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Paper des Monats
- ja (32)
Nickel-based alloys have been widely used for gas turbine blades owing to their excellent mechanical properties and corrosion resistance at high temperatures. The operating temperatures of modern gas turbines have been increased in pursuit of increased thermal efficiency. Turbine blades are exposed to these high temperatures combined with mechanical stresses, resulting in material damage through creep, fatigue, and other mechanisms. These turbine blades must be regularly inspected and replaced as needed, to prevent the loss of efficiency, breakdown, and catastrophic failure. Repair of the damaged turbine blades is often a more practical and cost-effective option than replacement, as replacement is associated with high costs and loss of material resources. To this end, state-of-the-art repair technologies including different additive manufacturing and brazing processes are considered to ensure efficient repair and optimum properties of repaired components.
In any repaired part, materials property-mismatches and/or inner defects may facilitate the crack initiation and propagation and thus reduce the number of load cycles to failure. Therefore, a fundamental understanding of the fatigue crack growth and fracture mechanisms in joining zones is required to enable the prediction of the remaining life of repaired components and to further improve and adapt the repair technologies.
Fatigue crack growth experiments have been conducted on SEN (Single Edge Notch) specimens joined via brazing, and pre-sintered Preform (PSP) and multi-materials (casted/printed) specimens layered via additive manufacturing (AM). The experiments were performed at 950 °C and various stress ratios. The crack growth was measured using DCPD (Direct Current Potential Drop) method. The stress intensity factors for joined SEN specimens were calculated using the finite element method and then used to derive the fatigue crack growth curves. Metallographic and fractographic analyses were conducted to get insight into the fracture mechanism.
Results show that the experimental technique for fatigue crack growth was successfully adapted and applied for testing joined specimens. Furthermore, the initial tests indicate that the investigated braze filler material provides a lower resistance to crack growth, and bonding defects cause a crack to deviate to the interface of the base material and joining zone. In AM-sandwich specimens, the crack growth rates are significantly reduced when the crack reaches the interface of printed material and casted material. The obtained crack growth data can be used to calibrate a crack growth model, which will further be utilized to predict the remaining life of repaired components.
High Temperature Fatigue Crack Growth in Nickel-Based Alloys Refurbished by Additive Manufacturing
(2024)
Bhadeliya, Ashok ; Rehmer, Birgit ; Fedelich, Bernard ; Jokisch, Torsten ; Skrotzki, Birgit ; Olbricht, Jürgen
Hybrid additive manufacturing plays a crucial role in the restoration of gas turbine blades, where, e.g., the damaged blade tip is reconstructed by the additive manufacturing process on the existing blade made of a parent nickel-based alloy. However, inherent process-related defects in additively manufactured material, along with the interface created between the additively manufactured and the cast base material, impact the fatigue crack growth behavior in bi-material components. This study investigates the fatigue crack growth behavior in bi-material specimens of nickel-based alloys, specifically, additively manufactured STAL15 and cast alloy 247DS. The tests were conducted at 950 °C with stress ratios of 0.1 and −1. Metallographic and fractographic investigations were carried out to understand crack growth mechanisms. The results revealed significant retardation in crack growth at the interface. This study highlights the potential contributions of residual stresses and microstructural differences to the observed crack growth retardation phenomenon, along with the conclusion from an earlier study on the effect of yield strength mismatch on crack growth behavior at a perpendicular interface in bi-material specimens.
Nickelbasierte Superlegierungen werden in großem Umfang für Gasturbinenschaufeln verwendet, da sie einer Kombination aus hoher Belastung und hohen Temperaturen widerstehen können. Um die Effizienz moderner Gasturbinen zu verbessern, werden hohe Betriebstemperaturen angestrebt. Diese hohen Temperaturen verbunden mit mechanischen Belastungen führen zu Materialschäden aufgrund von Kriechen, Ermüdung und anderen Schadensmechanismen. Aus diesem Grund werden Turbinenschaufeln regelmäßig im Rahmen von Wartungs- und Instandsetzungsmaßnahmen geprüft und falls erforderlich ausgetauscht, um ein katastrophales Versagen im Betrieb zu vermeiden. Ein kompletter Austausch ist mit sehr hohen Kosten verbunden, weshalb geeignete Reparaturverfahren entwickelt wurden und werden. Neue Reparaturtechnologien wie die Additive Fertigung, Lötverfahren und der Einsatz von vorgesinterten Vorformen (Presintered Preform PSP) sollen eine effiziente Reparatur und optimale Eigenschaften der reparierten Bauteile sichterstellen.
