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Erscheinungsjahr
- 2017 (244) (entfernen)
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- Zeitschriftenartikel (244) (entfernen)
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- Englisch (218)
- Deutsch (23)
- Russisch (2)
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- Nanoparticle (11)
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- Mechanochemistry (9)
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- KorroPad (7)
- SAXS (7)
- Small-angle X-ray scattering (7)
- Korrosionsschnelltest (6)
- NIR (6)
Ellipsometry is a useful tool for studying the optical properties of thin films such as photovoltaic devices. We employ Müller matrix ellipsometry to study the thin film photovoltaic material copper indium gallium selenide Cu(In,Ga) Se2 (CIGS), a commercially relevant material with high energy conversion efficiency. Confocal microscopy reveals an rms roughness of 68 nm, which greatly affects the ellipsometry data. Rayleigh-Rice theory is employed to account for the optical properties of the surface roughness in the ellipsometry experiment, and a library search method is used to compare Müller parameters calculated for various CIGS compositions, to the measured data. The Müller parameters calculated with the Rayleigh-Rice model are found to correspond well with the measured data, and a surface roughness of 37nm and a correlation length of 125nm are extracted.
Szczerba, Wojciech ; Schneider, M. ; Żukrowski, J. ; de Oliveira Guilherme Buzanich, Ana ; Riesemeier, Heinrich ; Sikora, M. ; Mandel, K.
Currently great effort is made to find materials and technologies for the recycling of phosphate from wastewater.
Herein, we present an in-depth study of the Phosphate adsorption mechanism of a promising adsorber material, a Zn−Fe−Zr oxyhydroxide-based nanostructured precipitate. The behavior of the multicomponent nanomaterial, consisting of both crystalline and amorphous parts, is investigated via X-ray absorption fine structure spectroscopy and Mössbauer spectroscopy, revealing the importance of the nanostructured composition for the phosphate adsorption. We found evidence that adsorption takes place especially in the vicinity of iron sites in the amorphous part of the material.
Detection of the electronic structure of iron-(III)-oxo oligomers forming in aqueous solutions
(2017)
Seidel, R. ; Kraffert, K. ; Kabelitz, Anke ; Pohl, M.N. ; Kraehnert, R. ; Emmerling, Franziska ; Winter, B.
The nature of the small iron-oxo oligomers in iron-(III) aqueous solutions has a determining effect on the chemical processes that govern the formation of nanoparticles in aqueous phase. Here we report on a liquid-Jet photoelectron-spectroscopy experiment for the investigation of the electronic structure of the occurring iron-oxo oligomers in FeCl3 aqueous solutions. The only iron species in the as-prepared 0.75 M solution are Fe3+ monomers. Addition of NaOH initiates Fe3+ hydrolysis which is followed by the formation of iron-oxo oligomers. At small enough NaOH concentrations, corresponding to approximately [OH]/[Fe] = 0.2–0.25 ratio, the iron oligomers can be stabilized for several hours without engaging in further aggregation. Here, we apply a combination of non-resonant as well as iron 2p and Oxygen 1s resonant photoelectron spectroscopy from a liquid microjet to detect the electronic structure of the occurring species. Specifically, the oxygen 1s partial electron yield X-ray absorption (PEY-XA) spectra are found to exhibit a peak well below the onset of liquid water and OH (aq) absorption. The iron 2p absorption gives rise to signal centered between the main absorption bands typical for aqueous Fe3+. Absorption bands in both PEY-XA spectra are found to correlate with an enhanced photoelectron Peak near 20 eV binding energy, which demonstrates the sensitivity of resonant photoelectron (RPE) spectroscopy to mixing between iron and ligand orbitals. These various signals from the iron-oxo oligomers exhibit Maximum intensity at [OH]/[Fe] = 0.25 ratio. For the same ratio, we observe changes in the pH as well as in complementary Raman spectra, which can be assigned to the Transition from monomeric to oligomeric species. At approximately [OH]/[Fe] = 0.3 we begin to observe particles larger than 1 nm in radius, detected by small-angle X-ray scattering.
