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Integrated Coating System for Corrosion Protection of Carbon Steel in Artificial Geothermal Brine
(2022)
Corrosive geothermal brines are a major challenge to geothermal power-plants. For cost reasons, plant designers prefer to use carbon and low alloyed steels, which are susceptible to uniform and localized corrosion when exposed to geothermal brines having acidic and saline properties. To solve such problem, coatings or inhibitors would be a protective solution as an alternative to the use of high alloyed materials.
This study investigated a coating system consisting of polyaniline/silicon dioxide based on resources locally available in Indonesia. Protection against corrosion of carbon steel was shown by long-term (28 day) exposure and electrochemical tests of coated carbon steels, performed in an artificial acidic and saline geothermal brine, comparable to the conditions encountered at a site in Indonesia.
Therefore, an integrated coating system is proposed for corrosion protection, combining the electrochemical functionality of polyaniline and the physical advantages of silica.
Valorizing “non-vegan” bio-fillers: Synergists for phosphorus flame retardants in epoxy resins
(2022)
Sustainable, biogenic flame retardant adjuvants for epoxy resins are receiving increased focus. Zoological products like insects, bone meal, and eggshells are available in large quantities, but remain uninvestigated as functional fillers to epoxy resins, although they are potential synergists to flame retardants. The efficacy and flame retardancy of “non-vegan” additives in combination with flame retardants is investigated and the fire behavior and thermal decomposition of bio-sourced epoxy resin composites is characterized. By comparing the fire performance of composites containing flame retardants or fillers at varying loadings (5, 10, and 20%), their role as synergists that enhance the function of organophosphorus flame retardants in bio-epoxy composites is identified and quantified. Peak heat release rates were 44% lower in composites containing both filler and flame retardant versus those containing only flame retardants, and fire loads were reduced by 44% versus the pure resin, highlighting the ability of “non-vegan” fillers to function as synergists.
The important take home message of this chapter: When multicomponent flame retardant systems are applied to polymeric materials, it becomes possible to address multiple fire properties, increase efficiency, and minimize flame retardant use to maximize polymer property balance. Flame retardants are combined or used together with adjuvants or synergists; fibers and fillers make a crucial contribution to their fire properties. Multicomponent systems are discussed in their capacity as an overall powerful strategy for achieving and optimizing non-halogenated flame-retardant polymeric materials.
Reliable assessment of earthen dams’ stability and tailing storage facilities widely used in the mining industry is challenging, particularly under seismic load conditions. In this paper, we propose to take into account the effect of the dominant frequency of seismic load on the stability assessment of tailing/earthen dams. The calculations are performed by finite element modelling (FEM) with the Mohr–Coulomb failure criteria. To separate the frequency content from other dynamic parameters describing the seismic wave, synthetic waveforms with identical amplitude and attenuation characteristics, but differing spectral characteristics have been used. The analysis has been performed for three different slope angles and two scenarios of seismic wave propagation. Consequently, the changes of total displacement and shear stresses depending on the frequencies have been determined and clearly show that lower frequencies cause higher stress levels and displacement. Finally, the response surface methodology has been applied to determine how different parameters affect the slope stability under dynamic load conditions. Overall, this study is a first step to improve the existing methods to assess slope stability when considering seismic load.
Phase-sensitive optical time domain reflectometry becomes an effective tool to realize distributed sensing, and the optical phase of the received light is usually used to quantify the strain for both dynamic and static measurement. The analysis on the overall phase error has been improved by considering the proportionality of the detection noise to the local optical power. The estimation accuracy is greatly improved by using the proposed theory, the probability density of the estimation accuracy over 99% is > 0.6, ∼39 times larger than the previously reported method. The phase unwrapping may malfunction due to the noisy signal, causing large phase errors. Point break detection algorithms are used to locate the incorrect phase unwrapping points, so the temporal evolution of the phase retrieved at each position can be divided into several sections with different offset. The phase unwrapping error is then suppressed by removing the offset.
