Datei im Netzwerk der BAM verfügbar ("Closed Access")
Filtern
Erscheinungsjahr
- 2014 (9) (entfernen)
Dokumenttyp
- Buchkapitel (9) (entfernen)
Referierte Publikation
- nein (9)
Schlagworte
- Ambient vibration (1)
- CRDS (1)
- Changing excitation (1)
- Damage detection (1)
- Forgery (1)
- Glas (1)
- IMS (1)
- Keramik (1)
- Korrosion (1)
- Korrosionsschutz (1)
The one-phase methods described in Chapter 2 were shown to be able to predict casting to some extent, but could not depict segregation, sedimentation and blockage occurring during flow. On the other hand, the distinct element methods described in Chapter 3 did not take into account the presence of two phases in the system and describes concrete as distinct elements interacting through more or less complex laws. A reliable numerical model of a multiphase material behaviour shall take into account both phases (solid and liquid). From the numerical point of view, concrete flow shall be seen therefore as the free surface flow of a highly-concentrated suspension of rigid grains.
Messtechnik und Sensorik
(2014)
Aufgabe der Messtechnik ist die experimentelle Bestimmung quantitativ erfassbarer Größen in Wissenschaft und Technik. Für die Ingenieurwissenschaften liefert die Mess- und Prüftechnik Unterlagen zur Optimierung der Entwicklung, Konstruktion und Fertigung von Bauteilen und technischen Systemen sowie zur Beurteilung der Eigenschaften, Funktion, Qualität und Zuverlässigkeit technischer Produkte.
In this chapter broadband dielectric spectroscopy (BDS) is employed to polymeric blend systems. In its modern form BDS can cover an extraordinary broad frequency range from 10-4 to 1012 Hz. Therefore, molecular and collective dipolar fluctuations, charge transport, and polarization effects at inner phase boundaries can be investigated in detail including its temperature dependence. In the first part of the chapter, the theoretical basics of dielectric spectroscopy are briefly introduced covering both static and dynamic aspects. This section is followed by short description of the various experimental techniques to cover this broad frequency range. To provide the knowledge to understand the dielectric behavior of polymeric blend systems, the dielectric features of amorphous homopolymers are discussed in some detail. This concerns an introduction of the most important relaxation processes observed for these polymers (localized fluctuations, segmental dynamics related to the dynamic glass transition, chain relaxation), a brief introduction to the conductivity of disordered systems as well as polarization effects at phase boundaries. Theoretical models for each process are shortly discussed. In the last paragraph the dielectric behavior of polymer blends is reviewed where special attention is paid to binary systems for the sake of simplicity. In detail the dielectric behavior of binary miscible blends is described. The two most important experimental facts like the broadening of the dielectric relaxation spectra and the dynamic heterogeneity of the segmental dynamics are addressed in depth. Appropriate theoretical approaches like the temperature-driven concentration fluctuation model and the self-concentration idea are introduced.
New developments in spectroscopic techniques for process control are, in general, driven by shortcomings of existing technology, for example, when sensitivity, selectivity, robustness, and so forth do not meet the demands. The perfect process analytical method would be based on a robust and easy to handle customized technique operating in real time, come without any need for calibration, that is, be an absolute method, have a professional support, and be compliant to increasing regulatory requirements. However, there are at least trends toward such an all-in-one device suitable for every purpose.
Small, low-field NMR systems equipped with permanent magnet technology have been developed and allow for quantitative analysis as on-line instruments in a production environment. Quantitative high-resolution on-line NMR spectroscopy contributes to process understanding in pilot plant and research environments.
Laser spectroscopy is a promising field in process analysis owing to its sensitivity and selectivity. Laser-induced breakdown spectroscopy LIBS is a promising field for direct in situ analysis and remote sensing. Applications of quantum-cascade lasers for process analytical applications are a promising technique. Techniques such as cavity ring-down spectroscopy (CRDS), tunable diode laser absorption spectroscopy (TDLAS), and photothermal techniques are briefly introduced.
Recent developments of new detectors have improved X-ray fluorescence analysis (XRF) for qualitative and quantitative on-line evaluation of the elementary composition of liquid or solid samples, regardless of whether compact or bulk material.
The chapter also introduces miscellaneous techniques such as ion mobility spectroscopy (IMS), microwave and dielectric spectroscopy, terahertz spectroscopy, ultrasonic acoustic spectroscopy, and other methods.
Tribologie
(2014)
Tribologie ist die Wissenschaft und Technik von aufeinander einwirkenden Oberflächen in Relativbewcgung (DIN 50 323, Teil I). Diese Definition ist aus der englischen Originalfassung abgeleitet: Tribology - Science and tcchnology of interacting surfaces in relative motion and the practiccs related thereto 11 ]. Die Tribologie umfasst die Teilgebiete Reibung, Verschleiß und Schmierung. Sie steht in enger Beziehung zu den Werkstoffen der beteiligten Körper, deshalb ihre Behandlung in Teil H.
Damage detection can be performed by detecting changes in the modal parameters between a reference state and the current (possibly damaged) state of a structure from measured output-only vibration data. Alternatively, a subspace-based damage detection test has been proposed and applied successfully, where changes in the modal parameters are detected, but the estimation of the modal parameters themselves is avoided. Like this, the test can run in an automated way directly on the vibration measurements. However, it was assumed that the unmeasured ambient excitation properties during measurements of the structure in the reference and possibly damaged condition stay constant, which is hardly satisfied by any application. A new version of the test has been derived recently that is robust to such changes in the ambient excitation. In this paper, the robust test is recalled and its performance is evaluated both on numerical simulations and a real application, where a steel frame structure is artificially damaged in the lab.
Werkstoffe
(2014)
Für die Realisierung des in der Produktentwicklung entstandenen Produkts in der Fertigung steht heutzutage eine Vielzahl moderner Werkstoffe zur Verfügung. Ein Werkstoff ist ein Stoff, der mit der Absicht einer technischen Verwendung hergestellt wird. Werkstoffe sind feste Stoffe und grenzen sich von flüssigen Stoffen wie beispielsweise Treibstoffen und Schmierstoffen ab. Eine Einteilung der Werkstoffe in verschiedene Gruppen kann auf verschiedene Arten erfolgen, beispielsweise nach dem Einsatzgebiet, der Art der chemischen Bindung oder dem inneren Aufbau.
Confronted with indications that the SNML could be a forgery, we reviewed data from our previous analyses again and supplemented it with additional readings. Again, we were short of time. During the first measurement campaign we employed X-ray fluorescence analysis to identify specific trace elements and thereby characterize different writing and drawing materials. In the new measurement campaign, we once again carried out an extensive X-ray fluorescence analysis. In addition, this time we also employed reflection infrared spectroscopy and confocal microscopy.
As with earlier measurement campaigns, we were determined not to take samples. Throughout the process, we have continued to regard the object in question as unique, and as such not to he physically altered in any way. Throughout the analysis, however, it has been clear that non-destructive testing provides less comprehensive results than methods that require testing physical samples. The examinations described below were carried out not only on the SNML, but also on reference objects. The most important of these in this framework was the SN Graz, which is generally accepted as authentic. The following illustrates the results of the analysis in detail.