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- Industry 4.0 (13)
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- Offshore wind energy (11)
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- High Entropy Alloy (10)
- High-entropy alloy (10)
- Hydrogen Embrittlement (10)
- ILC (10)
- In-situ monitoring (10)
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- Ionizing radiation (10)
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- Isotope analysis (10)
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- Nano aerial robot (10)
- Nanocrystal (10)
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- Sensorik (10)
- Single cell analysis (10)
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- Specialised information system (10)
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- Stainless steels (10)
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- Dangerous Goods Quickinfo (9)
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- In situ monitoring (9)
- Indirect hard modeling (9)
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- Scaled Boundary Finite Element Method (9)
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- additive manufacturing (9)
- Air-coupled ultrasound (8)
- Ammoniumnitrat (8)
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- BDS (8)
- Base damage (8)
- Base loss (8)
- Baustoffe (8)
- Bauteilprüfung (8)
- Bauwerksüberwachung (8)
- Benchtop NMR (8)
- Bridges (8)
- C-F bond activation (8)
- Chemically Complex Materials (8)
- Composite pressure vessel (8)
- Composite pressure vessels (8)
- Composite-Druckgefäße (8)
- Core-shell particles (8)
- Cultural heritage (8)
- DNA radiation damage (8)
- Damage detection (8)
- Dark-field transmission electron microscopy (DFTEM) (8)
- Data Analysis (8)
- Deactivation pathways (8)
- Defects (8)
- Dielectric spectroscopy (8)
- Digital Image Correlation (8)
- Digitization (8)
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- Duplex (8)
- Electron backscatter diffraction (8)
- Emission spectroscopy (8)
- Environmental monitoring (8)
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- Graphite furnace (8)
- HAXPES (8)
- Heat control (8)
- Heterogeneity (8)
- Hot cracking (8)
- Hybrid laser arc welding (8)
- In-situ (8)
- Isotope dilution (8)
- Isotopic shift (8)
- Korundschleifen (8)
- LPG (8)
- LTCC (8)
- Laser implantation (8)
- Laser-induced periodic surface structures, LIPSS (8)
- Layer formation (8)
- Life sciences (8)
- Low Cycle Fatigue (8)
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- Maintenance (8)
- Material Science (8)
- Materials Informatics (8)
- Metabolism (8)
- Microscopy (8)
- Mikrolegierungseinfluss (8)
- Mikrostruktur (8)
- Modular Production (8)
- Monte-Carlo simulation (8)
- NMR-Spektroskopie (8)
- NbC (8)
- Near ambient pressure xray photo electron spectroscopy (8)
- Nondestructive Testing (8)
- Online (8)
- Orientation (8)
- Oxygen evolution reaction (8)
- PS (8)
- Particle size (8)
- Persistence (8)
- Phased Array (8)
- Phased array (8)
- Phosphates (8)
- Pigment (8)
- Polymorphism (8)
- Prehydrated electron (8)
- Prozess-Sensoren 4.0 (8)
- Prüfmethoden (8)
- Pyrolysis (8)
- QI-Digital (8)
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- RFID sensors (8)
- Radiotherapy (8)
- Reduced volume method (8)
- Regulations (8)
- Reverse glass painting (8)
- Ringversuche (8)
- SEM/EDX (8)
- Scanning electron microscopy (8)
- Silica (8)
- Single-stranded DNA-binding proteins (8)
- Stahl (8)
- Strahlenschutz (8)
- Thermal Runaway (8)
- Verwertung (8)
- Wirbelstrom (8)
- X-ray fluorescence (8)
- XANES spectroscopy (8)
- Xray photo electron spectrocopy (8)
- Zinkdeckschichten (8)
- AES (7)
- ASR (7)
- Absolute fluorescence quantum yield (7)
- Abwasser (7)
- Admixtures (7)
- Alloy modification (7)
- Archäometrie (7)
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- Atomic Force Microscopy (AFM) (7)
