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In this study, quasi-static material tests on unidirectional and multi-angle glass fiber reinforced epoxy laminates at ambient temperatures from -213 K to 353 K (-60 °C to +80 °C) are performed. In addition, neat resin is investigated under tension and compression loads at different temperatures. The coefficient of thermal expansion is determined for neat resin and unidirectional reinforced specimens. The dependence of the resin’s thermomechanical properties on the ambient temperature is shown. The point of damage onset at which first cracks appear within the matrix under quasi-static loading is investigated by means of optical grey scale analysis. The correlation between damage onset and effective matrix stress at different ambient temperatures is identified. An approach for the calculation of thermomechanical loads and the prediction of the damage onset by means of inverse calculations is presented. The impact of the strain blocking effect of the matrix is considered as well as residual thermal stresses due to curing and resin shrinkage.
In this study, quasi-static material tests on unidirectional and multi-angle glass fiber reinforced epoxy laminates at ambient temperatures from -213 K to 353 K (-60 °C to +80 °C) are performed. In addition, neat resin is investigated under tension and compression loads at different temperatures. The coefficient of thermal expansion is determined for neat resin and unidirectional reinforced specimens. The dependence of the resin’s thermomechanical properties on the ambient temperature is shown. The point of damage onset at which first cracks appear within the matrix under quasi-static loading is investigated by means of optical grey scale analysis. The correlation between damage onset and effective matrix stress at different ambient temperatures is identified. An approach for the calculation of thermomechanical loads and the prediction of the damage onset by means of inverse calculations is presented. The impact of the strain blocking effect of the matrix is considered as well as residual thermal stresses due to curing and resin shrinkage.
Potential of martensitic stainless steel X5CrNiCuNb 16-4 as pipe steel in corrosive CCS environment
(2017)
Pipe steels suitable for carbon capture and storage technology (CCS) require resistance against the corrosive environment of a potential CCS-site (heat, pressure, salinity of the aquifer, CO2-partial pressure). X5CrNiCuNb16-4 has been proven to be sufficient resistant in corrosive environments, but shows rather unusual corrosion behaviour in CCS environment. Therefore differently heat treated coupons of 1.4542 were kept at T=60 °C and ambient pressure as well as p=100 bar for 700 h - 8000 h in an a) water saturated supercritical CO2 and b) CO2-saturated synthetic aquifer environment similar to on-shore CCS-sites in the Northern German Basin. Additionally fatigue tests were performed via push-pull tests with a series of 30 specimens was tested at stress amplitudes between 150 MPa and 500 MPa (sinusoidal dynamic test loads, R=-1; resonant frequency ~ 30 Hz). Best corrosion resistance in the liquid phase is achieved via normalizing prior to exposure and hardening+tempering at 670 °C leads to lowest corrosion rates in the supercritical phase. With no regard to atmosphere discontinuously ellipsoidal surface corrosion regions appear after exposure of 4000 h and more. The endurance limit of X5CrNiCuNb16-4 measured in air is reduced by more than 50% when exposed to CCS environment (maximum number of cycles (10 x 106) at a stress amplitude of 150 MPa) The scatter range TN = 1:34 is disproportionately large contributing to an overall unusual corrosion behaviour.
This paper focuses on the aspect on how damage evolution processes in composite materials and structures including matrix fracture, delamination, fibre-matrix debonding, and fibre fracture can be detected by taking advantage of the material’s inherit mechanical properties. These properties can be described on the basis of non-linear mechanical phenomena measurable as an inert frequency response signal. The approach is proposed as a means for residual life structural assessment specifically in the context of VHCF.
In Germany the damages on concrete motorways have increased during the past 15 years. This led often to a reduction of service life from 30 to 10 years. In spite of comprehensive research the reasons for these damages have not been clarified yet. But it is known that in this context the ASR plays a decisive role. Against this background ASR performance tests have been developed. However, these tests do not take into account the effects of mechanical loading due to cyclic traffic and climatic impact. Therefore in Germany the ASR research group 1498 was founded. The research group consists of three experimentally- and two multi-scale modelling oriented subprojects, which are working closely together. Selected findings of BAM’s experimental subproject SP4 are content of this contribution. The aim was to investigate the impact of a cyclic mechanical pre-damage on moisture transport. The pre-damaging was carried out on large-format beams using a cyclic four point bending test with a total number of 5 million load cycles. Thereby the damage process was monitored by using different NDT-techniques. After the mechanical pre-damaging, smallsized specimens were taken from loaded as well as unloaded areas of the large format beams. Absorption tests were carried out on these specimens using water and NaCl solution. Thereby moisture distribution was measured with Nuclear Magnetic Resonance (NMR) and Time Domain Reflectometry (TDR). Additionally, moisture suction was quantified integrally by means of gravimetric measurements. The analysis of the first test data shows that the mechanical loading influences the moisture transport.
