Ingenieurwissenschaften und zugeordnete Tätigkeiten
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- 2019 (16) (entfernen)
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- Laser implantation (8)
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Eingeladener Vortrag
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In einer Vielzahl technischer Anwendungen spielt die Aufrechterhaltung eines definierten Reibungs- und Verschleißverhaltens zwischen bewegten Oberflächen für die Sicherheit und Funktionalität eine ent-scheidende Rolle. Die Oberflächentechnik versucht durch geeignete Verfahren die Randschichten zu ertüchtigen, um Reibung und Verschleiß zu kontrollieren. Eine Verbesserung der Materialeigenschaften kann durch flächige Beschichtungen erreicht werden. Zusätzlich ermöglichen Oberflächenstrukturierun-gen breite Möglichkeiten zur Beeinflussung des Schmierungszustandes bzw. der Kontaktbedingungen. Neben Negativstrukturen bieten ebenfalls erhabene Mikrostrukturen großes Potenzial zur Beeinflussung des tribologischen Verhaltens. Ihr Einsatz ist aber aufgrund der besonderen Verschleißproblematik er-habener Strukturen momentan limitiert, so dass in der Regel zusätzliche verschleißreduzierende Be-schichtungen notwendig werden.
In diesem Beitrag wurde das Verfahren der Laserimplantation angewandt, mit dem erhabene und sepa-rierte Oberflächenstrukturen hoher Verschleißfestigkeit in einem Fertigungsschritt erzeugbar sind. Das Verfahren basiert auf einem lokalisierten Dispergieren von Hartstoffpartikeln. Hierfür wurde erstmalig ein gepulster Faserlaser mit hoher Strahlqualität zur Erzeugung punkt- und linienförmiger Mikrostrukturen angewandt. Versuche wurden auf dem Kaltarbeitsstahl X153CrMoV12 unter Anwendung von Titandibo-rid als Hartstoff durchgeführt. Anhand von Härtemessungen konnte gezeigt werden, dass sowohl punkt- als auch linienförmige Strukturen mit Härten über 1000 HV1 und einer feinkörnigen Mikrostruktur mit feinverteilten Hartstoffpartikeln herstellbar sind. Des Weiteren war es möglich, die Implantgeometrien, welche an Querschliffen und durch Weißlichtinterferometeraufnahmen erfasst wurden, durch die Puls-leistung und Pulsdauer zu steuern.
AISI D2 is one of the most applied cold-working tool steel for deep drawing operations, due to the materials good toughness and high wear resistance. However, since the lubricant-free deep drawing as well as the processing of high strength and ultra-high strength steel sheets remaining ongoing trends in the automotive industry, the tool surfaces need to be improved regarding their friction and wear behavior. For this purpose elevated micro textures can be applied. Since protruded micro features are predominantly affected by wear, a structuring process enabling the formation of suitable textures with high wear resistance is needed.
In this paper surface texturing at microscale was conducted by laser implantation. This technique allows the fabrication of highly wear resistant, separated and elevated features (implants) on steel surfaces via a discontinuous dispersing of ceramic particles by pulsed laser radiation. The aim of this study was to investigate the techniques potential for the creation of wear resistant elevated micro features on AISI D2 tool steel surfaces by the application of TiB2 particles. The laser parameters (pulse power and length) were varied and a comparative material analysis on AISI D2 laser remelted spots and TiB2 localized dispersed zones was examined. High-speed camera recordings allowed the description of the particle insertion mechanism from pre-coatings during laser processing. Mechanical properties were analyzed by (micro-) hardness measurements at top and cross sections. The microstructure was investigated by optical microscopy, scanning electron microscopy (SEM), energy dispersive Xray
spectroscopy (EDX) and X-ray diffraction (XRD). The implants geometrical properties (diameter, height, depth) were investigated by white light interferometry and optical microscopy. The experiments reveal that a pulsed laser remelting of AISI D2 leads to a significant hardness drop due to high retained austenite (γR) contents. Contrary, a localized dispersing of TiB2 particles leads to defect free dome- or ring-shaped elevated features with hardness values up to 1800 HV1. The high hardness values result from the dispersed TiB2 particles and an in-situ precipitation of new hard particle phases, which lead to a reduction of the γR content within the matrix.