- Austenitic stainless steel (7)
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- BBodSchV (7)
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- Betonstahl (7)
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- Black fungi (7)
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- Building Materials (7)
- CALPHAD (7)
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- Calcium cobaltite (7)
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- Carbon steel (7)
- Carbonation (7)
- Centrifugal Adhesion Testing (CAT) (7)
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- Distributed fiber optic sensing (7)
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- Faserverbundwerkstoffe (7)
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- Inconel 718 (7)
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- Interlaboratory Comparison (7)
- Ionic Liquid crystals (7)
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- Kriechen (7)
- Kunststoffdichtungsbahnen (7)
- Kupfer (7)
- Laser Thermography (7)
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- Organic peroxide (7)
- Ortsbewegliche Druckgeräte (7)
- P92 (7)
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- Quantitative NMR spectroscopy (7)
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- REM (7)
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- Smarte Sensoren (7)
- Smouldering (7)
- Specialised Information System (7)
- Structural integrity (7)
- Submerged arc welding (7)
- Surface group analysis (7)
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- TF Material (7)
- TMDSC (7)
- TPED (7)
- Thermisches Durchgehen (7)
- Thermoresponsive polymer (7)
- Titanium dioxide (7)
- Tolerance (7)
- Topas (7)
- Tribologie (7)
- Ultrakurze Laserpulse (7)
- Umweltgefährdend (7)
- Variational Bayesian (7)
- Vessels (7)
- Volatile organic compounds (7)
- WAXS (7)
- Warfarin (7)
- Weld pool shape (7)
- Zündquellen (7)
- 1d laser (6)
- 2. SprengV (6)
- 3D (6)
- AI (6)
- AISI 316L (6)
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- Adsorbed Layer (6)
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- Alumina (6)
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- Analytical method (6)
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- Crack propagation (6)
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- DTBP (6)
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- Formaldehyd (6)
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- Materialcharakterisierung (6)
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- Passivschicht (6)
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- i-TRIBOMAT (6)
- Acetylen (5)
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Organisationseinheit der BAM
- 8 Zerstörungsfreie Prüfung (1270)
- 6 Materialchemie (1199)
- 1 Analytische Chemie; Referenzmaterialien (955)
- 7 Bauwerkssicherheit (927)
- 9 Komponentensicherheit (834)
- 5 Werkstofftechnik (593)
- 4 Material und Umwelt (587)
- 3 Gefahrgutumschließungen; Energiespeicher (532)
- 9.4 Integrität von Schweißverbindungen (386)
- 7.6 Korrosion und Korrosionsschutz (373)
Häufig ist es wünschenswert, für neue Materialien oder Anwendungen künstliche Bewitterungsverfahren zu benutzen, die auf die spezifischen Anforderungen besser zugeschnitten sind, als es bei bestehenden standardisierten Verfahren der Fall ist. Nachdem man die spezifischen Parameter der Beanspruchung unter Anwendungsbedingungen und die spezifische Empfindlichkeit des Materials erfasst hat, beginnt ein Prozess, der als „Test Tailoring“ häufig abstrakt verwendet, auf den aber nur selten näher eingegangen wird. Genau dieser Prozess soll hier am Beispiel der Entwicklung eines künstlichen Bewitterungstests unter saurer Beaufschlagung, dem in der BAM entwickelten Acid Dew and Fog Test, beispielhaft erläutert werden.