Using continuum damage mechanics (CDM) for lifetime prediction requires numerical integration of evolving damage until the onset of failure. The primary challenge for the simulation of structural fatigue failure is caused by the enormous computational costs due to cycle-by-cycle temporal integration throughout the whole loading history, which is in the order of 103–107 cycles. As a consequence, most approaches circumvent this problem and use empirical methods such as Wöhler curves. They are well suited for approximating the lifetime, but they are not capable to capture a realistic degradation of the material including redistribution of stresses. The main objective of the paper is to provide a technique for finite element (FE) simulations of structures under fatigue loading while reducing computational costs.
A Fourier transformation-based temporal integration (FTTI) scheme is proposed, which adapts the conventional FE method for modeling the viscoplastic deterioration in a structure subjected to cyclic loading. The response fields are represented by a Fourier series which assumes a temporal scale separation: a microchronological (short time) scale arises from the oscillatory loading and a macrochronological (long time) scale is due to the slow material relaxation resulting from yielding and damage evolution. The original dynamic boundary value problem (BVP) is approximated by the stationary BVP on the microchronological scale. Alternation of the displacement field on the macrochronological scale is correlated with evolution of the history variables by means of a high order adaptive cycle jump method. Performance and significant acceleration of the FE simulations is demonstrated at different loading scenarios for a constitutive damage model where the progressive damage accumulation is driven by viscoplastic yielding.
The fatigue behaviour of cast iron is usually investigated on machined specimens. Components of cast iron, however, have a casting skin; therefore the investigation of the influence of the casting skin on the lifetime is of interest. To study this influence isothermal fatigue tests were carried out on heat-resisting spheroidal graphite cast iron EN GJS SiMo 4.05 in 4–point-bending set-up at 400 °C. Specimens with and without casting skin were investigated comparatively. The number of cycles to failure was significantly lower for specimens with casting skin. Metallographic investigations underline the reduction of lifetime caused by casting skin.
The current knowledge about fatigue behavior of concrete is still incomplete. This concerns especially the progress of fatigue which precedes the fatigue failure. Therefore, the process of fatigue itself under cyclic compressive loading was investigated in a systematic and comprehensive way. The aim of this investigation was to obtain a deeper insight and to provide a better understanding of the damage process occurring within the material during fatigue loading. Concrete cylinders were tested with a number of cycles to failure between 1E6 and 1E7. To investigate macroscopic and microscopic changes in the material, various methods of non-destructive and destructive testing were used. One main result was, in contrast to other authors, that the investigated changes in macroscopic material behavior could not be explained only by a development of micro-cracks. The results indicated rather, that the related changes in the fatigue behavior are mainly a result of viscous processes in the hardened cement paste, similar to the processes of creep. Based on the experimental results a description of the possible processes was derived which take place in the material structure during fatigue loading and also leads to the observed macroscopic changes in the material behavior. In this context, the results have shown that in case of isotropic material behavior a stiffness reduction related to a scalar value could not capture the damage effect on the stress-strain-relationship caused by fatigue.
Fatigue is of relevance not only for metals but also for concrete. The current knowledge about fatigue behaviour of concrete is, however, incomplete. This concerns especially the progress of fatigue which precedes the fatigue failure. Some macroscopic effects of this process are well known but the governing material changes behind them are still less studied. The focus of the present contribution lay on a systematic and comprehensive investigation of the fatigue process under cyclic compressive loading. The aim was to obtain a deeper insight and to provide a better understanding of the damage process in the material. Cylindrical specimens were tested with a number of cycles to failure between 106 and 107. Various methods of non-destructive and destructive testing were used to investigate macroscopic and microscopic changes in the material. One main result was that the changes in the macroscopic material behaviour could not be explained only by the development of micro cracks. The results indicated that the related changes in the fatigue behaviour originate rather from viscous processes in the cement stone, similar to the process of creep. A sound description of the possible processes was derived from the obtained experimental results which concerns material structure during fatigue loading. It has been shown that in case of isotropic material behaviour a stiffness reduction related to a scalar value could not capture the damage effect on the stress-strain relationship caused by fatigue.
Fatigue is of relevance not only for metals but also for concrete. The current knowledge about fatigue behaviour of concrete is, however, incomplete. This concerns especially the progress of fatigue which precedes the fatigue failure. Some macroscopic effects of this process are well known but the governing material changes behind them are still less studied. The focus of the present contribution lay on a systematic and comprehensive investigation of the fatigue process under cyclic compressive loading. The aim was to obtain a deeper insight and to provide a better understanding of the damage process in the material. Cylindrical specimens were tested with a number of cycles to failure between 106 and 107. Various methods of non-destructive and destructive testing were used to investigate macroscopic and microscopic changes in the material. One main result was that the changes in the macroscopic material behaviour could not be explained only by the development of micro cracks. The results indicated that the related changes in the fatigue behaviour originate rather from viscous processes in the cement stone, similar to the process of creep. A sound description of the possible processes was derived from the obtained experimental results which concerns material structure during fatigue loading. It has been shown that in case of isotropic material behaviour a stiffness reduction related to a scalar value could not capture the damage effect on the stress-strain relationship caused by fatigue.