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- Adsorption (10)
- Austenitic stainless steel (10)
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- i-TRIBOMAT (8)
- Additive manufacturing (AM) (7)
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- Alkali-silica reaction (7)
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- Automated synthesis (7)
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- CT (7)
- Calcium cobaltite (7)
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- Carbon steels (7)
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- Charpy impact toughness (7)
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- Environmental stress cracking (7)
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- ISO 3690 (7)
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- Silver (7)
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- TMDSC (7)
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- Titanium alloy (7)
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- UV (7)
- UV radiation (7)
- Ultrakurze Laserpulse (7)
- Ultrashort laser material interaction (7)
- Ultrashort laser pulses (7)
- WRC 1992 diagram (7)
- Water content (7)
- Werkstoffe (7)
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Paper des Monats
- ja (44)
Der Zweck der Dehnungsmessungen ist es in vielen Fällen, aus der Dehnung die zu erwartende Sicherheit eines Baukörpers zu ermitteln. Dazu müssen aus den Dehnungen über die Spannungen
die Lasten bestimmt werden.
Die Spannungsdehnungslinie des Werkstoffes ist aber von zahlreichen Parametern, wie Belastungsdauer, Beanspruchungsgeschwindigkeit, Spannungszustand, Eigenspannungen, abhängig.
Zur Deutung von Dehnungsmessungen muß die Vielfalt der Spannungsdehnungslinien einschließlich ihrer Endpunkte bekannt sein. Die Dehnungsmessung kann hierfür einen Teil, aber nicht die Gesamtheit der notwendigen Parameter liefern.
Die Feststellung der Spannungsdehnungskurve mit ihrer Hilfe ist Sache der Tragfähigkeitsforschung. Die hier zu lösenden Fragen, z.B. Bedeutung der Dehnungen im Atomgitter, Abhängigkeit der Verformungsfähigkeit vom Spannungszustand, Einfluß des Spannungsgefälles, der Beanspruchungsgeschwindigkeit usw., gehören zu den z.Z. wichtigsten Fragen der Werkstoffmechanik und Tragfähigkeitsforschung. Tragfähigkeitsforschung und Dehnungsmeßtechnik sind daher in ihrer Entwicklung gegenseitig voneinander abhängig.
In Auswertung der Theorie lassen sich die Bedingungen des spröden Bruches für eine bestimmte Probenform (Spannungszustand) im Geschwindigkeits-Temperatur-Schaubild durch eine gerade Linie (kritische Gerade) darstellen, welche im Schaubild das Gebiet des zähen Bruches vom Gebiet des spröden Bruches abgrenzt. Die Größe des Raumes zwischen der kritischen Geraden und den Gebrauchsbedingungen ist ein Maßstab für den Sicherheitsgrad des Werkstoffes gegenüber dem spröden Bruch. Die Formänderungsfähigkeit, die der Werkstoff unterhalb dieser Grenzen, also im Gebiet des zähen Bruches aufbringt, ist gänzlich unabhängig von den Sprödbruchbedingungen. Ein Werkstoffprüfverfahren bei Raumtemperatur muß mit Proben sehr scharfer Einkerbung bei entsprechendem Spannungszustand durchgeführt werden, damit die Ergebnisse in die Nähe der kritischen Geraden fallen; denn nur so lassen sich die Werkstoffe hinsichtlich ihrer Sprödigkeitsneigung differenzieren. Außerdem muß die Formänderungsfähigkeit herausdividierbar sein, damit sich die Sprödbruchbedingungen klar absondern lassen. Mildere Probenformen, z.B. die Kerbschlagbiegeprobe mit flacher, kreissegmentförmiger Kerbe, sind indifferent; sie geben nur die von der Sprödbruchneigung unabhängige Formänderungsfähigkeit wieder und bieten daher nichts Neues.
Bei dem vorliegenden Prüfverfahren wird der Sicherheitsgrad durch das Verhältnis der dynamischen zur statischen Brucheinschnürung Ψ(KS)/Ψ(K) bei der Kerbzugprobe wiedergegeben. Die statische Brucheinschnürung Ψ(K) kennzeichnet die Formänderungsfähigkeit, durch welche vor Eintritt der Sprödbruchbedingungen ein, die Sicherheit vermehrender plastischer Abbau von Spannungsspitzen ermöglicht wird.
