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- desorption control (1)
- dimensional metrology (1)
- discharge (1)
- eAttestation (1)
- eddy current (1)
- elastomeric polymer optical fiber POF (1)
- electrocatalysis (1)
- electron backscatter diffraction (1)
- energy gases (1)
- enriched isotope (1)
- estrogenic activity (1)
- excitation power density (1)
- extension (1)
- extraction (1)
- fluorescence standards (1)
- functional PVD coatings (1)
- glow (1)
- granulation (1)
- graphene related 2D materials (1)
- graphical models (1)
- guided waves (1)
- high voltage cable accessories (1)
- historic inks (1)
- i-TRIBOMAT (1)
- imaging (1)
- immunoaffinity (1)
- in-situ (1)
- infrared spectroscopy (1)
- ink (1)
- inspection (1)
- instrument utilization (1)
- interferences (1)
- ion source (1)
- isotope ratio (1)
- key comparison (1)
- komplexe Angriffe (1)
- laboratory automation (1)
- laboratory management (1)
- laser induced plasma (1)
- laser induziertes Plasma (1)
- laser-induced plasma (1)
- laser-spark (1)
- leaching (1)
- low energy electrons (1)
- magnetic beads (1)
- mechanical properties (1)
- mechanochemistry (1)
- mercury intrusion capillary pressure (1)
- mesoporous material (1)
- metadata collection (1)
- metal (1)
- metal phosphonates (1)
- microfluidics (1)
- micromechanical modeling (1)
- microplastics, sampling, sampling techniques, water (1)
- microstructure (1)
- microwave (1)
- milling (1)
- module (1)
- mof (1)
- moisture (1)
- monitoring (1)
- nPSize (1)
- nanoindentation (1)
- nanomaterial (1)
- nanostructured (1)
- nerve agent (1)
- nichtrostender Stahl (1)
- non-destructive testing (NDT) (1)
- nuclear magnetic (1)
- numerical uncertainty determination (1)
- numerische Messunsicherheitsbestimmung (1)
- nutritional supplements (1)
- ochratoxin A (1)
- openBIS (1)
- optical (1)
- pH Wert in Baustoffen (1)
- pH-Monitoring (1)
- pH-Sensor (1)
- pXRF (1)
- papyrus (1)
- partial discharge (1)
- particle injection (1)
- performance test (1)
- photothermisch (1)
- plasma dispersion layers (1)
- plasmonics (1)
- pole figure (1)
- poly(acrylamide-co-acrylonitrile) (1)
- pore radius (1)
- poultry odorous air monitoring (1)
- presentation (1)
- presolvated electron (1)
- pressure vessels (1)
- product specification (1)
- qNMR metrology (1)
- qNMR-Spektroskopie (1)
- quality assurcance (1)
- quality control (1)
- radical scavenger (1)
- reference materials, requirements, guidance (1)
- rekombinante Protein Expression (1)
- relaxation time (1)
- research efficiency (1)
- research landscape (1)
- resonance (1)
- robustness (1)
- rubber (1)
- räumliches Auflösungsvermögen (1)
- sample preparation (1)
- sc-ICP-ToF-MS (1)
- screed (1)
- screen-printed electrodes (1)
- sensor (1)
- serine-protease inhibitor (1)
- shape control (1)
- silicone rubber (1)
- silver nanoparticles (1)
- simulation (1)
- single cell analysis (1)
- single cell-ICP-ToF-MS (1)
- single particle-ICP-ToF-MS (1)
- slurry (1)
- small-angle X-ray scattering (1)
- smart standards (1)
- smartphone (1)
- spectral induced polarization (1)
- spectroscopy (1)
- sporting track (1)
- spray drying (1)
- standardization (1)
- surface group analysis (1)
- synthesis (1)
- t90 value (1)
- t90-Zeit (1)
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- temperature (1)
- thermoresponsive (1)
- total scattering (1)
- traceable standards (1)
- ultra-small-angle X-ray scattering (1)
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- uncertainty (1)
- validation, qualitative methods (1)
- wave propagation (1)
- zerstörungsfreie Ortung (1)
- zerstörungsfreie Prüfung (1)
- zerstörungsfreie Prüfung im Bauwesen (1)
- µCT (1)
- µJ-DPSS laser (1)
