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Multi-sensory monitoring and ultrasound for quality assurance at underground sealing structures
(2023)
Within the safety concepts of underground disposal sites of nuclear waste, engineered barriers play an important role. As these sealing structures have high demands concerning integrity, we aim at advancing the available construction materials, monitoring, and inspection techniques within the project SealWasteSafe. A specifically developed alkali-activated material is compared to classical salt concrete. A comprehensive multi-sensory monitoring scheme is used at 150-340 l specimens to monitor setting and hardening of both materials. All sensors are demonstrated to resist the highly alkaline environments. Besides cabled and wireless temperature and humidity of the materials, strain variations using fibre optic sensors and acoustic emissions are recorded over periods of at least 28 days, partly for more than eight months. After hardening of the specimens, further nondestructive evaluations using ultrasonic echo and thermographic measurements are conducted.
Preliminary results proof the suitability of the tested sensors and clearly highlight differences between the tested materials. Particularly, the newly developed alkali-activated material shows lower acoustic emission activity indicating less cracking activity. Additionally, unique ultrasonic methods will enable better images of potential internal objects and cracks at in-situ sealing structures. A largescale ultrasonic system is optimised to reliably detect objects at a depth exceeding 9 m while still obtaining a good resolution. Modelling studies show the potential of further increasing the distance between individual transducer arrays. Additionally, a new ultrasonic borehole probe using phased arrays allowing for beam focussing is constructed and tested. Laboratory measurements at a halfcylindrical concrete specimen coincide well with the previous modelling. In total, the presented safe materials, detailed monitoring approaches and ultrasonic quality assurance methods will help to obtain safe sealing structures within salt as a host rock. The concepts can partly be transferred to sealing structures in alternative host rocks and will also be valuable for non-nuclear waste repositories.
Chemical and pharmaceutical companies have to find new paths to survive successfully in a changing environment, while also finding more flexible ways of product and process development to bring their products to market more quickly – especially high-quality high-end products like fine chemicals or pharmaceuticals. A current approach uses flexible and modular chemical production units, which can produce different high-quality products using multi-purpose equipment with short downtimes between campaigns and reduce the time to market of new products.
NMR spectroscopy appeared as excellent online analytical tool and allowed a modular data analysis approach, which even served as reliable reference method for further Process Analytical Technology (PAT) applications. Using the available datasets, a second data analysis approach based on artificial neural networks (ANN) was evaluated. Therefore, amount of data was augmented to be sufficient for training. The results show comparable performance, while improving the calculation time tremendously. In future, such fully integrated and interconnecting “smart” systems and processes can increase the efficiency of the production of specialty chemicals and pharmaceuticals.
Chemical and pharmaceutical companies need to find new ways to survive successfully in a changing environment, while finding more flexible ways of product and process development to bring their products to market faster - especially high-value, high-end products such as fine chemicals or pharmaceuticals. This is complicated by changes in value chains along a potential circular economy.
One current approach is flexible and modular chemical production units that use multi-purpose equipment to produce various high-value products with short downtimes between campaigns and can shorten time-to-market for new products. Online NMR spectroscopy will play an important role for plant automation and quality control, as the method brings very high linearity, matrix independence and thus works almost calibration-free. Moreover, these properties ideally enable automated and machine-aided data analysis for the above-mentioned applications.
Using examples, this presentation will outline a possible more holistic approach to digitalization and the use of machine-based processes in the production of specialty chemicals and pharmaceuticals through the introduction of integrated and networked systems and processes.