Kaltreckschäden sind nicht so aufzufassen, daß sie nur bei "alterungsanfälligen" Stählen vorkommen; alle Werkstoffe erleiden Kaltreckschäden. Bemerkbar und gefährlich werden diese nur dann, wenn von vornherein der Quotient Ψ(KS)/Ψ(K) und damit der Sicherheitsgrad klein ist. Diese quantitative Erklärung macht es verständlich, daß der Quotient Ψ(KS)/Ψ(K) im ungeschädigtem Zustand so gute Voraussagen erlaubt.
Die prüfmäßige Ermittlung der Sprödigkeitsgrenzen von Baustählen im Anlieferungszustand ergibt eine breite Differenzierung, die für die Übergangstemperatur bei statischer Beanspruchung einen Bereich zwischen etwa -90 and -225°C, also von etwa 135°C einnimmt. Bei der Aufschweißbiegeprobe drängt sich dieser Bereich auf etwa 40°C, zwischen etwa +30 und -10°C liegend zusammen. Daraus geht hervor, daß die besseren Stähle durch das Schweißen eine größere Schädigung erfahren als die minderwertigen. Die Ursache sind innere Spannungen, die als Folge räumlich begrenzter Plastizierungen bei Erwärmung und Wiederabkühlung entstehen und die am stärksten bei den Stählen auftreten, welche bei den höchsten Geschwindigkeiten und tiefsten Temperaturen noch plastizieren. Dieselbe Theorie, welche die Qualität der Stähle in Anlieferungszustand bedingt (Becker - Orowan - Kochendörfer), begründet auch die Schädigung der qualifiziertesten Stähle durch das Schweißen. Trotzdem bleiben die qualifizierten Stähle noch überlegen:
1.) sie behalten noch einen, wenn auch kleinen Überschuß an Zähigkeit beim Aufschweißbiegeversuch,
2.) im Sprödigkeitsgebiet (-20°C) ertragen sic höhere elastische Biegewinkel und damit höhere Spannungen,
3.) die inneren Spannungen lassen sich durch Ausglühen umso leichter beseitigen, je besser die Qualität ist; bei Stählen minderer Qualität können schon beim Schweißen Schrumpfrisse entstehen.
Die Qualität ist dadurch gekennzeichnet, daß die Sprödigkeitsgrenzen des Stahles weit von den Gebrauchsbedingungen entfernt liegen. Die Ermittlung des Brucheinschnürungsquotienten aus dem Kerbschlagzug- und Kerbzugversuch im Anlieferungszustand und bei Raumtemperatur ist das einfachste Verfahren, welches anstelle der umständlichen Ermittlung der Temperaturkurven einen Maßstab für die Sprödigkeitsgrenzen abgibt. Zwischen diesem Prüfwert und den Ergebnissen des Aufschweißbiegeversuches wurden folgende Zusammenhänge gefunden:
1.) Die Bruchgefahr bei der Aufschweißbiegeprobe ist durch einen kleinen Brucheinschnürungsquotienten gekennzeichnet.
2.) lm Gebiet des spröden Bruches ordnen sich die elastischen Biegewinkel, d.h. die ertragenen Spannungen, nach der Größe des Brucheinschnürungsquotienten ein.
3.) Der Erfolg des Spannungsfreiglühens kann nach der Größe des Brucheinschnürungsquotienten vorausgesagt werden.
Die Sprödigkeitsfrage bei geschweißten dicken Profilen läuft also auf die Auswahl des Stahles unter Berücksichtigung seiner Sprödigkeitsgrenzen im Anlieferungszustand hinaus, wofür die Ermittlung des Brucheinschnürungsquotienten das geeignetste Prüfverfahren ist, und auf die Vervollkommnung der Vorrichtungen zum Vorwärmen oder Ausglühen großer Bauteile. Der Erfolg hängt hier von der richtigen Auswahl des Stahles ab.
Außer den Schrumpfspannungen treten noch Umwandlungsspannungen unter Martensitbildung auf. Ihre Beziehungen zu den ursprünglichen Sprödigkeitsgrenzen des Stahles, sowie zum Brucheinschnürungsquotienten im Anlieferungszustand sind noch durch Versuche aufzuklären.