- µPAD (1)
- µXRF (1)
- Ägyptisch Blau (1)
- β-cristobalite structure type (1)
- μ-CT imaging (1)
- μ-CT imaging, (1)
Organisationseinheit der BAM
- 8 Zerstörungsfreie Prüfung (1031)
- 1 Analytische Chemie; Referenzmaterialien (939)
- 6 Materialchemie (705)
- 8.2 Zerstörungsfreie Prüfmethoden für das Bauwesen (257)
- 8.0 Abteilungsleitung und andere (255)
- 6.1 Oberflächen- und Dünnschichtanalyse (244)
- 8.4 Akustische und elektromagnetische Verfahren (213)
- 1.4 Prozessanalytik (201)
- 8.1 Sensorik, mess- und prüftechnische Verfahren (195)
- 1.1 Anorganische Spurenanalytik (183)
- 6.3 Strukturanalytik (181)
- 4 Material und Umwelt (180)
- 6.6 Physik und chemische Analytik der Polymere (147)
- 1.2 Biophotonik (141)
- 1.8 Umweltanalytik (135)
- 1.9 Chemische und optische Sensorik (130)
- 8.5 Röntgenbildgebung (130)
- S Qualitätsinfrastruktur (103)
- 6.5 Synthese und Streuverfahren nanostrukturierter Materialien (99)
- 4.5 Kunst- und Kulturgutanalyse (95)
- 7 Bauwerkssicherheit (93)
- S.2 Digitalisierung der Qualitätsinfrastruktur (87)
- 1.6 Anorganische Referenzmaterialien (85)
- 6.7 Materialsynthese und Design (77)
- 1.7 Organische Spuren- und Lebensmittelanalytik (65)
- 1.5 Proteinanalytik (56)
- 8.6 Faseroptische Sensorik (56)
- 5 Werkstofftechnik (54)
- 1.3 Instrumentelle Analytik (44)
- 4.2 Material-Mikrobiom Wechselwirkungen (37)
- 7.6 Korrosion und Korrosionsschutz (34)
- 4.1 Biologische Materialschädigung und Referenzorganismen (28)
- 9 Komponentensicherheit (28)
- VP Vizepräsident (28)
- VP.1 eScience (27)
- 7.4 Baustofftechnologie (26)
- 4.3 Schadstofftransfer und Umwelttechnologien (25)
- P Präsident (23)
- 5.1 Mikrostruktur Design und Degradation (20)
- 6.2 Material- und Oberflächentechnologien (19)
- P.0 Präsident und andere (17)
- 2 Prozess- und Anlagensicherheit (16)
- 7.1 Baustoffe (16)
- 9.0 Abteilungsleitung und andere (15)
- S.1 Qualität im Prüfwesen (14)
- 3 Gefahrgutumschließungen; Energiespeicher (13)
- 6.0 Abteilungsleitung und andere (13)
- 7.5 Technische Eigenschaften von Polymerwerkstoffen (13)
- 2.1 Sicherheit von Energieträgern (12)
- 5.4 Multimateriale Fertigungsprozesse (11)
- 5.3 Polymere Verbundwerkstoffe (9)
- 1.0 Abteilungsleitung und andere (8)
- 4.4 Thermochemische Reststoffbehandlung und Wertstoffrückgewinnung (8)
- 5.0 Abteilungsleitung und andere (7)
- PST Präsidiale Stabsstelle (7)
- 3.5 Sicherheit von Gasspeichern (6)
- 4.0 Abteilungsleitung und andere (6)
- 9.5 Tribologie und Verschleißschutz (6)
- 3.1 Sicherheit von Gefahrgutverpackungen und Batterien (5)
- 5.2 Metallische Hochtemperaturwerkstoffe (5)
- 9.4 Integrität von Schweißverbindungen (5)
- 9.6 Additive Fertigung metallischer Komponenten (5)
- 7.2 Ingenieurbau (4)
- VP.2 Informationstechnik (4)
- 2.5 Konformitätsbewertung Explosivstoffe/Pyrotechnik (3)
- 7.0 Abteilungsleitung und andere (3)
- 9.2 Versuchsanlagen und Prüftechnik (3)
- 2.0 Abteilungsleitung und andere (2)
- 3.6 Elektrochemische Energiematerialien (2)
- 5.6 Glas (2)
- 7.3 Brandingenieurwesen (2)
- S.0 Abteilungsleitung und andere (2)
- 3.0 Abteilungsleitung und andere (1)
- 3.2 Gefahrguttanks und Unfallmechanik (1)
- 5.5 Materialmodellierung (1)
- 9.3 Schweißtechnische Fertigungsverfahren (1)
- MP Mitglied des Präsidiums (1)
- MP.0 Mitglied des Präsidiums und andere (1)
- Z Zentrale Dienstleistungen (1)
- Z.1 Organisation, Controlling (1)
Die Probenpräparation ist ein wichtiger Schritt für die Qualität der Massenspektren in MALDI-TOF MS. Es werden Polymerproben, die lösungsmittelbasiert und lösungsmittelfrei präpariert worden sind, verglichen. Dabei werden die Intensitätsverhältnisse von ternären Mischungen von PEG-, PS- und PMMA-Polymeren beachtet.