Elektromagnetische Porenreduktion beim Laserstrahlschweißen von Aluminium-Druckgusslegierungen
(2019)
Innerhalb der vorliegenden Untersuchung wurde ein elektromagnetisches Schmelzbadbeeinflussungssys-tem zur Reduktion des Porenanteils beim Laserstrahlschweißen von Aluminium-Druckguss verwendet. Hierbei wird der Unterschied der elektrischen Leitfähigkeiten zwischen Gas- bzw. Lufteinschlüssen und geschmolzenem Aluminium gezielt genutzt, um die im Schmelzbad eingeschlossenen Poren während des Laserstrahlprozesses zur Oberfläche zu verdrängen. Die dafür erforderlichen Lorentzkräfte werden durch ein oszillierendes Magnetfeld erzeugt. Bei den Laserstrahlschweißversuchen handelt es sich um Ein-schweißungen in Wannenlage (PA-Position) von 6 mm dickem Aluminium-Druckguss AC-AlSi9MnMg. Über einen zuvor optimierten Laserschweißprozess wurde durch zusätzlichen Einsatz eines elektromag-netischen Feldes dessen Wirkung hinsichtlich des Porengehaltes und der Oberflächenrauheit untersucht. Die Auswertung der Schweißnähte erfolgte anhand von Querschliffaufnahmen, Röntgenbildern sowie Computer-Tomographie (CT) Aufnahmen. In Abhängigkeit von der verwendeten magnetischen Fluss-dichte konnte eine Reduktion des Porenanteils von bis zu 75 % erzielt werden, wobei vor allem großvolu-mige Poren erfolgreich aus dem Schmelzbad entfernt werden konnten. Zudem konnte eine Reduktion der Oberflächenrauigkeit von ebenfalls bis zu 75 % erreicht werden.
As humanity contemplates manned missions to Mars, strategies need to be developed for the design and operation of hospitable environments to safely work in space for years. The supply of spare parts for repair and replacement of lost equipment will be one key need, but in-space manufacturing remains the only option for a timely supply. With high flexibility in design and the ability to manufacture ready-to-use components directly from a computeraided model, additive manufacturing (AM) technologies appear extremely attractive. For the manufacturing of metal parts, laser-beam melting is the most widely used AM process. However, the handling of metal powders in the absence of gravity is one prerequisite for its successful application in space. A gas flow throughout the powder bed is successfully applied to compensate for missing gravitational forces in microgravity experiments. This so-called gas-flow-assisted powder deposition is based on a porous Building platform acting as a filter for the fixation of metal particles in a gas flow driven by a pressure difference maintained by a vacuum pump.
The paper describes a systematic investigation of the EM influenced laser beam welding of the aluminum die casting alloy AlSi12(Fe) in comparison to a reference material, a wrought aluminum alloy AlMg3. By using of a face centred CCD test plan, the influencing variables laser power, welding velocity and magnetic flux density are varied with regard to their influence on the remaining porosity. The global pore fraction of the weld seams was analyzed by X-ray images with ImageJ. This enabled a qualitatively very good regression model to be derived for the respective material, which identifies the dominant influencing variables. The results prove, statistically verified, for the investigated parameter range, that
- the magnetic flux density is the main cause for the porosity reduction,
- the porosity rises with increasing laser power the porosity in the weld seams rises,
- the influence of the welding velocity is negligible,
- the pore quantity in wrought alloy is more strongly minimized by the magnetic flux density than in die casting,
- the porosity decreases due to the EM influence by approx. 70 % compared to the unaffected welds. This effect is emphasized by the contour line charts, which illustrate the relationship between laser power and magnetic flux density.
With the exception of the quadratic influence of B at the wrought alloy, the statistical correlation shows a linear development of the respective influence variables for both aluminum alloys. In order to investigate these deviations, further simulations with a focus on weld pool geometry and weld pool flow are to be performed. In addition, the welding results can be classified in accordance with DIN EN ISO 13919-2 in the highest evaluation group B for AlMg3 and in evaluation group C for AlSi12(Fe) by applying a magnetic flux density of 350 mT. The analysis of the CT images at constant laser power and welding velocity allows a direct comparison both between the two alloys and also as a function of the magnetic flux density with regard to the number and size of pores. An increase in the magnetic flux density leads to a significant decrease in the number and volume of pores, which can be seen more clearly in wrought alloy than in die casting. Very acceptable results can be achieved for both materials and different welding parameters. This successfully demonstrates the desired process robustness and functionality of the EM system for practical applications. For subsequent investigations of overlap joints, the lowest possible laser power and a high magnetic flux density are recommended.
The potential of lowered surface features as well as the application of wear resistant coatings have been known for many years to improve the tribological behavior of forming tools. More recent studies also discuss the capability of protruded microfeatures for adjusting the tribological behavior between contacting surfaces. The demand for a high wear resistance of such structures as well as their economical and reliable production, however, often limits the industrial application. The laser implantation process can overcome these limitations. In contrast to conventional cw-laser dispersing processes, where the formation of uniform metal matrix composite layers is intended, this surface engineering technique aims to improve the tribological behavior of contacting surfaces by a localized dispersing of pre-placed hard ceramic particles. This enables the formation of deterministic textures composed of separated wear resistant dome- or ring-shaped microstructures (implants).