Wenn man eine Kerbzugprobe im Pendelhammer zerschlägt und eine gleiche Probe in der Zerreißmaschine zu Bruch bringt, dann gibt der Quotient aus beiden gemessenen Brucheinschnürungen vollständigen Aufschluß über die Sprödigkeitsgrenzen des Werkstoffes, als Folge von Temperatur, Belastungsgeschwindigkeit und Spannungszustand. Die Sprödigkeitsgrenze ist dadurch gekennzeichnet, daß die Elastizität vollständig unterbunden ist. Man ermittelt die Sprödigkeitsgrenze, indem man das Plastizitätsgefälle in Abhängigkeit von einem der genannten Einflüsse feststellt. Geschieht dies in Abhängigkeit von der Temperatur, so treten große Versuchsstreuungen auf, die insbesondere bei tiefen Temperaturen und im Abfallgebiet der Zähigkeit sehr groß werden. Wird dagegen bei konstanter Raumtemperatur die Belastungsgeschwindigkeit variiert und das Plastizitätsgefälle durch Brucheinschnürungsmessungen festgestellt, dann sind die Ergebnisse so gut wie fehlerfrei. Daß man hierbei mit nur zwei Einschnürungsmessungen auskommt, hat seine Begründung in der Eindeutigkeit des Sprödigkeitsgesetzes. Es läßt keine vielseitigen Variationen aus der vier Bedingungen: Stoff, Temperatur, Geschwindigkeit und Spannungszustand zu, sondern seine gesetzmäßigen Möglichkeiten sind nur durch einen Punkt des vierdimensionalen Diagramms festgelegt. Diese empirische Entdeckung war die Folge der Versuchsauswertungen im obigen Bericht. Der Spannungszustand ist die für den Baustatiker wichtigste Bedingung. Sein Einfluß auf den Sprödbruch läßt sich auf das einfache Verhältnis der linearen Streckgrenze σ(S) zur Normalspannung σ(NF) im tragenden Querschnitt bei Fließeintritt zurückführen. Dieses Verhältnis ist - wenn es nicht unmittelbar experimentell gemessen werden kann - aus den räumlichen Spannungszuständen und der Spannungsverteilung zu entwickeln. Daß die Reduzierung beliebiger räumlicher Kräfte auf die drei Hauptspannungen und die Reduzierung dieser auf eine in gewünschter haupttragender Richtung schwierig oder auch noch nicht gelöst ist, wenn die primär angreifenden Kräfte mit einer ungleichmäßigen Spannungsverteilung behaftet sind, ist Künstlerpech der Elastostatik. Seitens der Physik, Werkstoffmechanik und Werkstoffprüfung kann das Problem des Sprödbruches als gelöst angesehen werden. Aber selbst, wenn solche präzisen Feststellungen nicht möglich sind, ist eine Einordnung des Spannungsquotienten σ(S)/σ(NF) in die von 0 bis 1 (linearer Zustand) reichende Skala leicht abschätzbar, innerhalb welcher die vorliegende Kerbzugprobe mit 0,33 zu beziffern ist.
Dieser umfassende Erfolg der Kerbschlagzugprüfung ist auf die Verbindung zwischen Versuchspraxis und Theorie zurückzuführen, die eine Folge der Kreissymmetrie der Probenform und der Einschnürungsmessung ist. Etwa aus diesen Gründen das Verfahren als umständlich oder schwierig anzusehen, entbehrt der Berechtigung, da sich die praktische Prüfung neben ihrer Exaktheit als einfacher herausstellt als die gealterte Kerbschlagbiegeprobe.