Bei der Erhaltung von Stahlbetonbauwerken ist der Chloridgehalt im Beton ein wichtiger Parameter zur Festlegung geeigneter Instandsetzungsmaßnahmen. Die bisher etablierten Verfahren basieren auf der nasschemischen Analyse einer Probe, Bohrmehl oder aufgemahlener Segmente eines Bohrkerns. Das Verfahren liefert einen Chloridgehalt je Tiefensegment, was mit einer starken Homogenisierung der Probe einhergeht, wodurch detaillierte Informationen zu Chloridunterschieden im Millimeterbereich verloren gehen. Eine alternative Methode ist die laserinduzierte Plasmaspektroskopie (LIBS), die nicht nur die quantitative ortsaufgelöste Bestimmung des Chloridgehalts im Bezug zur Zementmasse ermöglicht, sondern auch simultan detaillierte Informationen über die Verteilung vieler anderer chemischer Elemente liefert. Die räumliche Auflösung liegt in der Regel im Bereich von einigen Millimetern, kann aber bei Bedarf auf 0,1 mm oder weniger erhöht werden. Das neue Merkblatt B14 „Quantifizierung von Chlorid in Beton mit der laserinduzierten Plasmaspektroskopie (LIBS)“ der Deutschen Gesellschaft für Zerstörungsfreie Prüfungen (DGZfP) regelt und vereinheitlicht erstmals die zuverlässige und reproduzierbare Ermittlung des Chloridgehalts mit LIBS. In diesem Beitrag wird das Merkblatt vorgestellt und anhand praktischer Anwendungsbeispiele das Potenzial von LIBS für Fragestellungen in der Betonerhaltung verdeutlicht.
The use of ashes from municipal solid waste incineration as secondary building materials is an important pillar for the circular economy in Germany. However, leaching of potential toxic elements from these materials must be at environmentally acceptable levels. Normally, a three-month ageing period immobilizes most hazardous heavy metals, but antimony (Sb) and vanadium (V) showed previously unusual leaching. In order to clarify the mechanisms, we analyzed the Sb and V species in various bottom and fly ashes from municipal waste incineration by XANES spectroscopy. Antimony oxidizes from Sb(+ III) species used as flame retardants in plastics to Sb(+ V) compounds during waste incineration. However, owing to the similarity of different Sb(+ V) compound in the Sb K- and L-edge XANES spectra, it was not possible to accurately identify an exact Sb(+ V) species. Moreover, V is mainly present as oxidation state + V compound in the analyzed ashes. However, the coarse and magnetic fraction of the bottom ashes contain larger amounts of V(+ III) and V(+ IV) compounds which might enter the waste incineration from vanadium carbide containing steel tools. Thus, Sb and V could be critical potential toxic elements in secondary building materials and long-term monitoring of the release should be taken into account in the future.
Volatile organic compounds (VOCs) emitted by furniture and building materials can cause health issues. For an improvement of indoor air quality low emitting materials should be used. Quality assurance and –control (QA/QC) measures require an emission reference material (ERM) with a predictable emission rate of VOCs. The idea is to use porous materials as ERM, which store the VOCs inside their pores and emit them constantly.
Volatile organic compounds (VOCs) emitted by furniture and
building materials can cause health issues. For an
improvement of indoor air quality low emitting materials
should be used. Quality assurance and –control (QA/QC)
measures require an emission reference material (ERM) with a
predictable emission rate of VOCs. The idea is to use porous
materials as ERM, which store the VOCs inside their pores and
emit them constantly.
Isotope analysis plays a critical role in various disciplines, including environmental science, archaeology, and forensic investigations. Traditional methods such as mass spectrometry provide precise isotopic data but often require complex, costly setups and extensive sample preparation. As an alternative, optical spectrometry has emerged as a versatile and less invasive technique. This presentation explores the advancements and applications of optical spectrometry methods in isotope analysis, emphasizing their benefits and challenges.