Um den wachsenden Anforderungen an den stofflichen und konstruktiven Leichtbau sowie den Forderungen nach Ressourceneffizienz Rechnung zu tragen, werden in vielen Industriebranchen zunehmend höherfeste Feinkornbaustähle mit Streckgrenzen über 690 MPa eingesetzt. Allerdings werden mit zunehmender Festigkeit deutlich höhere Anforderungen an deren schweißtechnische Verarbeitung gestellt, da die Sensibilität gegenüber einer Herabsetzung der mechanischen Eigenschaften durch den beim Schweißen aufgenommenen diffusiblen Wasserstoff mit steigender Festigkeit zunehmen kann. In den vergleichenden Untersuchungen von konventionellem Übergangslichtbogen und modifiziertem Sprühlichtbogen bei reduziertem Nahtöffnungswinkel konnte gezeigt werden, dass die Schweißprozessparameter die in das Schweißgut eingebrachte Wasserstoffkonzentration beeinflussen. Grundsätzlich ist den erarbeiteten Ergebnissen zu entnehmen, dass im Schweißgut von Stumpfstoßverbindungen mit reduziertem Nahtöffnungswinkel erhöhte mittlere Wasserstoffkonzentrationen vorliegen. Diese können mit geeigneten Wärmeführungen signifikant reduziert werden. Dabei erwies sich eine Nachwärmprozedur aus der Schweißwärme heraus als zielführend. Zudem konnte der Effekt der Nachwärmprozedur anhand fremdbeanspruchter Kaltrissprüfungen nachgewiesen werden.
Prozess-Sensoren 4.0 vereinfachen ihre Einbindung über Plug and Play, obwohl sie komplexer werden. Sie bieten Selbstdiagnose, Selbstkalibrierung und erleichterte Parametrierung. Über die Konnektivität ermöglichen die Prozess-Sensoren den Austausch ihrer Informationen als Cyber-physische Systeme mit anderen Prozess-Sensoren und im Netzwerk. Der Aufbruch von der aktuellen Automation zum smarten Sensor hat bereits begonnen. Automatisierungstechnik und Informations- und Kommunikationstechnik (IKT) verschmelzen zunehmend. Wenn die Prozessindustrie dieses nicht definiert, tun es andere.
Für die weitere Entwicklung von der Ist‐Situation zu einer Industrie-4.0-Welt in der Prozessindustrie werden mehrere Szenarien diskutiert. Diese reichen vom erleichterten Abruf sensorbezogener Daten über zusätzliche Kommunikationskanäle zwischen Sensor und mobilen Endgeräten über vollständig bidirektionale Kommunikation bis hin zur Einbindung der Cloud und des Internets in virtualisierte Umgebungen.
Um zu einer störungsfreien Kommunikation aller Sensoren untereinander zu kommen, muss mindestens ein einheitliches Protokoll her, das alle Sensoren sprechen und verstehen. Der derzeit greifbarste offengelegte Standard, der moderne Kommunikationsanforderungen erfüllt, ist OPC Unified Architecture (OPC-UA). Viele halten das Sortieren der Kommunikationsstandards für eines der wesentlichen Errungenschaften von Industrie 4.0.
Eine Topologie für smarte Sensoren, das Zusammenwirken mit daten- und modellbasierte Steuerungen bis hin zur Softsensorik sowie weitere Anforderungen an Sensoren sind jedoch heute noch nicht angemessen beschrieben. Wir müssen jetzt schnell die Weichen für eine smarte und sichere Kommunikationsarchitektur stellen, um zu einer störungsfreien Kommunikation aller Sensoren auf Basis eines einheitlichen Protokolls zu kommen, welches alle Sensoren ausgeben und verstehen.
Aktuelle und zukünftige öffentliche Förderung von Industrie 4.0-Projekten sind eine gute Investition. Wegen der hohen Komplexität und Interdisziplinarität gelingt die Umsetzung nur gemeinsam zwischen Anwendern aus der Prozessindustrie, Software- und Geräteherstellern und Forschungsgruppen. Anwender sind gefragt, diese neue Technologie durch eine beschleunigte Validierung und Akzeptanz umzusetzen. Sie erhalten die einzigartige Chance, ihre Prozesse und Anlagen wettbewerbsfähig zu halten. Kooperativ betriebenen F&E-Zentren und gemeinsam anerkannten Applikationslaboren kommt dafür eine hohe Bedeutung zu.