Keines der z.Zt. zur Diskussion stehenden Sprödigkeitsprüfverfahren erlaubt so weitgreifende Auswertungen der Versuchsergebnisse. Insbesondere sind die auf Biegung beanspruchten unsymmetrischen Probenformen mit Schlagarbeitsmessung nicht geeignet, eine Theorie so unmittelbar in die Wirklichkeit umzusetzen und man ist mit ihnen aufs Probieren angewiesen. Wenn man heute die Kerbschlagbiegezähigkeit künstlich gealterter Stähle als Maßstab für die Sprödigkeitsneigung einführen möchte, so läßt sich - ohne erst ausprobieren zu müssen - auf Grund theoretischer Erkenntnis sagen, daß sich die Stähle hinsichtlich ihres Alterungseffektes überhaupt nicht differentieren, da alle eine etwa gleich große Schädigung erfahren, die in einer Verschiebung der kritischen Geraden um etwa +70°C besteht. Wenn also die Kerbzähigkeit gealterter Stähle eine Differentierung erfährt, so nur deshalb, weil schon vor der künstlichen Alterung die kritische Gerade eine ungünstige Lage hatte. Das läßt sich aber ohne die Umständlichkeit des künstlichen Alterns mit der Kerbzugprobe ermitteln. Im übrigen werden im obigen Bericht die Unsicherheiten und die starken Streuungen der Kerbschlagbiegezähigkeit im gealterten Zustand erläutert, die darauf zurückzuführen sind, daß dieser Begriff kein so reiner Ausdruck für die Sprödigkeitsgrenzen wie der Brucheinschnürungsquotient ist, sondern Einflüsse enthält, die mit der Sprödigkeitsgrenze nichts zu tun haben.
Die Becker-Orowan-Kockendörfersche Plastizitätstheorie bildet eine anschauliche Grundlage für die Sprödigkeitsbedingungen. Danach sind für den Eintritt des Sprödbruches außer den Materialeigenschaften drei äußere Faktoren maßgebend: Temperatur, Belastungszeit und Spannungszustand (Gestalt). Um den Sprödbruch herbeizuführen, braucht man nur einen dieser drei Faktoren genügend zu verschärfen. Diesen Umstand macht sich die Materialprüfung zu Nutze, indem z.B. bei der Kerbschlagbiegeprobe Schlaggeschwindigkeit und Probenform unveränderlich bleiben und nur die Temperatur soweit erniedrigt wird, bis der Sprödbruch erfolgt. Die so ermittelte "Übergangstemperatur" ist - obgleich sie nur für diese speziellen Zeit- und Gestaltverhältnisse Gültigkeit hat - ein guter Vergleichsmaßstab für verschiedene Werkstoffe.
Nun ist aber die Prüfung bei veränderlichen, insbesondere niedrigen Temperaturen sehr umständlich. Deshalb wird bei dem hier beschriebenen Prüfverfahren nicht die Temperatur, sondern die Belastungszeit verändert. Infolge der achsen-symmetrischen Einkerbung und der daraus folgenden Möglichkeit, die Brucheinschnürung sehr einfach zu messen, kommt man mit nur zwei Geschwindigkeitsstufen aus, weil das zwischen beiden liegende meßbare Zähigkeitsgefälle für die Beurteilung der Sprödigkeitsneigung ausreicht, vorausgesetzt, daß man sich nahe der Sprödigkeitsgrenze befindet ohne aber die wirkliche Sprödbruchgrenze erreichen zu müssen.
In der vorliegenden Note beginnen wir mit der Untersuchung eines partiellen Differentialoperators vierter Ordnung, der in der Mechanik bei der Behandlung von rechteckigen, isotropen, schubbeanspruchten Platten eine Rolle spielt. Zunächst soll bewiesen werden, daß der genannte Operator in einem Hilbertschen Raume L2 nach unten halbbeschränkt ist. Später gedenken wir Betrachtungen über Fortsetzbarkeit und Darstellbarkeit durch Kernmatrizen anzustellen.
Kunststoffe im Bauwesen
(1962)
In den letzten Jahren hat die Verwendung von Kunststoffen im Bauwesen einen erheblichen Aufschwung genommen. Hierbei hat nicht nur der Umsatz, sondern auch der Verwendungsumfang von Jahr zu Jahr zugenommen, was nicht zuletzt seine Ursache in den Variationsmöglichkeiten der Eigenschaften von Kunststoffen hat. So befindet sich eine Vielzahl von Kunststoff-Erzeugnissen für das Bauwesen mit unterschiedlichen Eigenschaften auf dem Markt. Um Bauherren, Bauträgern und Architekten eine Übersicht über geeignete Kunststoff-Erzeugnisse und ihre technischen Anwendungsmöglichkeiten im Bauwesen zu geben, ist vom Bundesministerium für Wohnungswesen, Städtebau und Raumordnung die Aufstellung eines Verzeichnisses „Kunststoffe im Bauwesen“ angeregt worden. Dieses Verzeichnis soll die Anwendung von solchen Kunststoff-Erzeugnissen erleichtern, die sich als geeignet und bewährt herausgestellt haben. Dadurch wird indirekt eine Steigerung der Güte, der baulichen Ausführung und Wohnungsausstattung ermöglicht, überdies wird das Kunststoff-Verzeichnis dazu beitragen, Vorurteile gegen die Verwendung von Kunststoffen zu beseitigen. Das Verzeichnis hat keinerlei amtlichen Charakter, wobei jedoch angenommen wird, das sich auch amtliche Stellen des Verzeichnisses bedienen werden. Es enthält keine Preisangaben.
