gradients along the width and length of the sample for the longitudinal and transverse stress components. On the other hand, lower residual stresses were found in the bulk of the material measured using neutron diffraction. The longitudinal component was tensile and decreased towards the boundary of the sample. In contrast, the normal component was nearly constant and compressive in nature. The transversal component was almost negligible. The results indicate that a stress re-distribution takes place during the deposition of the consecutive layers. Further investigations are planned to study the phenomenon in detail.
Additive manufacturing (AM) offers an effective solution to the medical sector. It enables the production, on demand, of customised implants which match the patient’s anatomy, with grafts that promote bone growth, as well as surgical guides that help the surgeons.
The objective of this project is to provide a comprehensive basis to enable the safe use of medical AM products with traceable and reliable dimensionalmeasurements. This will guarantee the reliability of medical AM products to notified bodies and facilitate acceptance of AM in the medical sector for a better quality of life.
Fibre-reinforced plastics (FRP) especially carbon-fibre-reinforced polymer (CFRP) and glass-fibre-reinforced polymer (GFRP) are commonly used materials in high pressure vessels and storage units for automotive and aerospace purposes. Optical fibres are suitable to be integrated or directly applied to the surface of FRP components. Using optical fibres it is possible to monitor the distributed strain profiles and changes within the fatigue life of a pressure vessel to ensure the operational safety. Within artificial ageing experiments we used swept wavelength interferometry (SWI) based distributed strain sensing for the monitoring of commercial high-pressure composite cylinder. This artificial ageing was performed using test conditions of 503bar pressure load (service pressure 300 bar) and 89 °C for 100 h. The polyimide coated optical fibres were glued to the surface externally in circumferential and axial direction. Using distributed strain sensing (DSS) material expansion of over 0.5% were monitored with sub-centimetre spatial resolution. Within the circumferential direction we observed up to 10 % local fluctuation compared to the median strain caused by inhomogeneous material expansion, which could cause local material fatigue. In addition, we determined material degradation manifested itself as localized remaining material expansion and/or contraction. Results have been validated by other non-destructive methods like digital strip projection.
Fibre-reinforced plastics (FRP) especially carbon-fibre-reinforced polymer (CFRP) and glass-fibre-reinforced polymer (GFRP) are commonly used materials in high pressure vessels and storage units for automotive and aerospace purposes. Optical fibres are suitable to be integrated or directly applied to the surface of FRP components. Using optical fibres it is possible to monitor the distributed strain profiles and changes within the fatigue life of a pressure vessel to ensure the operational safety. Within artificial ageing experiments we used swept wavelength interferometry (SWI) based distributed strain sensing for the monitoring of commercial high-pressure composite cylinder. This artificial ageing was performed using test conditions of 503bar pressure load (service pressure 300 bar) and 89 °C for 100 h. The polyimide coated optical fibres were glued to the surface externally in circumferential and axial direction. Using distributed strain sensing (DSS) material expansion of over 0.5% were monitored with sub-centimetre spatial resolution. Within the circumferential direction we observed up to 10 % local fluctuation compared to the median strain caused by inhomogeneous material expansion, which could cause local material fatigue. In addition, we determined material degradation manifested itself as localized remaining material expansion and/or contraction. Results have been validated by other non-destructive methods like digital strip projection.
Glass-fibre-reinforced plastics (GFRP) are commonly used for the construction of pressure vessels and tanks for example in automotive and aerospace industries. Especially for pressure vessels used for the storage of natural gas or hydrogen with operation pressures up to 700 bar, an early material fatigue detection is of great interest. Measuring the distributed strain profile of GFRP structures helps to understand and detect material fatigue. In this article, we demonstrate the great potential of swept wavelength interferometry (SWI) based distributed strain sensing for the monitoring of pressure vessels made from GFRP. A resin transfer molding (RTM) process was used to manufacture GFRP-tube specimens. Commercial optical fibres with polyimid coating were glued to the surface externally in circumferential and axial direction. A cyclic load of up to 150 bar was applied to the samples using a servo-hydraulic test bench. Comparing the loaded and unloaded test conditions, we determined up to 2 % elongation in circumferential direction. We demonstrate reliable distributed strain measurements with sub-centimetre spatial resolution. By monitoring these high-resolution strain profiles, we were able to detect local material degradation that manifested itself as localized strain changes. Crucially, the material Degradation could be detected already after 75 % of dat the fatigue life before a crack appeared that led to leakage.