Since TaC shows very promising material properties for improving the wear resistance of tools exposed to severe operating conditions, this paper analyzes its suitability for pulsed laser implantation on X38CrMoV5-3 tool steel for the first time. In the experiments, the influence of the particles and the laser parameters (pulse power, pulse duration and focal diameter) on the material properties of the localized dispersed zones was studied by optical microscopy, scanning electron microscopy, energy dispersive X-ray spectroscopy and X-ray diffraction. The composite´s (micro-) hardness was measured and calculated by using a rule of mixture. Additionally, the influence of the laser parameters and the TaC particles on the geometrical properties of the implants was studied by optical microscopy and white light interferometry.
The results showed that defect-free implants with hardness values of ~900 HV1 can be obtained at the focal spot, since a localized dispersing of the TaC particles is possible using a pulsed millisecond laser. However, in dependence of the laser intensity, also a partial dissolution of the initial particles occurs. This leads to the precipitation of new dendritic TaC nanoparticles and to varying contents of retained austenite in the matrix. Both effects have a strong influence on the implant hardness and must be considert by the rule of mixture. Regarding the geometrical response it was pointed out that protruded microfeatures with heights up to 10 µm can be created. In comparison to laser remelted zones, the implanted zones showed significantly altered weld pool profiles due to the influence of the particles on the melt convection. A transition of the implant shape from predominantly dome-shaped to predominantly ring-shaped was observed for intensities >1.7∙106 W/cm2 due to the onset of the keyhole effect.
The laser implantation technique bases on a localized dispersing of ceramic particles in metallic surface layers for changing their micro geometry as well as their material properties. Using TiB2 and NbC hard particles, tailored microtextures consisting of elevated dome-, ring-, or line-shaped Features can be manufactured. Especially TiB2 implants feature high hardness values up to 1800 HV1 and ceramic particle contents up to 55 %, indicating superior wear resistant properties.
Die Laserimplantation erlaubt die Herstellung verschleißbeständiger, erhabener Mikrostrukturen (Implants) auf Stahloberflächen durch ein diskontinuierliches Dispergieren von keramischen Partikeln mittels gepulster Laserstrahlung. Durch die flexible Anordnung separierter Implants zu komplexen Mustern erlaubt das Verfahren eine gezielte Oberflächenstrukturierung zur Beeinflussung des Reibungs- und Verschleißverhaltens. Insbesondere erwies sich Titandiborid (TiB2) als Implantationsmaterial für geeig-net, da eine Manipulation der Implantgeometrie in einem breiten Bereich vorgenommen werden konnte, ohne dass Materialdefekte wie Risse oder Poren auftraten.
Ziel der Untersuchungen war es, den Einfluss implantierter TiB2-Partikel auf die Materialeigenschaften von X153CrMoV12 zu ermitteln. Hierfür wurden im Rahmen der Arbeit die Laserparameter (Pulsleistung und -dauer) in einem breiten Parameterfeld variiert und vergleichende Untersuchungen an TiB2 implan-tierten Zonen sowie an punktuell umschmelzstrukturierten Zonen durchgeführt. Die Ergebnisse zeigen, dass eine reine Umschmelzstrukturierung zu einer deutlichen Reduktion der Oberflächenhärte aufgrund erhöhter Restaustenitgehalte (γR) führt. Im Gegensatz dazu führt das Laserimplantieren von TiB2-Partikeln zu einer deutlichen Härtesteigerung in den kuppel- oder ringförmigen Implants. Härtewerte von bis zu 1800 HV1 resultieren aus dispergierten TiB2-Primärpartikeln sowie in-situ ausgeschiedenen Se-kundärphasen, durch die der Restaustenitanteil zudem deutlich reduziert wird.
Localized laser surface treatments are able to produce tailor-made surface properties to fulfill requirements of a variety of technical applications. Especially micrometric surface topologies can be beneficial for optimizing tribological contact situations. Structures with lowered surface features are already utilized for bearings or cylinders of combustion engines. There are also other fields of application, where the potential of protruding surface features is known, e. g. for metal forming tools.
A promising approach for a tailored surface treatment working in the microsecond range is the localized dispersing of hard ceramic particles by pulsed laser radiation, the so-called laser implantation. This technique is able to produce micrometric surface structures and to improve simultaneously the wear resistance by creating metal matrix composites.
In this talk, the laser implantation technique is described and compared to the state of the art. The potential to adjust the geometry as well as the mechanical properties of laser implanted surfaces is demonstrated by means of microstructural and topographical investigations of different ceramic materials and steel substrates. Finally, results of research projects are presented aiming on the application of such structured surfaces. Their capability to change and optimize friction and wear are demonstrated for fully lubricated contacts, tools for hot sheet metal forming and tools for cold rolling of sheets for automotive applications.