In den letzten Jahren hat die Verwendung von Kunststoffen im Bauwesen einen erheblichen Aufschwung genommen. Hierbei hat nicht nur der Umsatz, sondern auch der Verwendungsumfang von Jahr zu Jahr zugenommen, was nicht zuletzt seine Ursache in den Variationsmöglichkeiten der Eigenschaften von Kunststoffen hat. So befindet sich eine Vielzahl von Kunststoff-Erzeugnissen für das Bauwesen mit unterschiedlichen Eigenschaften auf dem Markt. Um Bauherren, Bauträgern und Architekten eine Übersicht über geeignete Kunststoff-Erzeugnisse und ihre technischen Anwendungsmöglichkeiten im Bauwesen zu geben, ist vom Bundesministerium für Wohnungswesen, Städtebau und Raumordnung die Aufstellung eines Verzeichnisses „Kunststoffe im Bauwesen“ angeregt worden. Dieses Verzeichnis soll die Anwendung von solchen Kunststoff-Erzeugnissen erleichtern, die sich als geeignet und bewährt herausgestellt haben. Dadurch wird indirekt eine Steigerung der Güte, der baulichen Ausführung und Wohnungsausstattung ermöglicht, überdies wird das Kunststoff-Verzeichnis dazu beitragen, Vorurteile gegen die Verwendung von Kunststoffen zu beseitigen. Das Verzeichnis hat keinerlei amtlichen Charakter, wobei jedoch angenommen wird, das sich auch amtliche Stellen des Verzeichnisses bedienen werden. Es enthält keine Preisangaben.
In den letzten Jahren hat die Verwendung von Kunststoffen im Bauwesen einen erheblichen Aufschwung genommen. Hierbei hat nicht nur der Umsatz, sondern auch der Verwendungsumfang von Jahr zu Jahr zugenommen, was nicht zuletzt seine Ursache in den Variationsmöglichkeiten der Eigenschaften von Kunststoffen hat. So befindet sich eine Vielzahl von Kunststoff-Erzeugnissen für das Bauwesen mit unterschiedlichen Eigenschaften auf dem Markt. Um Bauherren, Bauträgern und Architekten eine Übersicht über geeignete Kunststoff-Erzeugnisse und ihre technischen Anwendungsmöglichkeiten im Bauwesen zu geben, ist vom Bundesministerium für Wohnungswesen, Städtebau und Raumordnung die Aufstellung eines Verzeichnisses „Kunststoffe im Bauwesen“ angeregt worden. Dieses Verzeichnis soll die Anwendung von solchen Kunststoff-Erzeugnissen erleichtern, die sich als geeignet und bewährt herausgestellt haben. Dadurch wird indirekt eine Steigerung der Güte, der baulichen Ausführung und Wohnungsausstattung ermöglicht, überdies wird das Kunststoff-Verzeichnis dazu beitragen, Vorurteile gegen die Verwendung von Kunststoffen zu beseitigen. Das Verzeichnis hat keinerlei amtlichen Charakter, wobei jedoch angenommen wird, das sich auch amtliche Stellen des Verzeichnisses bedienen werden. Es enthält keine Preisangaben.