Glass-fibre-reinforced plastics (GFRP) are commonly used for the construction of pressure vessels and tanks for example in automotive and aerospace industries. Especially for pressure vessels used for the storage of natural gas or hydrogen with operation pressures up to 700 bar, an early material fatigue detection is of great interest. Measuring the distributed strain profile of GFRP structures helps to understand and detect material fatigue. In this article, we demonstrate the great potential of swept wavelength interferometry (SWI) based distributed strain sensing for the monitoring of pressure vessels made from GFRP. A resin transfer molding (RTM) process was used to manufacture GFRP-tube specimens. Commercial optical fibres with polyimid coating were glued to the surface externally in circumferential and axial direction. A cyclic load of up to 150 bar was applied to the samples using a servo-hydraulic test bench. Comparing the loaded and unloaded test conditions, we determined up to 2 % elongation in circumferential direction. We demonstrate reliable distributed strain measurements with sub-centimetre spatial resolution. By monitoring these high-resolution strain profiles, we were able to detect local material degradation that manifested itself as localized strain changes. Crucially, the material Degradation could be detected already after 75 % of dat the fatigue life before a crack appeared that led to leakage.
X-ray imaging techniques have an enormous potential to understand the microstructure, its evolution, and its link to mechanical, thermal, and transport properties. In this lecture we report the use of a powerful, yet not so wide-spread, set of X-ray techniques based on refraction effects. X-ray refraction allows determining the internal specific surface of materials (surface per unit volume) in a non-destructive fashion, position and orientation sensitive, and with a nanometric detectability. We demonstrate showcases of ceramics and composite materials, where microstructural parameters could be achieved in a way unrivalled even by high-resolution techniques such as electron microscopy or computed tomography. We present in situ analysis of the damage evolution during tensile load and the identification of void formation in parts produced by selective laser melting.
Having been introduced almost two decades ago, Additive Manufacturing (AM) of metals has become industrially viable for a large variety of applications, including aerospace, automotive and medicine. Powder bed techniques such as Selective Laser Melting (SLM) based on layer-by-layer deposition and laser melt enable numerous degrees of freedom for the geometrical design. Developing during the manufacturing process, residual stresses may limit the application of SLM parts by reducing the load bearing capacity as well as induce unwanted distortion depending on the boundary conditions specified in manufacturing.
The residual stress distribution in IN718 elongated prisms produced by SLM was studied non-destructively by means of neutron (bulk) and laboratory X-ray (surface) diffraction. The samples with different scanning strategies, i.e. hatching length, were measured in as-build condition (on a build plate) and after removal from the build plate.
The absolute values of all stress components decreased after removal from the build plate. Together with surface scan utilizing a coordinate-measuring machine (CMM), it is possible to link the stress release to the sample distortion. Obtained results indicated different residual stress states for each of the transversal, longitudinal and normal component depending on the thermal gradient in the respective direction.
Having been introduced almost two decades ago, Additive Manufacturing (AM) of metals has become industrially viable for a large variety of applications, including aerospace, automotive and medicine. Powder bed techniques such as Selective Laser Melting (SLM) based on layer-by-layer deposition and laser melt enable numerous degrees of freedom for the geometrical design. Developing during the manufacturing process, residual stresses may limit the application of SLM parts by reducing the load bearing capacity as well as induce unwanted distortion depending on the boundary conditions specified in manufacturing.
The residual stress distribution in IN718 elongated prisms produced by SLM was studied non-destructively by means of neutron (bulk) and laboratory X-ray (surface) diffraction. The samples with different scanning strategies, i.e. hatching length, were measured in as-build condition (on a build plate) and after removal from the build plate.
The absolute values of all stress components decreased after removal from the build plate. Together with surface scan utilizing a coordinate-measuring machine (CMM), it is possible to link the stress release to the sample distortion. Obtained results indicated different residual stress states for each of the transversal, longitudinal and normal component depending on the thermal gradient in the respective direction.