Irregularities of the track are a main cause of train-induced ground vibration, and track maintenance is of great importance. Although geometric irregularities at the wheel-rail contact are widely used, other types of irregularities, such as stiffness irregularities, irregularities from different track positions and irregularities in the wave propagation, were analysed in the present study. The track behaviour was investigated by a multi-beam-on-soil model. This track model is coupled with a vehicle model to calculate the vehicle–track interaction. The track model was also used for the track filtering, which transfers a track support error to the equivalent rail irregularity or, conversely, the sharp axle pulse on the rail to a smoother pulse on the soil. In the case in which this filtering varies randomly along the track, the pulses of the moving static load induce a certain ground Vibration component (“the scatter of axle pulses”). This effect was calculated by the superposition of axle pulses in the frequency domain and by a stochastic simulation. Simultaneous vehicle, track and soil measurements at a certain site were used to evaluate the different excitation and ground Vibration components. The agreement between calculations and axle-box and soil measurements is good. The ground vibrations calculated from rail irregularities and corresponding dynamic loads, however, clearly underestimate the measured ground vibration amplitudes. Only the static load that is moving over a varying track support stiffness can produce the important mid-frequency ground Vibration component by the scatter of axle pulses.
The knowledge of the thermal parameters of a particular concrete is essential for thermal design of a building, but also could help to identify and assess the state of a concrete structure. Active thermography has the potential to be applied onsite and to provide a fast investigation of thermal properties. In this work, three different concrete samples were investigated by active thermography in reflection and in transmission setup. It was found that this method yields the same results without direct contact as the Transient Plane Source (TPS) method as an established inspection tool.
Die verteilte faseroptische akustische Sensorik (DAS) wird vorgestellt, hinsichtlich ihrer Leistungsfähigkeit beschrieben und verschiedenste Anwendungsfelder, z.B. für das Zustandsmonitoring oder für seismische Messungen, beispielhaft gezeigt. Zudem werden mögliche Anwendungsfelder von DAS für den Kontext Kerntechnische Entsorgung (KTE) und Rückbau aufgezeigt.
The incorporation of nanoparticles like multilayer graphene (MLG) into elastomeric composites boosts their technical performance, such as their mechanical behavior and electrical conductivity. Common filler types (carbon black (CB) and aluminum trihydroxide (ATH)) generally fulfill single, specific purposes and are often used in high loadings. CB typically reinforces rubber mechanically, while ATH increases flame retardancy. Small amounts of MLG reduce these high filler contents and maintain the multifunctional characteristics of rubber composites. In chlorosulfonated polyethylene (CSM) + ATH, an intrinsically flame-retardant rubber was designed to achieve the highest standards such as maximum average of heat emission (MARHE) <90 kW m−2, 3 phrMLG was substituted for 15 phr CB and/or 3 phr ATH via an industrially applicable processing approach. Replacing either CB or ATH resulted in a property profile that was multifunctionally improved in terms of features such as mechanical performance, reduced sorption, and flame retardance. MLG nanocomposites are reported to show promise as an industrially utilizable route to obtain multifunctional high-performance rubbers.
To set up recommendations on how to define “reasonable minimum composition thresholds” for CO2 streams to access CO2 pipeline networks, we investigated potential impacts of CO2 streams with different and temporally variable compositions and mass flow rates along the CCS chain. All investigations were based on a generic “CCS cluster scenario” in which CO2 streams captured from a spatial cluster of eleven emitters (seven fossil-fired power plants, two cement plants, one refinery and one steel mill) are collected in a regional pipeline network. The resulting CO2 stream (19.78 Mio t impure CO2 per year) is transported in a trunk line (onshore and offshore) and injected into five generic replicate storage structures (Buntsandstein saline aquifers) offshore. Experimental investigations and modeling of selected impacts revealed beneficial as well as adverse impacts of different impurities and their combinations. Overall, no fundamental technical obstacles for transporting, injecting and storing CO2 streams of the considered variable compositions and mass flow rates were observed. We recommend to define minimum composition thresholds for each specific CCS project through limiting
i) the overall CO2 content,
ii) maximum contents of relevant impurities or elements,
iii) acceptable variability of concentrations of critical impurities, and defining impurity combinations to be avoided.