Das Staatsbad Oeynhausen bot einen würdigen Rahmen für den DVM-Tag. Die große Zahl der Teilnehmer und Gäste — es waren annähernd 350 Teilnehmer aus neun Ländern anwesend — unterstreicht eindrucksvoll die Bedeutung, die dieser Tagung in in- und ausländischen Fachkreisen beigemessen wird. 15 Vorträge über Fragen aus den verschiedensten Stoffbereichen ließen klar erkennen, daß die bleibende Verformung von Werkstoffen und ihre Prüfung ein von der Stoffart unabhängiges, allgemeines Problem für Wissenschaft und Technik ist. Den Teilnehmern war auch Gelegenheit gegeben, in persönlichem Gespräch ihre Erfahrungen und Erkenntnisse auszutauschen.
Bei der Begrüßung der Teilnehmer durch den bisherigen Vorsitzenden, Prof. Dr.-Ing. habil. H. Diergarten, Schweinfurt, wird dem Staatsbad Oeynhausen und seinem Kurdirektor Dr. med. habil. Schmid im Namen des DVM für das Entgegenkommen und die Gastfreundschaft gedankt. Ein ehrendes Gedenken gilt den unvergessenen Verstorbenen Prof. Dr.-Ing. Dr.-Ing. E. h. E. Siebel, Prof. Dr.-Ing. E. H. Schulz, Prof. Dr. rer. nat. W. Weltzien, Prof. Dr. phil. O. Dahl und Prof. Dr.-Ing. E. Houdremont, mit denen der DVM in verhältnismäßig kurzer Zeit viele führende Männer verloren hat.
Eine rationelle, verarbeitungs- und anwendungsgerechte Nutzung der Werkstoffe ist ohne Anwendung der Materialprüfung nicht mehr denkbar. Zu Beginn der industriellen Entwicklung beschränkte sich die Materialprüfung mit einfachen technologischen Prüfungen auf eine Gleichmäßigkeitskontrolle. Dies änderte sich mit der Zunahme der Vielfalt der Probleme. An die Werkstoffe werden immer höhere Ansprüche und Sonderwünsche gestellt. So werden neue Werkstoffe geschaffen, deren Eigenschaften, ohne daß man auf Erfahrung zurückgreifen kann, im Laboratorium geprüft werden müssen, bevor sie sich im Betrieb bewähren sollen. Bei der Breite des Anwendungsgebietes sind Wissenschaftler und Ingenieure aller technischen Zweige an der Materialprüfung beteiligt. Um allen die Möglichkeit zu geben, Fragen gleicher Natur auch gemeinsam zu behandeln, wurde bereits 1896 der DVM unter A. Martens gegründet. Ziel des DVM ist es, die Entwicklung und Kenntnisse sowie die Zusammenarbeit auf dem Gebiet der Materialprüfung zu fördern. Dies geschieht durch die Herausgabe der Zeitschrift „Materialprüfung“, durch Versand der „Zwanglosen Mitteilungen“, durch Veranstaltung von Kolloquien und nicht zuletzt durch die alle zwei Jahre wiederkehrende Veranstaltung des DVM-Tags.
Zum neuen ersten Vorsitzenden des DVM wurde in der am 11. März abgehaltenen Mitgliederversammlung Prof. Dr. mont. H. Krainer gewählt und der Senior der Materialprüfung in Deutschland, Bundesbahndirektor i. R. Dr.-Ing. R. Kühnel in Anerkennung seiner großen Verdienste zum Ehrenmitglied ernannt.
Zur Aktivierung der im Schrifttum vorhandenen Werte an Wissen ist die Dokumentation unbedingt erforderlich, denn der Umfang an Informationen u. dgl. überschreitet das Aufnahmevermögen jedes Einzelnen.
Nachdem kurz auf die Bedeutung der Dokumentation hingewiesen wurde, wurden Einzelheiten über das Erfassen, Sichten, Überprüfen und Sammeln des Fachwissens angegeben. Als Grundlage für die gesamte Arbeit ist die Schaffung eindeutiger Begriffe mit präziser Aussage erforderlich. Auf die auf diesem Gebiete vorliegenden Arbeiten wird hingewiesen.
Von ausschlaggebender Bedeutung ist die Ordnung und Aufschlüsselung des Gesamtgebietes, damit die Schrifttumsangaben schnell, sicher und zuverlässig geordnet und wieder gefunden werden können. Die bereits vorhandenen Ordnungssysteme werden kurz gekennzeichnet.