The syntheses, structures, and photophysical properties of two new zinc(II) complexes bearing the tridentate N,N′-dimethyl-N,N′-dipyridin-2-ylpyridine-2,6-diamine (ddpd) ligand are presented. Structural investigations through single-crystal X-ray diffractometry, NMR spectroscopy, and density functional theory calculations revealed a diverse coordination behavior that depends on the counterion. Spectroscopic (UV/Vis and emission spectroscopy) and theoretical techniques (DFT and time-dependent DFT calculations) were employed to explore the photophysical properties of the complexes.
Dong, S. ; Leng, J. ; Feng, Y. ; Liu, M. ; Stackhouse, C. J. ; Schönhals, Andreas ; Chiappisi, L. ; Gao, L. ; Chen, W. ; Shang, J. ; Jin, L. ; Qi, Z. ; Schalley, C. A.
Although the concept of structural water that is bound inside hydrophobic pockets and helps to stabilize protein structures is well established, water has rarely found a similar role in supramolecular polymers. Water is often used as a solvent for supramolecular polymerization, however without taking the role of a comonomer for the supramolecular polymer structure. We report a low–molecular weight monomer whose supramolecular polymerization is triggered by the incorporation of water. The presence of water molecules as comonomers is essential to the polymerization process. The supramolecular polymeric material exhibits strong adhesion to surfaces, such as glass and paper. It can be used as a water-activated glue, which can be released at higher temperatures and reused many times without losing its performance.
Data correction is probably the least favourite activity amongst users experimenting with small-angle X-ray scattering: if it is not done sufficiently well, this may become evident only during the data analysis stage, necessitating the repetition of the data corrections from scratch. A recommended comprehensive sequence of elementary data correction steps is presented here to alleviate the difficulties associated with data correction, both in the laboratory and at the synchrotron. When applied in the proposed order to the raw signals, the resulting absolute scattering cross section will provide a high degree of accuracy for a very wide range of samples, with its values accompanied by uncertainty estimates. The method can be applied without modification to any pinhole-collimated instruments with photon-counting direct-detection area detectors.
Anlagenkomponenten aus nichtrostendem Stahl sind durch eine Passivschicht auf der Oberfläche vor Korrosion geschützt. Ist diese unvollständig ausgebildet oder beschädigt, geht der Schutz verloren.
Hohe Investitionen für Reparaturen und Instandhaltung können die Folge sein. TÜV Süd Chemie Service beteiligte sich an der Prüfung eines von der Bundesanstalt für Materialforschung und -prüfung (BAM) entwickelten Verfahrens zur Charakterisierung der Korrosionsbeständigkeit der Passivschicht. Der KorroPad-Schnelltest liefert in nur 15 Minuten ein valides Prüfergebnis.
Rostfreie Stähle werden in prozesstechnischen Anlagen oft extremen Umgebungsbedingungen ausgesetzt. Eine schützende Passivschicht an der Oberfläche nichtrostender Stähle sorgt dafür, dass es zu keiner Materialauflösung kommt. Wenn diese unvollständig oder beschädigt ist, kann es zu Komplikationen kommen. Lesen Sie im Artikel, wie die von TÜV SÜD Chemie Service erprobte Methode funktioniert, mit der die Passivschicht überprüft werden kann.
Rohrsysteme und Behälter aus nichtrostendem Stahl sind mit einer Passivschicht vor Korrosion geschützt. Ist diese jedoch unvollständig ausgebildet oder beschädigt, geht der Schutz verloren. Das KorroPad-Verfahren ist ein Schnelltest zur Überprüfung der Passivschicht. Im Vergleich mit bisher üblichen Bewertungsmethoden ist die Anwendung sehr einfach und nimmt nur 15 Minuten in Anspruch.