Im Allgemeinen stellen die Fügezonen typische Schwachstellen dar, da sie die Anrissbildung und Rissausbreitung erleichtern und die Anzahl der Lastzyklen bis zum Bruch reduzieren können. Aus diesem Grund ist eine umfassende Untersuchung des Rissfortschrittsverhaltens in diesen, durch neue Reparaturtechnologien entstandenen Bereichen erforderlich, um die Restlebensdauer der Turbinenschaufeln vorherzusagen.
Als ein erster Beitrag zu dieser Fragestellung werden Ergebnisse von Rissfortschrittsversuchen (Fig. 1) an SENT-Proben vorgestellt, die durch Engspaltlöten gefügt wurden. Die Versuche wurden bei einer Temperatur von 950 °C und einem Spannungsverhältnis R = 0,1 durchgeführt. Die Erfassung des Rissfortschritts erfolgte mit dem Gleichstrom-Potentialsonden-Verfahren. Mit der Finite-Element-Methode konnte der Spannungsintensitätsfaktor für gefügte SENT-Proben berechnet werden, der dann zur Berechnung der Risswachstumskurven verwendet wurde. Eine abschließende licht- und rasterelektronenmikroskopische Untersuchung der Bruchflächen soll einen Beitrag zum Verständnis der Bruchmechanismen liefern und klären, ob der Riss sich im Lotwerkstoff, im Grundwerkstoff oder in der Grenzfläche ausbreitet. Die Ergebnisse werden zur Kalibrierung des Rissfortschrittsmodells und der Auslegung zukünftiger Komponenten verwendet.
Photon-based additive manufacturing technologies such as SLA, DLP, LCM, moreover volumetric two-photon-polymerization, Xolography and holographic technologies promise the highest accuracy and dimensional freedom. But to transfer the light through the feedstock it needs sufficient transparency at the used light wavelength. Ceramic particles used for powder processing routes act as scattering sites and therefore hinder the light transmission, unless…
The particle size and particle size distribution are chosen small and narrow enough. Particles which are smaller than roughly 1/10th of the light wavelength, mostly nanoparticles around 5nm size, decrease scattering vastly. This turns resins even with homogeneously distributed ceramic weight fraction of up to 80% transparent again. Feedstocks could be prepared for the highly accurate two-photon-polymerization gaining the smallest yttria stabilized zirconia structures with a resolution of 500nm and unique mechanical properties. The same feedstocks could be applied to DLP and LCM as layer-by-layer AM-technologies for bigger parts. Hybridizing both technologies lead to ceramic parts with microscopic accuracy at macroscopic dimensions. The feedstock was even applied to the volumetric Xolography with the highest transparency requirement so far and to versatile and flexible holographic AM.
Highly filled nano-particle containing transparent ceramic feedstocks open the way for technical ceramics in high precision manufacturing where the performance and durability and accessibility are increased and created by the unique ceramic properties such as mechanical strength, chemical and thermal resistance and biocompatibility
In order to be able to manipulate ceramic powder compacts and ceramic suspensions (slurries) in their volume with light, a minimum transparency of the materials is required. Compared to polymers and metals, ceramic materials are characterized by the fact that they have a wide electronic band gap and therefore a wide optical window of transparency. The optical window generally ranges from less than 0.3 µm to 5 µm wavelength. Therefore, to focus light into the volume of a ceramic powder compact, its light scattering properties need to be tailored. In this study, we present the physical background and material development strategies for the application of two-photon polymerization (2PP), Xolography and selective volumetric sintering for the additive manufacturing of structures in the volume of ceramic slips and green compacts.
Nickel-based alloys have been widely used for gas turbine blades owing to their excellent mechanical properties and corrosion resistance at high temperatures. The operating temperatures of modern gas turbines have been increased in pursuit of increased thermal efficiency. Turbine blades are exposed to these high temperatures combined with mechanical stresses, resulting in material damage through creep, fatigue, and other mechanisms. These turbine blades must be regularly inspected and replaced as needed, to prevent the loss of efficiency, breakdown, and catastrophic failure. Repair of the damaged turbine blades is often a more practical and cost-effective option than replacement, as replacement is associated with high costs and loss of material resources. To this end, state-of-the-art repair technologies including different additive manufacturing and brazing processes are considered to ensure efficient repair and optimum properties of repaired components.
