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Organisationseinheit der BAM
- 6 Materialchemie (207)
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- 1 Analytische Chemie; Referenzmaterialien (46)
- 4 Material und Umwelt (36)
Eingeladener Vortrag
- nein (1)
Methanogenic Archaea
(2017)
Different environmental samples reveal that methanogenic Archaea are part of a multi-species biofilm on corroding metallic structures. Studies on microbial influenced corrosion (MIC) focus mainly on sulphate reducing Bacteria (SRB), leading to the assumption that they are exclusively responsible for metal corrosion. In fact, methanogenic Archaea are known to be involved in metal corrosion as well (e.g. Methanococcus maripaludis DSM 2067). In some cases SRB and methanogenic Archaea have comparable high corrosion rates. However, the underlying mechanisms causing corrosion are still unknown.
The goal of this study is to develop suitable methods for analyzing two environmental isolates (M. maripaludis DSM 2067, M. maripaludis KA1) and two human-related isolates (Methanobrevibacter oralis and Methanobrevibacter smithii) for their ability to deteriorate/transform metals, which are relevant for technical and clinical applications. Moreover, the studies will provide essential information on the interaction mechanisms of human-related Archaea, which are frequently found in peri-implantitis, with dental material such as implants, crowns and bridges leading to their degradation and transformation.
The project has developed a variety of new multifunctional and flexible building components for a healthier indoor environment. [H] house solutions are durable, energy efficient, safe and affordable. They are suitable for use in new buildings and for renovation. [H] house solutions cover aspects of long service life, reduced maintenance and long-term improvement of energy efficiency.
We investigated, the damped Received Signal Strength Indicator (RSSI) of a Bluetooth Low Energy (BLE) signal, transmitted from the BLE-module embedded in building materials with changing moisture content, Fig. 1. The BLE-module communicates with a mobile Smart Device as tablet via 2.45 GHz-ISM-frequency band where water dipoles start to oscillate, Fig. 2. The damping model demonstrates this damping effect on RSSI by the abstraction of the reality observed in a real system. Through the reproduction of the active relationships, the system behavior is decomposed in such a way that a separate consideration of the required system parameters is possible.
Mechanochemistry has become a valuable method for the synthesis of new materials, especially for pharmaceutical cocrystals. The Advantages of fast reactions in high purity and yield face a lack of understanding the underlying mechanism. Therefore, in situ setups to study mechanochemical reactions have been established. Herein, we present an in situ investigation of the mechanochemical cocrystal formation of pyrazinamide (PZA) with pimelic acid (PM) using synchrotron XRD. Two new polymorphs of PZA:PM (1:1) were synthesized by milling the starting materials in milling jars of different materials. While Form I is only obtained using a steel jar, Form II can be obtained purely in jars made of Perspex. In situ XRD experiments reveal a direct formation of Form II in Perspex and an intermediate formation of Form II in steel jars converting to Form I upon further grinding. Heating experiments and DFT calculations predict that Form II is the thermodynamically more stable polymorph. Therefore, the reaction progress in the steel jar contradicts Ostwald’s rules of stages as the more stable Form II converts into the metastable Form I. Hence, mechanochemistry offers the possibility to synthesize new materials that cannot be obtained using conventional methods.
Obtaining high quality upconverting nanocrystals with only little crystal defects and hence, a high luminescence, affords a reliable synthesis route. Only this guarantees the reproducibility of the material and its spectroscopic properties required for future application. The fluorolytic sol-gel synthesis appears to be a convenient attempt, as this is a method with only few steps influencing the material properties, which can be well controlled.
Also creating bright upconverting nanocrystals requires a profound understanding of the interplay of photophysical processes like multiphoton absorption, radiative and non-radiative pathways, and energy transfer in the material.
Based on steady-state and time resolved luminescence measurements at different excitation power densities, the influence of the lanthanide doping ratio and synthesis parameters such as the annealing process on SrF2-nanocrystals obtained via the fluorolytic sol-gel synthesis was systematically studied.
Die Detektion bzw. Charakterisierung von Oberflächenrissen in Stahl ist eine herausfordernde Aufgabe für die zerstörungsfreie Prüfung. Dies gilt insbesondere, wenn eine solche Prüfung bereits während der Produktion selbst erfolgen soll. Die hier vorgefundenen Randbedingungen, wie z.B. die hohen Probentemperaturen (>700°C) oder Vorschubgeschwindigkeiten von bis zu 0,9 m/min, machen die Anwendung etablierter und vor allem berührender ZfP-Methoden praktisch meist unmöglich. Laser-thermografische Verfahren können hier eine Alternative bieten, da sie berührungslos und schnell arbeiten. Wir stellen die Ergebnisse einer Weiterentwicklung der Laser-thermografischen Prüfung vor, bei der die Anwendbarkeit bzw. die Übertragbarkeit der Methode auf die Bedingungen der Stahlproduktion untersucht wurde.