BAM ensures and represents high standards for safety in technology and chemistry. Additive manufacturing (AM) changes the requirements for conventional non-destructive testing (NDT) as new processes of defect creation occur. Especially in safety critical areas, such as aerospace and automotive, new manufacturing processes and materials always require reliability tests and new standards which is a big challenge for NDT.
Microstructure characterisation of advanced materials via 2D and 3D X-ray refraction techniques
(2018)
3D imaging techniques have an enormous potential to understand the microstructure, its evolution, and its link to mechanical, thermal, and transport properties. In this conference paper we report the use of a powerful, yet not so wide-spread, set of X-ray techniques based on refraction effects. X-ray refraction allows determining internal specific surface (surface per unit volume) in a non-destructive fashion, position and orientation sensitive, and with a nanometric detectability. We demonstrate showcases of ceramics and composite materials, where microstructural parameters could be achieved in a way unrivalled even by high-resolution techniques such as electron microscopy or computed tomography. We present in situ analysis of the damage evolution in an Al/Al2O3 metal matrix composite during tensile load and the identification of void formation (different kinds of defects, particularly unsintered powder hidden in pores, and small inhomogeneity’s like cracks) in Ti64 parts produced by selective laser melting using synchrotron X-ray refraction radiography and tomography.
Additive manufacturing (AM) offers a range of novel applications. However, the manufacturing process is complex and the production of defect-free parts with high reliability and durability is still a challenge. Thermography is a valuable tool for process surveillance, especially in metal AM processes. The high process temperatures allow one to use cameras usually operating in the visible spectral range. Here, we compare the results of measurements during the manufacturing process of a commercial laser metal deposition setup using a mid-wavelength-IR camera with those from a visual spectrum high-speed camera with band pass filter in the near-IR range.
The Scaled Boundary Finite Element Method (SBFEM) is a semi-analytical method that shows promising results in modelling of guided ultrasonic waves. Efficiency and low computational cost of the method are achieved by a discretisation of the boundary of a computational domain only, whereas for the domain itself the analytical solution is used. By means of the SBFEM different types of defects, e.g. cracks, pores, delamination, corrosion, integrated into a structure consisting of anisotropic and isotropic materials can be modelled.
In this contribution, the SBFEM is used to analyse the propagation of guided waves in a structure consisting of an isotropic metal bonded to anisotropic carbon fibre reinforced material. The method allows appropriate wave types (modes) to be identified and to analyse their interaction with different defects. Results obtained are used to develop a structural health monitoring system for composite pressure vessels used in automotive and aerospace industries.
The Scaled Boundary Finite Element Method (SBFEM) is a semi-analytical method that shows promising results in modelling of guided ultrasonic waves. Efficiency and low computational cost of the method are achieved by a discretisation of the boundary of a computational domain only, whereas for the domain itself the analytical solution is used. By means of the SBFEM different types of defects, e.g. cracks, pores, delamination, corrosion, integrated into a structure consisting of anisotropic and isotropic materials can be modelled.
In this contribution, the SBFEM is used to analyse the propagation of guided waves in a structure consisting of an isotropic metal bonded to anisotropic carbon fibre reinforced material. The method allows appropriate wave types (modes) to be identified and to analyse their interaction with different defects. Results obtained are used to develop a structural health monitoring system for composite pressure vessels used in automotive and aerospace industries.
The Scaled Boundary Finite Element Method (SBFEM) is a semi-analytical method that shows promising results in modelling of guided ultrasonic waves. Efficiency and low computational cost of the method are achieved by a discretisation of the boundary of a computational domain only, whereas for the domain itself the analytical solution is used. By means of the SBFEM different types of defects, e.g. cracks, pores, delamination, corrosion, integrated into a structure consisting of anisotropic and isotropic materials can be modelled.
In this contribution, the SBFEM is used to analyse the propagation of guided waves in a structure consisting of an isotropic metal bonded to anisotropic carbon fibre reinforced material. The method allows appropriate wave types (modes) to be identified and to analyse their interaction with different defects. Results obtained are used to develop a structural health monitoring system for composite pressure vessels used in automotive and aerospace industries.