Ingenieurwissenschaften und zugeordnete Tätigkeiten
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- 7 Bauwerkssicherheit (6)
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- 5.4 Multimateriale Fertigungsprozesse (5)
- 2 Prozess- und Anlagensicherheit (4)
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- 7.5 Technische Eigenschaften von Polymerwerkstoffen (4)
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- 6.5 Synthese und Streuverfahren nanostrukturierter Materialien (3)
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- 3 Gefahrgutumschließungen; Energiespeicher (2)
- 4.1 Biologische Materialschädigung und Referenzorganismen (2)
- 4.2 Material-Mikrobiom Wechselwirkungen (2)
- 5.5 Materialmodellierung (2)
- 7.1 Baustoffe (2)
- 8.1 Sensorik, mess- und prüftechnische Verfahren (2)
- 9.5 Tribologie und Verschleißschutz (2)
- 1.9 Chemische und optische Sensorik (1)
- 3.1 Sicherheit von Gefahrgutverpackungen und Batterien (1)
- 3.2 Gefahrguttanks und Unfallmechanik (1)
- 4.0 Abteilungsleitung und andere (1)
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- 9.0 Abteilungsleitung und andere (1)
The advantages of treating prefabricated components made of Ultra-High-Performance Concrete (UCPC) at 90 °C are largely recognized, while hydrothermal treatment at 185 °C and the corresponding saturation pressure of 1.1 MPa, in contrast, is not applied in building practice so far and was studied only by a few researchers.
In the research presented, the parameters pre-storage-time before treatment and dwell time in the autoclave were systematically varied. The results illustrate in which way compressive strength increases with the duration of treatment. Already samples which were only heated up and immediately cooled down show an increase in strength compared to the 28-day reference of about 10 %. After 20 h the maximum increase of about 25 % is reached. Interestingly the compressive strength of samples treated very long hardly decreases. It can be therefore concluded that for the composition investigated the achievable mechanical strength is not severely sensitive regarding the duration of the treatment.
Also, pre-storage times before autoclaving longer than 0.5 days showed no significant impact on strength development. The phase composition measured by XRD exhibits significant changes compared to the reference. The amount of ettringite and portlandite have vanished, the cement clinker phases are substantially decreased and hydroxylellestadite and hydrogarnet are formed as new phases. The increase in strength can be assigned to an improved pozzolanic and hydraulic reaction. Contradictory to literature, there was found no obermorite, a mineral which is known to be susceptible for disintegration at Long autoclaving duration. This explains why no significant strength loss appeared.
µCT is used to validate the capability of online monitoring for in-situ detection of defects during the L-PBF build process, which is a focus of the TF project ProMoAM.
Our first experiments show that online monitoring using thermography and optical tomography cameras are able to detect defects in the built part. But further research is needed to understand root cause of the correlation.
The Influence of the Temperature Gradient on the Distribution of Residual Stresses in AM AISI 316L
(2019)
Steep temperature gradients and solidification shrinkage are the main contributors to the formation of residual stresses in additively manufactured metallic parts produced by laser beam melting. The aim of this work was to determine the influence of the temperature gradient.
Diffraction results show a similar pattern for both specimens, indicating the shrinkage to be more dominant for the distribution of residual stresses than the temperature gradient. Thermography results imply that a higher energy input result in higher compressive residual stresses in the bulk.
Fiber reinforced polymers (FRPs) are a well established material in lightweight applications, e.g. in automotive, aerospace or wind energy. The FRP components are subjected to multiaxial mechanical as well as hygrothermal loads. Common operation temperatures are in the range of 213 K and 373 K (-60 °C and 100 °C) at a relative humidity of 10% to 90%. In spacecraft applications, the environmental conditions are even more extreme. However, the correlation between multiaxial mechanical loading and harsh environment conditions have to-date not been investigated in detail. The project aims to investigate the fatigue behavior of FRPs dependent on multiaxial mechanical loading, temperature, and humidity. Extensive experimental testing is performed on flat plate and cylindrical tube specimens, accompanied by numerical and analytical calculations.
19th and 20th centuries glass paint layers consist of a colour body and a colourless lead silicate flux, in which borax or boric acid was added as further component to improve the paint ability and to reduce the firing temperature for multiple layers of paint. Model glasses were used in laboratory tests to investigate the stability of glass paints with additions of boron oxide. To determine boron in paint layers, a LIBS-system with pulsed NdYAG-laser was used.