Die Prüfprobleme bei Verbundwerkstoffen sind im wesentlichen bestimmt durch die Zweckbestimmung des betreffenden Gegenstandes, die materielle und organisatorische Basis für die Verwirklichung des Vorhabens, die untersuchende und vergleichende Auswahl geeigneter Stoffe und Verarbeitungsverfahren und durch die bestätigende und deshalb meist komplexe Prüfung seiner Funktion mit vorgegebenem Leitwert und darauf bezogenen Variablen bei oft nicht als Konstanten beherrschbaren Parametern.
Die erfolgreiche Lösung einer solchen Aufgabe setzt voraus die ausreichende Kenntnis physikalischer, chemischer, mechanischer und technologischer Eigenschaften von verfügbaren und preiswürdigen Stoffen und Stoffzuständen, deren Beeinflußbarkeit und deren Auswirkungen auf den angestrebten Zweck einschließlich erwünschter belangloser oder auch unerwünschter aber erträglicher oder zusätzlich zu kompensierender Nebenwirkungen. Dafür wiederum braucht man ausreichende qualitative und quantitative Vorstellungen über die mit der angestrebten Funktion zusammenhängenden physikalischen Vorgänge, mechanischen Anstrengungen und chemischen Einwirkungen in dem so bedingten Verbundsystem von Werkstoffen entsprechender Eigenschaften. Aufgaben dieser Art sind z. B. Konstruktionen für die Wandlung, Verteilung, Nutzung oder Abwehr von Energie für die Herstellung, die Verarbeitung und den Transport von Stoffen, für die Darstellung von Wohnung, Kleidung und Nahrung sowie jener materiellen und organisatorischen Voraussetzungen, die dem Menschen als Gesellschaftswesen und über den physischen Bereich hinaus dienen.
Hinweisende Beispiele zeigen, daß die Problematik der Prüfung von Verbundwerkstoffen am zuverlässigsten erfaßt und beherrscht werden kann, wenn die Kenntnis der Eigenschaften von Stoffen und Materialien dem konstruktiv zu behandelnden Funktionszweck entspricht, dadurch eine souveräne Auswahl im Sinne einer weiter reichenden Kombination einzelner hervorragender Eigenschaften möglich ist und das Geplante als geschaffene Wirklichkeit durch den prüfenden Versuch und die beobachtete Bewährung bestätigt wird.
Eine auf den Werkstoff und seine Umwelteinflüsse bezogene Festigkeitsforschung muß auf Vorgänge im elastischen und im überelastischen Beanspruchungsbereich in gleicher Weise bezogen sein. Merkformeln für mechanische Untersuchungen, Parameterwahl und mögliche Zusammenhänge erleichtern die jeweilige Problemstellung, die Kombination entsprechender Untersuchungsverfahren und die Auswahl oder die Entwicklung geeigneter Prüf-, Registrier- und Auswertgeräte.
Beispiele aus der mechanischen Werkstoffprüfung lassen Vorstellungen ableiten über die Vielfalt und die unterschiedlichen Leistungen solcher Untersuchungseinrichtungen. Vor allem interessieren dabei die Beziehungen zwischen der Formänderung und dem Formänderungswiderstand von Proben aus Stoffen und Gemengen und von Konstruktionen bei ein- und mehrachsiger, elastischer und überelastischer, bei zügiger, ruhender, schwingender und stoßförmiger Beanspruchung bis zum Versagen durch unzulässig große Gestaltänderungen, durch Erschöpfen des Formänderungsvermögens, durch Zerrütten der Werkstoffestigkeit oder durch spröden Bruch. Daraus folgt, daß umfangreiche Stoff- und Materialdaten als Grundlage für die zuverlässige und erfolgreiche Prüfung von Werkstoffen und daraus meist im Verbund hergestellten Konstruktionen verfügbar sein sollten. Dafür wiederum ist erforderlich die Beschreibung der Werkstoffe selbst, der für ihr Festigkeitsverhalten typischen Beanspruchungen von zusätzlich einwirkenden Variablen und von Parametern einschließlich der Besonderheiten langer Einwirkungsdauer. Mit dem Denken in solchen Zusammenhängen können grundsätzliche Folgerungen für die Beurteilung und für die Entwicklung von Prüfmaschinen und Geräten gewonnen werden.