Die „auffälligen großen Streifen“ sind von echten Schwingstreifen nur sehr schwer zu trennen, weil sie parallel zu den Schwingstreifen verlaufen und meistens ebenfalls nicht sehr groß sind. Die im Labor getesteten Proben zeigten, dass diese großen Streifen zusammen mit Verreibungen auftraten und „tire tracks“ („Reifenspuren“) verursachten. Dies wurde durch eine hochauflösende REM-Untersuchung bestätigt, die „tire tracks“ auf den „großen Streifen“ zeigte. Ein weiterer Hinweis ist die Änderung des R-Werts von -1 auf 0,1, was zu einer Bruchfläche ohne große Streifen und „tire tracks“ führt.
Currently research in chemical manufacturing moves towards flexible plug-and-play approaches focusing on modular plants, capable of producing small scales on-demand with short down-times between individual cam-paigns. This approach allows for efficient use of hardware, a faster optimization of the process conditions, and thus, an accelerated introduction of new products to the market. Driven mostly by the search for chemical syntheses under biocompatible conditions, so-called “click” chemistry rapidly became a growing field of research. The re-sulting simple one-pot reactions are so far only scarcely accompanied by an adequate optimization via compara-bly straightforward and robust analysis techniques. Here we report on a fast and reliable calibration-free online high field NMR monitoring approach for technical mixtures. It combines a versatile fluidic system, continuous-flow measurement with a time interval of 20 s per spectrum, and a robust, automated algo-rithm to interpret the ob-tained data. All spectra were acquired using a 500 MHz NMR spectrometer (Varian) with a dual band flow probe having a 1/16 inch polymer tubing working as a flow cell. Single scan 1H spectra were recorded with an acquisition time of 5 s, relaxation delay of 15 s.
Currently research in chemical manufacturing moves towards flexible plug-and-play approaches focusing on modular plants, capable of producing small scales on-demand with short down-times between individual campaigns. This approach allows for efficient use of hardware, a faster optimization of the process conditions, and thus, an accelerated introduction of new products to the market [1]. Driven mostly by the search for chemical syntheses under biocompatible conditions, so-called “click” chemistry rapidly became a growing field of research. The resulting simple one-pot reactions are so far only scarcely accompanied by an adequate optimization via comparably straightforward and robust analysis techniques. Here we report on a fast and reliable calibration-free online high field NMR monitoring approach for technical mixtures. It combines a versatile fluidic system, continuous-flow measurement with a time interval of 20 s per spectrum, and a robust, automated algo-rithm to interpret the obtained data. All spectra were acquired using a 500 MHz NMR spectrometer (Varian) with a dual band flow probe having a 1/16 inch polymer tubing working as a flow cell. Single scan 1H spectra were recorded with an acquisition time of 5 s, relaxation delay of 15 s.
Currently research in chemical manufacturing moves towards flexible plug-and-play approaches focusing on modular plants, capable of producing small scales on-demand with short down-times between individual campaigns. This approach allows for efficient use of hardware, a faster optimization of the process conditions, and thus, an accelerated introduction of new products to the market. Driven mostly by the search for chemical syntheses under biocompatible conditions, so-called “click” chemistry rapidly became a growing field of research. The resulting simple one-pot reactions are so far only scarcely accompanied by an adequate optimization via comparably straightforward and robust analysis techniques. Here we report on a fast and reliable calibration-free online high field NMR monitoring approach for technical mixtures. It combines a versatile fluidic system, continuous-flow measurement with a time interval of 20 s per spectrum, and a robust, automated algorithm to interpret the obtained data. All spectra were acquired using a 500 MHz NMR spectrometer (Varian) with a dual band flow probe having a 1/16 inch polymer tubing working as a flow cell. Single scan 1H spectra were recorded with an acquisition time of 5 s, relaxation delay of 15 s. As a proof-of-concept, the thiol-ene coupling between N-boc cysteine methyl ester and allyl alcohol was conducted in non-deuterated solvents while its time-resolved behaviour was characterised with step tracer experiments
Through the application of spectral modeling the signal area for each reactant can be deconvoluted in the online spectra and thus converted to the respective concentrations or molar ratios. The signals which were suitable for direct integration were used herein for comparison purposes of both methods.