In any repaired part, materials property-mismatches and/or inner defects may facilitate the crack initiation and propagation and thus reduce the number of load cycles to failure. Therefore, a fundamental understanding of the fatigue crack growth and fracture mechanisms in joining zones is required to enable the prediction of the remaining life of repaired components and to further improve and adapt the repair technologies.
Fatigue crack growth experiments have been conducted on SEN (Single Edge Notch) specimens joined via brazing, and pre-sintered Preform (PSP) and multi-materials (casted/printed) specimens layered via additive manufacturing (AM). The experiments were performed at 950 °C and various stress ratios. The crack growth was measured using DCPD (Direct Current Potential Drop) method. The stress intensity factors for joined SEN specimens were calculated using the finite element method and then used to derive the fatigue crack growth curves. Metallographic and fractographic analyses were conducted to get insight into the fracture mechanism.
Results show that the experimental technique for fatigue crack growth was successfully adapted and applied for testing joined specimens. Furthermore, the initial tests indicate that the investigated braze filler material provides a lower resistance to crack growth, and bonding defects cause a crack to deviate to the interface of the base material and joining zone. In AM-sandwich specimens, the crack growth rates are significantly reduced when the crack reaches the interface of printed material and casted material. The obtained crack growth data can be used to calibrate a crack growth model, which will further be utilized to predict the remaining life of repaired components.
Photoresponsive molecular crystals have sparked interest owing to their potential application prospects. In this study, we achieved dual mechanical responses of a cyanostilbene-based crystal BN. The crystal exhibited both stress-induced mechanical flexibility and light-induced photomechanical bending. Two distinct mechanical responses are related to different underlying phenomena and were not interlinked. While elasticity is attributed to criss-cross packing arrangement in the isotropic structure, photomechanical bending is attributed to the formation of heterogeneous phase distribution due to monomer to dimer cycloaddition product formation. The crystal did not demonstrate photoswitching activity. However, it exhibited thermal reversibility, highlighting reversible dimer to monomer conversion.
This talk presents the EU funded project PlasticTrace. It shows the challenges in micro- and nanoplastic reference materials and gives some solutions regarding spectroscipc methods such as Raman or IR microscopy to determine the particle numbers. Materials are prepared by cryo milling to get some powder that is later pressed into tablets. The polymer type used is PET, because that is highly important for drinking water directive of EU commission.
Protection against terrorist or accidental scenarios in industrial settings requires suitable designs of structures to resist blast loads. Field testing as well as finite element simulations are among the techniques available to engineers in the understanding of the structural behavior against blast loading. As blast testing of complex scenarios can be very resource intensive, tests are generally performed for simplified scenarios. Numerical tools can be used to model these scenarios in order to get a better insight into blast loading, structural response and the resulting damage to the structure. In the next steps, the simplified scenario is successively modified in numerical simulations to incorporate complexities that cannot be covered in blast testing experiments. One of the conditions for this approach to work is that the original simplified numerical simulation is valid. The scopes and challenges encountered in such a validation are the focus of this presentation. A relatively ‘simple’ field test of a horizontal reinforced concrete (RC) slab subjected to blast loading is taken as an example for validation of the performance of numerical tools. The blast test incorporated various measurement techniques to quantify the blast load as well as the behavior of the RC slab. Blast load was measured using flush-mounted piezoelectric pressure gauges, whereas acceleration sensors and fiber-optic sensor cables were used to characterize the dynamic behavior of the slab under blast loading. Additionally, damage characteristics were ascertained also using fiber-optic sensing. The application of such measurement techniques, along with different numerical software available for the analysis of the scenario in question,
demonstrate the scope of our contribution.
Traceable morphological and chemical characterization of nanomaterials with respect to the various possible sizes, size distributions, shapes, and concentrations of real-world nanoparticles (NPs) is a challenging task. Particularly for the nonspherical, non-monodisperse nanoparticles – as typically for most of the commercial particles, including their strong tendency to agglomerate, there is a lack of standard operation procedures providing accurate nanoparticle characterisation.