The church of Koszewko (Poland) is a brick building edified in the 15th century built on cobblestone foundations. There are five windows in the sanctuary. Three of them enclose heraldic panels from the Küssow’s family from the 15th century which are surrounded with Goethe glass from the 18th century to complete the windows. The colored heraldic panels are strongly damaged and corroded with massive paint layer losses, glass- and leadbreakages. Those medieval glass fragments have been shortly discovered and are of particular interest for Poland since only few medieval glazing have been conserved.
The damages as well as the glass compositions have been investigated with ESEM/EDX. Two categories of medieval glass compositions have been identified. The blue glass is particularly sensible to corrosion because of his high content in K2O. The colorless and the red glass samples belong to a stable glass type. Due to the thickness of the gel layer, it is easy to see that the degradation is strongly proceeded. The protection of those medieval stained-glass panels is absolute necessary.
The medieval panels have been restored and surrounded from a copper frame. Then they have been fixed on the wood frame in the church. The exterior glazing has been closed with a panel of Goethe glass. The gap between the Goethe- and the medieval glass is about 3 cm. The Goethe glass panel has been stabilized with a film based on polyester to protect the medieval glasses against any damages. In this way, a low cost protective glazing has been installed for a long-term conservation of each medieval stained-glass panels. The climate measurements over the period of one year on the restored windows are in process. The temperature and the relative humidity are recorded in the church interior, in the gap between the original and the Goethe glass and outdoors.
Coating materials are nowadays often required to deliver not only sufficient barrier performance and suited optical appearance but a broad range of other functional properties. The incorporation of inorganic nanoparticles (NPs) is known to improve many key characteristics and provide new functionalities in polymer materials. Presented work aims to prepare and characterize an organic-inorganic coating material designed to bring together advantageous properties of hybrid materials and reinforcement effect delivered from the inorganic NPs embedment.
Siloxane-based hybrid resins hold great advantages as coating materials as their properties can be tuned between those of polymers and those of glasses, thus, the compositions with superior thermal and mechanical properties can be achieved. We used Cycloaliphatic Epoxy Oligosiloxane (CEOS) resin as a polymeric matrix where the network formation was achieved by UV induced cationic polymerisation. Boehmite Alumina (BA) nanoparticles were added to CEOS resin as a reinforcing agent and resultant material was processed into films either by bar-coating or by spin-coating depending on further characterization procedure. Two different types of BA NPs, hydrophilic and organophilic, were used in order to assess the impact of particles surface on the resin characteristics. CEOS synthesis by condensation reaction was confirmed using 13C and 29Si NMR. Changes in CEOS photocuring process, resulting from particles incorporation, were monitored by real-time IR spectroscopy. At the same time, the thermal behaviour was evaluated by DSC and TGA methods. Morphology of the coatings was investigated by means of SEM operated in transmission mode.
It was observed that BA presence increased the epoxy conversion degree and glass transition temperature. Material formulations providing best film characteristics were determined with regard to the particle type and loading. Compared to the hydrophilic nanoparticles, organophilic BA NPs yield superior overall performance of the foils.
In this work, the structural integrity of LBM fabricated IN625 small cylinders (d = 1 mm, h = 6 mm) was investigated regarding the porosity and the surface roughness by means of computed tomography. The measurements were carried out on a GE v|tome|x L 300/180 with a reconstructed voxel size of 2 µm. The pores were analyzed for size, shape and spatial distribution. The correlation between compactness C and spatial distribution showed that elongated pores (C < 0.2) appear exclusively within a distance of 80 µm to the sample surface. The reconstructed surface was digitally meshed and unwrapped to evaluate the mean roughness Ra. Since the gravity correlates linearly with the sine of the build angle, the influence of gravity on porosity and surface roughness was determined.
TIG welding process was monitored using LIBS for the in situ measurement of chemical compositions in austenitic stainless steels. This research aims to prototype a real-time chemical composition analysis system for welding applications and prove the feasibility of such a quality control loop.
The chemical compositions of the weld pool, considering the welding metallurgy, is the most critical parameter for any occurring weld defects, e.g. hot cracking. Hence, controlling the weld pool chemical composition allows governing of the weld pool solidification behavior by monitoring and adjusting the respective welding parameters, e.g. welding current.
LIBS measurements were conducted during a TIG-welding process. The effect of the welding plasma on the LIBS signal was thoroughly investigated by varying various LIBS settings, e.g. delay and exposure time. Quantification of the main alloying elements Cr and Ni in the weld pool during welding was achieved by univariate calibration procedure.