Eine auf den Werkstoff und seine Umwelteinflüsse bezogene Festigkeitsforschung muß auf Vorgänge im elastischen und im überelastischen Beanspruchungsbereich in gleicher Weise bezogen sein. Merkformeln für mechanische Untersuchungen, Parameterwahl und mögliche Zusammenhänge erleichtern die jeweilige Problemstellung, die Kombination entsprechender Untersuchungsverfahren, die Auswahl oder die Entwicklung geeigneter Prüf-, Registrier- und Auswertgeräte sowie die auch auf komplexe Probleme gerichteten Schlußfolgerungen.
Beispiele aus der mechanischen Werkstoffprüfung lassen Vorstellungen ableiten über die Vielfalt, die Möglichkeiten und die Notwendigkeit solcher Untersuchungsmethoden. Vor allem interessieren dabei die Beziehungen zwischen der Formänderung und dem Formänderungswiderstand von Proben aus Stoffen und Gemengen und von Konstruktionen bei ein- und mehrachsiger, elastischer und überelastischer, bei zügiger, ruhender, schwingender und stoßförmiger Beanspruchung bis zum Versagen durch unzulässig große Gestaltänderungen, durch Erschöpfen des Formänderungsvermögens, durch Zerrütten der Werkstoffestigkeit oder durch spröden Bruch. Daraus folgt, daß umfangreiche Stoff- und Materialdaten als Grundlage für die zuverlässige und erfolgreiche Prüfung von Werkstoffen und daraus meist im Verbund hergestellten Konstruktionen verfügbar sein sollten. Dafür wiederum ist erforderlich die Beschreibung der Werkstoffe selbst, der für ihr Festigkeitsverhalten typischen Beanspruchungen von zusätzlich einwirkenden Variablen und von Parametern einschließlich der Besonderheiten langer Einwirkungsdauer. Mit dem Denken in solchen Zusammenhängen können grundsätzliche Folgerungen für die Beurteilung der Problemstellung, für die Entwicklung geeigneter Lösungen und für das Erfassen grundsätzlicher Erkenntnisse gewonnen werden. Diese Möglichkeiten gelten in gleicher Weise für die Stoffkunde, für die Werkstoff- und damit auch für die Fügetechnik, für die Festigkeitsforschung und damit für die dabei überall mitwirkende Materialprüfung ebenso wie auf deren Verfahren, Geräte und Einrichtungen.
The radiation-induced degradation of PMMA is known to be inhibited by low-molecular-weight substances, mainly of aromatic structure. In the case of linear and angular condensated aromatic compounds a protection of 80 % was attained. The efficiency is proportional to the concentration up to beginning saturation. Its dependence from resonance energy and from the first excited singulet state allows the conclusion that the additives act by means of excitation transfer and radical scavenging. The yield of chain-scissions is noticed to be constant up to high doses. This suggests that the additives are not destroyed by reason of the considerable radiation resistance of aromatic compounds. The fact that the mixtures are more intensively coloured than the pure polymer in spite of lower degradation is in contradiction to this assumption. This colouration, not noticed at the pure additives at corresponding doses, is a sign of a significant decomposition of the additives combined with the protection of the polymer against degradation. The object of our investigation was to study this connection in detail with special regard to energy transfer.
Wir beehren uns, die Mitarbeiter und Freunde der Bundesanstalt für Materialprüfung, die Mitglieder und Freunde des Deutschen Verbandes für Materialprüfung, die Mitarbeiter des Fachnormenausschusses Materialprüfung und die interessierten Fachkollegen aus der Wissenschaft, Technik und Wirtschaft des In- und Auslandes herzlich zu den Veranstaltungen anläßlich der gemeinsamen Jubiläen einzuladen:
- 100 Jahre Bundesanstalt für Materialprüfung (BAM),
- 75 Jahre Deutscher Verband für Materialprüfung (DVM) und
- 25 Jahre Fachnormenausschuß Materialprüfung im DNA,
- in Verbindung mit der Deutschen Industrie-Ausstellung Berlin 1971 unter dem Leitthema: "Werkstoffe - erforscht, geprüft, verarbeitet",
- in Berlin vom 8. bis 12. November 1971.