In the framework of the pre-standardisation framework of VAMAS (Versailles Project on Advanced Materials and Standards, www.vamas.org) two interlaboratory comparison (ILC) studies are being carried out under the Technical Working Area (TWA) 34 “Nanoparticle Populations”:i) Project #15 addresses the analysis of the size and shape distribution of TiO2 bipyramidal NPs by traceable imaging methods such as TEM, SEM, STEM-in-SEM, AFM as well as with SAXS as an ensemble method. This ILC is thought as the next level development of the case studies exemplified in the published ISO standards ISO 21363 and ISO 19749. It was agreed to complete the first ILC with the NPs already prepared according to the same procedure on a TEM grid, and, at a later stage, to carry out second ILCs with the same NPs distributed to the participants as liquid suspensions together with protocols for the uniform NP deposition on suited substrates - as developed and optimized within the European project nPSize. Once having good deposition protocols available, the door for automated image analysis gets opened. Corresponding image analysis protocols and reporting templates have been distributed to the ILC participants, too.
ii) Project #16: two spherical SiO2 NP samples with bi-modal size distributions in two nominal relative number concentrations were prepared and distributed also as liquid suspensions accompanied by sample preparation, measurement, and image analysis protocols and reporting templates. Here, the NP concentration is the primary parameter to be measured. For the imaging methods it is targeted to
measure the relative nanoparticle concentrations (relative populations of the two modes).
The results of all the participating laboratories, in both ILCs, compiled in comparative representations will be shown and discussed for the first time. The reduction of the measurement uncertainties associated to the size, shape and number-concentration results induced by the significant improvement of the sample preparation on substrates (as single particles with a high-density coverage), combined with well-defined image analysis procedures will be highlighted.
Finally, a very recent 3rd ILC an the determination of lateral size of Graphene Oxide flakes by SEM is presented as project P13 under VAMAS TWA41 Graphene and Related 2D.
Bonds and local atomic environments are crucial descriptors of material properties. They have been used to create design rules and heuristics and as features in machine learning of materials properties. Implementations and algorithms (e.g., ChemEnv and LobsterEnv) for identifying local atomic environments based on geometrical characteristics and quantum-chemical bonding analysis are nowadays available. Fully automatic workflows and analysis tools have been developed to use quantum-chemical bonding analysis on a large scale. The lecture will demonstrate how our tools, that assess local atomic environments and perform automatic bonding analysis, help to develop new machine learning models and a new intuitive understanding of materials. Furthermore, the general trend toward automation in computational materials science and some of our recent contributions will be discussed.
Many organisations are being driven towards employing sustainable practices to counteract the growing concerns of environmental and social issues. With various stakeholders including governments, suppliers and customers putting on pressure the process industry is no exception. However, many industrial firms struggle to implement sustainability measures. One of the usual first steps when conducting implementation is to analyse the current situation. For this analysis, indicators are commonly used to measure, monitor, and report a company’s sustainable development performance. However, the selection of appropriate indicators is often challenging due to the current lack of relevant methodologies, guidelines, and insights into a practitioner perspective.
To address this challenge, this work focuses on the creation of a user-orientated method, which helps practitioners in the process industry to select relevant indicators for their plant and assist in the deduction of sustainability measures. This includes addressing the difficulties of implementation and regarding the current needs like the inclusion of indicators for reporting or the quantification of gathered metrics.
The presentation is divided into two parts. The first part is about the influence of the oxygen content to results testing the oxygen compatibility. BAM performed tests with several nonmetallic sealing materials such as PTFE, PA 6.6, and EPDM with different oxygen contents between 21 Vol% and pure oxygen. Using the standardized oxygen pressure surge tester, the results have shown, that even a small increase in the oxygen content above 21% in air is associated with a significant reduction on the maximum test pressure at which no reaction of the material occurs. Using the standardized tester to determine the autogenous ignition temperature of the materials in oxygen, the results have shown, that even a small increase in the oxygen content above 21% in air is associated with a significant reduction on the autogenous ignition temperature at which the material shows self-ignition without an additional ignition source. The second part of the presentation is about the oxygen endurance test according to DIN EN ISO 10297, which is generally performed with air or with nitrogen. However, BAM performed this test with oxygen. In some cases, different test results were found: Valves failed the endurance test with oxygen but passed the endurance test with air. Based on the results with different oxygen content and with the oxygen endurance tester, it is unclear, why materials and valves for oxygen are still not consistently tested with oxygen.