Lithium (Li), Boron (B), Nitrogen (N), Magnesium (Mg), and Calcium (Ca) are pivotal elements across various spheres such as the hydrosphere, biosphere, and lithosphere, significantly impacting (bio-) geochemical and physiological processes. These elements exhibit stable isotopes with substantial roles in geological, environmental, and biological studies. The traditional method for measuring isotope amount ratios has been through mass spectrometry, which, despite its accuracy, comes with high operational costs, the need for skilled operators, and time-consuming sample preparation processes.
Combining optical spectroscopy with chemometrics introduces an innovative, cost-effective approach by the hand of high-resolution continuum source atomic and molecular absorption spectrometry (HR-CS-AAS and HR-CS-MAS) for the analysis of isotope ratios in Li, B, N, Mg, and Ca. By analyzing the atomic or molecular absorption spectrum of the in-situ generated cloud of atoms of diatomic molecules (e.g., Li, BH, NO, MgF, CaF) during the electronic transition from the fundamental state, this method allows for the rapid determination of isotope ratios directly from sample solutions without the need for complex sample preparation.
For each element, the respective atomic or molecule's absorption spectrum was deconvoluted into its isotopic components using partial least squares regression or machine learning algorithms. Robust calibration models were developed, calibrated with enriched isotope, and validated against certified reference materials. Spectral data underwent preprocessing to optimize the modeling to determine the optimal number of latent variables.
The findings showcase that this optical spectrometric method yields results that agree with those obtained via inductively coupled plasma mass spectrometry (ICP-MS), offering a promising, cost-effective, and rapid alternative for isotope analysis with precisions as low as ± 0.2‰. This approach is a significant advancement in analytical chemistry, providing a new way to study isotope variations in biological, environmental, and geological samples.
What does GD-OES reveal about the aging and manufacturing processes of lithium-ion batteries?
(2024)
Glow-Discharge Optical Emission Spectroscopy (GD-OES), a powerful analytical technique, sheds light on the two critical aspects of lithium-ion batteries (LIBs): manufacturing and aging 1, 2. We optimized cell production in manufacturing by adjusting parameters, including cathode doping, electrolyte concentration, and pressing force. GD-OES provided in-depth elemental composition and homogeneity analysis, which is crucial for identifying optimal manufacturing conditions. These findings were validated by electrochemical impedance spectroscopy, confirming the quality of the manufactured batteries.
Shifting the focus to aging, we use GD-OES for fluorine depth profiling, a key element in understanding polymer and electrolyte degradation. However, fluorine presents analytical challenges. We addressed this by substituting argon with a neon:argon mixture, which significantly enhanced fluorine detection sensitivity. This advancement not only improves accuracy but also holds the potential to guide sustainable and cost-efficient manufacturing strategies.
Through its versatility, GD-OES has proven to be a powerful tool for not only optimizing LIB manufacturing processes but also gaining deeper insights into their aging mechanisms. This research extends beyond academic interest, offering tangible benefits for the industry by translating into improved battery quality, extended lifespan, and overall performance.
Im Rahmen der von der BAM und anderen Partnern ins Leben gerufenen Initiative „Digitale Qualitätsinfrastruktur“ liegt der Fokus u.a. auf der Entwicklung von neuen Zertifizierungsworkflows. Dabei ist eine besondere Bedeutung dem Zusammenführen von Operational Technology (OT) und Informationstechnik (IT) beizumessen. Zur Datenintegration aus der Sensor-Feldebene einer Versuchs-wasserstofftankstelle wurde eine solche Infrastruktur zunächst in einer Laborumgebung aufgebaut.
Faecal contaminants in water are considered serious threats for human health, due to the presence of viruses, bacteria and other harmful microorganisms.1 Urobilin (UB) is a well-known faecal pigment and can be used as a marker for faecal matter in water.2 UB is commonly present in the urine of all mammals as the catabolic end product of bilirubin degradation.2 As the only simple chemical approach to its detection, Schlesinger’s test is usually used to enhance the weak fluorescence of UB in alcoholic media by complexation with Zinc.2, 3 The major limitation of this method is the only weak enhancement of the intrinsically weak UB fluorescence in aqueous media.3 This work presents an approach to introduce different Zn salts for improved fluorescence response, where we found a clear dependence of the fluorescence yield of UB-Zn(II) complexes on the counterion of the salt in water. By employing a combination of fluorescence parameters like transition energy, fluorescence intensity, and fluorescence lifetime, a photophysical understanding of the structure and conformation of the UB-Zn(II) complexes responsible for the fluorescence enhancement in water could be gained. The possibilities of developing a sensitive analytical method based on the acquired understanding are also discussed.