Analytische Chemie
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Organisationseinheit der BAM
- 8 Zerstörungsfreie Prüfung (23)
- 8.1 Sensorik, mess- und prüftechnische Verfahren (23)
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- 1.9 Chemische und optische Sensorik (4)
- 8.2 Zerstörungsfreie Prüfmethoden für das Bauwesen (2)
- 6 Materialchemie (1)
- 6.7 Materialsynthese und Design (1)
- 8.0 Abteilungsleitung und andere (1)
- 8.6 Faseroptische Sensorik (1)
- VP Vizepräsident (1)
A new concept for the self-diagnosis of embedded fiber Bragg grating (FBG) strain sensors was developed, simulated and experimentally tested. This concept is based on a magnetostrictive metallic layer directly coated on the fibre cladding over the grating segment of the FBG sensor, so that an on-demand external magnetic field in a millitesla scale can produce a controllable artificial strain as an indication signal for the remote optical interrogator. The relationship between the pre-defined magnetic field and its induced Bragg wavelength shift characterizes this validation concept. Any deviation of the local bonding state of the interfaces from the initial or/and any change of shear strain transferring mechanism from composite matrix to the optical fibre core will result in alterations in this sensitive relationship, and thus triggers an immediate alert for a further inspection. The finite element method is used to simulate the strain of this configuration as result of different values of the magnetic field in order to optimize the geometrical sensor parameters. The simulations are verified by experiments results. © (2016) COPYRIGHT Society of Photo-Optical Instrumentation Engineers (SPIE). Downloading of the abstract is permitted for personal use only.
Damages in infrastructure due to moisture amount to billions of Euros every year. For a more predictive structural health monitoring in civil engineering, the detection and monitoring of hazardous moisture in steel reinforced concrete constructions is of high interest. The sensors have to be wireless, elsewise they weaken the concrete cover of the rebars. The lifetime of such constructions is normally decades, thus the sensors have to be battery-free and fully passive. Considering these requirements, passive RFID-based sensors are developed. Communication and energy supply are realized wireless via the electromagnetic field of a RFID transmitter. The passive RFIDbased sensors are embedded into the concrete to enable the monitoring of moisture transport in porous materials. Results of the hydration process are shown.
Embedded wireless sensor systems for long-term SHM and corrosion detection in concrete components
(2017)
State-of-the-art communication standards like RFID and Bluetooth Low Energy enable the development of sensor systems which can be completely embedded into concrete components for long-term SHM and early damage detection. Objective of the project KonSens which is carried out at BAM is the development, implementation, and validation of sensors for measuring of Parameters relevant for corrosion, like moisture, pH value, and electrical conductivity, inside steel reinforced concrete components. The primarily addressed application is detection and evaluation of corrosion processes in concrete bridges.
In contrast to cable connected sensors, embedded wireless sensors avoid any pathways for intrusion of moisture and chemicals, e.g., chlorides which could trigger corrosion activity. To allow for long-term, ideally life-time operation, the once embedded sensor systems must work highly energy efficient. One option are passive RFID sensor systems, which work without battery. The energy is transmitted to the system through the electromagnetic field, even to operate sensors. A crucial parameter is the transmission depth in concrete. First experiments with RFID sensors working at frequencies of 13.56 MHz (HF) and 868 MHz (UHF) embedded in concrete specimen resulted positive for transmission depths of up to 13 cm, which is quite promising, considering that corrosion would appear first at the top level of rebars.
A second generation of passive RFID sensor systems has been implemented with improved antenna design. Current experiments using these systems focus on the Transmission characteristics in terms of transmission depths and the impact of concrete moisture. Low-energy humidity sensors are used and analysed regarding their capability for measuring the material moisture. Additionally, a relation between transmitted power to the embedded sensor and the moisture content of the concrete specimen caused by energy absorption can be presumed and is under systematic investigation.
Because ammonia and its reaction products can cause considerable damage to human health and ecosystems, there is a need for reliably operating and reversibly interacting sensor materials to monitor traces of gaseous ammonia in ambient air, which at best can be used on-site for in-the-field measurements. Herein, the development of a sensor material for gaseous ammonia in the lower ppm to ppb range using optical fluorescence as transduction mechanism is presented. A fluorescent dye, which shows reversible fluorescence enhancement in the presence of ammonia is incorporated into a polymer matrix, the latter to ensure the accumulation of ammonia. The sensor material is integrated into a prototype of a miniaturized sensor device, facilitating long-term operation. To calibrate the optical sensor system a gas standard generator, producing standard gas mixtures, is used, leading to a sensitivity down to lower ppm concentrations of ammonia.
This paper deals with the development and investi-gation of a volatile organic compound (VOC) system for differ-ent scenarios. The integrated multi-sensor unit can detect dif-ferent gases through the integrated 3-fold VOC sensor, where-by a continuous measurement takes place. The system-integrated flow control, with pump and flow sensor, allows the gas molecules to be transported directly to the VOC sensor. The entire measurement is permanently stored on an integrat-ed Secure Digital (SD) card. If the previously determined limit range is exceeded, an alarm is generated. Due to the combina-tion of different components, numerous applications are possi-ble. The system is the first step or a tool towards further devel-opments in the field of gas sensors and is primarily used for the validation of chemically based gas sensors, and it is still largely extended by application-specific influences.