Motivation: A precise diagnosis of atherosclerosis is of clinical importance, since cardiovascular disease remain one of the leading causes of death worldwide.
Goal(s): The goal of this study was to evaluate the feasibility of characterizing a disintegrin and metalloproteinase with thrombospondin motifs (ADAMTS4) using molecular magnetic resonance imaging in a preclnical model of atherosclerosis.
Approach: Molecular magnetic resonance imaging using a novel probe targeted against ADAMTS4 was used in a high-fat murine model.
Results: It was possible to image atherosclerotic lesions in a mouse model using an ADAMTS4- specific probe for magnetic resonance imaging.
Impact: Using molecular MRI targeting ADAMTS4 is a promising method for characterization of plaque composition and could possibly impact plaque vulnerability assessment in the diagnosis and treatment of atherosclerosis in patients.
In this paper we present a new hydrogen-based test rig for an ongoing feasibility study of using hydrogen as an energy source for the thermal testing of transport packages containing radioactive materials. The test rig will be capable of combusting hydrogen for a wide range of different burner geometries, mass flows and if necessary hydrogen blends. As this type of fire test according to the IAEA boundary conditions does not yet exist, a large number of preliminary investigations, safety assessments and calculations must be carried out in order to develop a viable concept for hydrogen fires. In the first step of the feasibility study, the temperature, structure, and radiation of various hydrogen flames are surveyed. In future works, the results will make it possible to design burner frames that are suitable for fire reference tests in order to make comparisons with pool and propane fires used in assessment procedures today. In parallel comparative numerical simulations are conducted to model the thermal behaviour of hydrogen flames using the software package Ansys®. On the one hand, the numerical simulations support the experiments by providing an overview of numerous parameters and the measuring range; on the other hand, they will help with the design of the burner frame in future work. This paper gives an overview in the design and capabilities of the test rig. Furthermore, the results of the parameter studies show that burner geometry and mass flow provide a significant design margin for the thermal shape of the hydrogen flames. In addition, the results of the initial numerical calculations will be used to determine the necessary sensors, the positions, and their operating range. Only the optimal interaction allows a controlled system that permits user-defined hydrogen fires.
In Germany, the search for a final repository for highly radioactive material is currently based on the assumption that interim storage will take considerably longer than was anticipated. At that time, authorization procedures assumed that interim storage would be brief, until the containment systems could be placed in a final repository. For today's new approvals and extensions, the IAEA (International Atomic Energy Agency) regulations for the transport of radioactive material require an assessment of all components and component groups with regard to ageing. To assess the safety requirements not only over the previously envisaged periods but also over long durations, numerous individual parts and component groups must be examined and evaluated for ageing and interactions between materials. The metal seals of a double lid sealing system, for example, are critical components that must be studied with respect to ageing. In a containment system for radioactive material, metal seals must not only undergo classic ageing, but also withstand mechanical influences and radiation over extended periods. In addition to assessments by the applicants, BAM must also independently analyze and evaluate these ageing mechanisms as part of its sovereign mandate.
Another challenge in both new approvals and extensions is the assessment of transport regarding changes in the state of the art, which are not synchronously assessed in the regulations. In transporting radioactive material, a classic oil fire has been assumed in a hypothetical accident scenario from the development of the regulations to the present day. Due to the rapid development of propulsion technologies in recent years, such as battery or hydrogen-powered vehicles, investigations must be conducted in the revision process of the IAEA regulations to assess the impact of these new technologies on safety assessments. It is important for the member states of the IAEA to know whether new technologies are covered by the regulations or if changes are necessary to continue issuing international licenses. By focusing on batteries from the material to the cell to the module and the application, BAM contributes to the evaluation of batteries at every step of the chain. In addition to the safety of current and new battery technologies, BAM also endeavors to address issues of compositional trace and sustainable energy materials.
The integration of advanced simulation models into industrial applications, especially in civil engineering, is a challenge that requires to develop new concepts. In particular, this is related to the validation of models using open access and FAIR data as well as objective methods for identifying model parameters and model comparison with the integration of both the models and their calibration into reproducible workflow systems.