Neben der Simulation der Produktionsbedingungen im Labor und der experimentellen Untersuchung der entscheidenden Einflussgrößen, wurden umfangreiche FEM-Simulationen durchgeführt. Mit Hilfe dieser theoretischen und experimentellen Ergebnisse wurde das Verfahren auch hinsichtlich der Analyse-Algorithmen weiterentwickelt, um eine zuverlässige und schnelle In-Line Prüfung während des Produktionsprozesses zu ermöglichen. Um zudem die Fähigkeiten der Thermografiekamera für schnelle online-Messungen und ihre Integrierbarkeit in verschiedene Anwendungssysteme zu verbessern, wurde die für die Verarbeitung der Detektordaten erforderliche Non-Uniformity Correction der Pixeldaten auf schneller Spezialhardware innerhalb der Kamera implementiert.
In this paper, titanium-di-boride is dispersed on a cold-working tool steel by use of a pulsed fiber laser with high beam quality to produce separated and elevated surface features. The potential to adjust the geometry as well as the mechanical properties of the produced structures in dependence on the process parameters (pulse power, pulse duration) is described by means of metallographic and topographical investigations. It can be ascertained that very hard (hardness > 1000 HV1) surface features of different shape (spots and short lines) can be produced. They are characterized by a fine-grained microstructure resulting from a rapid solidification and finely dispersed TiB2 particles. Finally, the paper proposes different applications for this structuring technique.
Solar glass in arid and semi-arid regions is exposed to sand storms which can affect the durability of PV modules. Related erosion processes have been extensively studied but the results given are difficult to compare due to being obtained by different variables like particle speed and sand mass. This study correlates the damage of solar panels to the cumulative impact energy as a global parameter.
Der nichtrostende Lean-Duplexstahl 1.4062 (X2CrNiN22-2) verbindet die hohe Festigkeit des Ferrits mit der Duktilität und Zähigkeit des Austenits in einem zweiphasigen Gefüge mit sehr hoher Korrosionsbeständigkeit. Die höchste Korrosionsbeständigkeit wird erreicht, wenn das ferritisch-austenitische Gefüge frei von weiteren Sekundärphasen ist. Dies wird durch ein gezieltes Lösungsglühen bei 1050 °C mit anschließender Abschreckung in Wasser erreicht. Durch thermische Beeinflussung (z.B. beim Schweißen) können Sekundärphasen ausgeschieden und die Korrosionsbeständigkeit des Werkstoffs gesenkt werden. Dies wurde durch eine isotherme Warmauslagerung bei 500 °C bis 900 °C für 0,1 h bis zu 72 h simuliert. Die Veränderung der Korrosionsbeständigkeit wurde mit dem DL-EPR-Verfahren und durch die angepasste KorroPad-Prüfung ermittelt. Die ermittelten Anfälligkeitsbereiche wurden miteinander Verglichen und in zwei Sensibilisierungsschaubildern zusammengefasst.
Gefüge und Eigenschaften nichtrostender Stählen werden maßgeblich von ihrer chemischen Zusammensetzung und der Wärmebehandlung bestimmt. Eine spezielle Werkstoffgruppe der austenitischen nichtrostenden Stähle enthält ca. 19 Gew.-% Mangan und 0,8 Gew.-% Stickstoff, um das austenitische Gefüge ohne das Legieren mit Nickel sicherzustellen. Die herausragenden mechanischen Eigenschaften dieser Werkstoffe (Rm von 900 2.000 MPa, A5 > 50 %, Av > 350 J) werden nach der Wärmebehandlung (Lösungsglühen und Abschrecken) durch gezielte Kaltverfestigung eingestellt. Das Lösungsglühen beseitigt vorhandene Kaltverfestigung und unerwünschte Ausscheidungsphasen (Cr2N, M23C6 und Sigma-Phase) und bewirkt die homogene Verteilung der Legierungselemente (insbesondere Stickstoff) im Austenit. Dies ist zur Erzielung der Korrosionsbeständigkeit von entscheidender Bedeutung. Im Poster werden systematische Untersuchungen zur Korrosionsbeständigkeit dieser vielversprechenden Werkstoffklasse vorgestellt und die Interaktion zwischen Legierungszusammensetzung, Wärmebehandlung, Gefüge und Korrosionsbeständigkeit dargestellt. Die vom Gefüge bedingten Veränderungen der Korrosionsbeständigkeit werden durch verschiedene Methoden ermittelt und interpretiert.