Piezoresistive accelerometers use a strain-sensing element, generally made of semiconductor material, e.g., silicon to convert the mechanical motion into an electrical signal. This element is usually designed in form of a cantilever beam loaded with a mass. Acceleration causes bending of the beam, which produces a change of electrical resistance proportional to the applied acceleration.
Main advantages of piezoresistive accelerometers in comparison to other types, e.g., piezoelectric and capacitive, is their robust and highly dynamic behavior, which qualifies them for application in high impact shock applications. Mechanical damping is typically implemented with silicon oil in a way that the output signal is undistorted over a wide frequency range. These characteristics principally qualify them for the application in drop tests carried out at BAM, for which they are calibrated over the frequency range from 1 to 4 kHz. However, using silicon oil for damping, has the drawback of temperature dependent change of its viscosity, leading to temperature dependent deviation of the accelerometer’s sensitivity.
This study presents experimental results of the temperature behavior of a piezoresistive accelerometer with a dynamic range up to ±5000 g.
This type of accelerometer is applied for drop tests which are partially performed at temperatures of -40 or +100 °C.
In Glasfasern eingeschriebene Bragg-Gitter (FBG: fibre-based Bragg gratings) sind über die Verschiebung der Bragg-Wellenlänge in der Lage, Stauchungen und Dehnungen von Glasfasern hochgenau zu erfassen. In Kompositwerkstoffe eingebettete faseroptische Sensoren können Bauteile bezüglich ihrer mechanischen Integrität überwachen und früh-zeitig Informationen über Materialveränderungen gewinnen.
Um die Zuverlässigkeit eines solchen Sensors zu gewährleisten, ist es wichtig, die korrekte Funktion des Sensors im Verbund mit der Werkstoff-Matrix on-line und in-situ sicherzu-stellen. Im Rahmen des DFG-Projekts FAMOS² (FAser-basierter Magneto-Optischer SchichtSensor) wurde ein selbstdiagnosefähiger Schichtsensor entwickelt, der mit Hilfe von magnetostriktiven Aktorschichten aus Nickel bzw. Eisen-Nickel validiert werden kann.
Der FAMOS²-Schichtsensor wird durch ein PVD (physical vapour deposition)/ECD (electro-chemical deposition) Hybridschichtsystem realisiert, das auf dem Fasermantel im Bereich des FBG haftfest, homogen und langzeitfunktional abzuscheiden ist. Dabei wird in einem ersten Schritt ein etwa 100 Nanometer dünnes PVD-Schichtsystem aus Chrom und Kupfer als Haftvermittler auf der Glasfaser bzw. als leitfähige Startschicht für den nachfolgenden ECD-Prozess abgeschieden. Um eine rotationssymmetrische Schich-tabscheidung zu gewährleisten, erfolgt während der PVD-Beschichtung eine Rotation der Glasfasern. In einem zweiten Schritt wird dann unter Verwendung eines klassischen Watts-Elektrolyten in einer speziell entwickelten ebenfalls rotationssymmetrisch aufgebau-ten ECD-Durchströmungszelle dann die etwa 30 Mikrometer dicke, magnetostriktive Ak-torschicht auf dem PVD-Schichtsystem abgeschieden, im Vergleich sowohl reine Nickel-Schichten als auch Nickel-Eisen-Schichten.
Ein äußeres Magnetfeld dehnt die magnetostriktive Aktorschicht und damit auch die Faser reversibel. Diese Dehnung führt zu einer Verschiebung der Bragg-Wellenlänge, welche direkt mit der Stärke eines zu messenden oder zu Validierungszwecken vorgegebenen Magnetfeldes korreliert. Die Anpassung der Beschichtungsverfahren an die Fasergeome-trie und die mechanischen Eigenschaften der Hybridschichten werden hinsichtlich der me-chanischen Integrität des faseroptischen Sensors diskutiert und der Nachweis der Selbst-diagnosefähigkeit erbracht.
Es wird ein vereinfachtes Verfahren für die Bestimmung und Implementierung der Maschinennachgiebigkeit bei der Verwendung eines sphärischen Indenters dargestellt. Die Maschinennachgiebigkeit wird bei deutlicher Kraftabhängigkeit als Funktion der Kraft in die Auswertung implementiert. Als sensitiver Kennwert dient der aus der instrumentierten Eindringprüfung an Härtevergleichsplatten ermittelte Eindringmodul.
Temperature characteristics of a piezoresistive accelerometer for high impact shock application
(2018)
This study presents the characterization of a piezoresistive accelerometer damped with silicon oil for the application in drop tests carried out at BAM. Experiments were performed with the Hopkinson Bar method in close correlation to the real-world application conditions. The results point out certain limitations regarding the temperature influence and the frequency response. Additional experiments were performed with a gas damped type of piezoresistive accelerometer, which has superior specifications, particularly for low temperatures. The results allow for a comparison.
This paper describes a wireless mobile prototype able to perform optical measurements by means of a miniatur-ized spectrometer for low light analysis, e.g. fluorescent sensors. Evaluations, calculations, calibration management and result display are performed by a computer or a standard tablet. The device was designed primarily to detect traces of oil in drinking or ground water and for the analyses of crude oils. However, it can also address a wide range of fluorescent sensors. The fast and user-friendly inspection of water quality or oil properties, as well as the adaptability and mobility, make the device attractive for a variety of users. Further application areas could be easily imple-mented by adapting the optics and the software (database, data processing and calibration plots, etc.)