The challenges are illustratively discussed for a variety of applications ranging from bridge monitoring over the structural behavior under blast loading up to the additive manufacturing of concrete. An important basis for model validation is the existence of machine-readable data structures for experimental data, e.g. based on semantic representations. In addition, platforms to share this structured data in a searchable format in addition with reproducible scientific workflows must be established.
Based on these tools, objective methods for model parameter estimation and validation of the models are a critical step in ensuring their accuracy and usefulness in industrial applications. Bayesian inference is one approach that can be used to optimize simulation parameters, improving the accuracy of the model while being able to estimate the uncertainty. Integrating these procedures in a real-time application with a bidirectional information exchange between the physical systems and the virtual simulation model leads to the concept of digital twins.
For complex simulation models, the computational efficiency is a significant barrier both for real-time applications and in the context of model calibration with potentially millions of required forward-model evaluations. As a consequence, reduced order modeling approaches such as the proper generalized decomposition method can be used to build an efficient to evaluate model - speeding up the online computation but requiring a precomputation in an offline phase.
Finally, a perspective for integrating material and structural design into a joint design optimization is given. The integration of advanced simulation models into industrial applications is a rapidly evolving field with significant potential for innovation and progress. From additive manufacturing of concrete to digital twins and reduced order modeling, there are many tools and approaches that can be used to improve industrial processes and drive progress in a variety of industries.
Experimental And Numerical Analyses For The Evaluation Of Heat Fluxes Of A Fire Reference Test
(2024)
Packages for the transport of high-level radioactive material are designed to endure severe accidents. To obtain approval, these transport packages must adhere to the specification-based criteria of the IAEA SSR-6 [1]. To ensure compliance with these requirements, specific mechanical and thermal tests need to be appointed with respect to the package type. Typically, IAEA SSR-6 [1] prescribes mechanical tests followed by a thermal fire test as part of a cumulative test sequence. To approve the fire test, BAM uses a reference package representing the original package in its outer geometry for characterizing the actual fire and its impact on the package. This serves a dual purpose: it allows the precise adjustment of experimental parameters for the package design to be approved, and it provides input parameters for thermomechanical simulations, cf. [2]. With the help of this methodology for characterizing boundary conditions of the package, temperature evolutions within the reference package can be studied in a Finite-Element Analyses (FEA). This helps to compare the experiments with the numerical simulations on the case of the reference package, but also serves at the same time for preliminary simulations with the package design to be approved.
The thermal test consists of a 30-minute fully engulfing 800°C pool fire or an equally severe fire, e.g. a propane gas fire. The fire reference test is performed prior to the regulatory fire test with the package design to be approved. The fire reference package in the described case is a closed sheet 316L steel cylinder with a wall thickness of 10 mm, a length of 182 mm, and a diameter of 102 mm. The package was instrumented with thermocouples and filled with heat resistant insulating material.
Metal additive manufacturing (Metal AM) continues to gain momentum. Many companies explore the manufacturing of innovative products, including components for safety critical applications. Despite the intensive research of recent years, a fundamental understanding of the process‑structure‑property relationships remains challenging due to, i.a., the inherently complex and highly hierarchical microstructures arising from the wide range of build process parameter variability. This contribution presents the resu lts of an experimental study on the creep behavior of an austenitic 316L stainless steel produced by laser powder bed fusion (PBF LB/M/316L) with an emphasis on understanding the effects of microstructure on creep mechanisms. Hot tensile tests and constant force creep tests at 600 °C and 650 °C, X ray computed tomography, as well as optical and electron microscopy were performed. The produced PBF LB/M/316L exhibits a low void population 0.01 %) resulting from the manufacturing parameters used and which a llowed us to understand the effects of other microstructural aspects on creep behavior, e.g., grain morphology and dislocation substructure. A hot‑rolled variant of 316L hwas also tested as a reference. The produced PBF LB/M/316L possesses shorter primary and secondary creep stages and times to rupture and smaller creep stress exponents than the hot‑rolled variant. Overall, the creep damage is more extensive in the PBF LB/M/316L and is characterized as predominantly intergranular. It is considered that the damage behavior is mainly impacted by the formation of precipitates at the grain boundaries combined with their unfavorable orientation. The dislocation substructure and local elemental segregation appear to have a decisive impact on the overall creep behavior.