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Paper des Monats
- ja (11)
A method of solving the thermo-fluid dynamics problem is presented, enabling the prediction of the shape and dimensions of the weld pool during keyhole laser welding of thick plates. It is shown that the rear weld pool boundary can be satisfactorily approximated by a set of superellipses (Lamé curves). The presence of a convex rear weld pool boundary in the mid-plane has been observed experimentally and reproduced numerically. It was shown that in this zone the concentration of liquating impurities increases and the local solidification temperature decreases, contributing to the susceptibility to hot cracking.
AbstractThe sustainable and resource-efficient production of wind energy plants requires the use of modern high-strength fine-grain structural steels. This applies to both foundation and erection structures, like mobile or ship cranes. During the assembly of steel structures, unacceptable defects can occasionally be found in the weld area. In most cases, the economical solution would be local thermal gouging of the affected areas and re-welding. Due to the high shrinkage restraint of the joint groove in the overall structure, the superposition of global and local welding-induced stresses may lead to crack formation and component failure, particularly in interaction with the degradation of the microstructure and mechanical properties of high-strength steels during the repair process. However, manufacturers hardly have any information about these issues and there is a lack of recommendations and guidelines to take these safety-relevant aspects into account in adequate repair concepts. The aim of this research is to derive recommendations for repair concepts appropriate to the stresses and materials involved providing a basis for standards and guidelines to avoid cold cracking, damage and expensive reworking especially for high-strength steels. Part 1 of this study involves systematic investigations of influences of shrinkage restraint during repair welding of two high-strength steels S500MLO for offshore application and S960QL for mobile crane structures. The quantification of the shrinkage restraint of repair weld joints was achieved by means of experimental and numerical restraint intensity analysis. In welding experiments with self-restrained slot specimens, restraint intensity and introduction of hydrogen via the welding arc using anti spatter spray were varied systematically to analyse the effect on welding result, residual stresses and cold cracking. It could be shown that increasing restraint intensities result in significantly higher transverse residual stress levels. In the case of hydrogen introduction S500MLO showed no cold cracking independent of the restraint conditions. However, S960QL was found to be considerably cold cracking sensitive if hydrogen is introduced. With increasing restraint intensity length and number of cold cracks increases significantly. Part 2 [1] of this study is focussed on microstructure and residual stresses due to gouging and stress optimization via adequate heat control parameters in repair welding.
The high potential of hydrogen as a key factor on the pathway towards a climate neutral economy, leads to rising demand in technical applications, where gaseous hydrogen is used. For several metals, hydrogen-metal interactions could cause a degradation of the material properties. This is especially valid for low carbon and highstrength structural steels, as they are commonly used in natural gas pipelines and analyzed in this work.
This work provides an insight to the impact of hydrogen on the mechanical properties of an API 5L X65 pipeline steel tested in 60 bar gaseous hydrogen atmosphere. The analyses were performed using the hollow specimen technique with slow strain rate testing (SSRT). The nature of the crack was visualized thereafter utilizing μCT imaging of the sample pressurized with gaseous hydrogen in comparison to one tested in an inert atmosphere.
The combination of the results from non-conventional mechanical testing procedures and nondestructive imaging techniques has shown unambiguously how the exposure to hydrogen under realistic service pressure influences the mechanical properties of the material and the appearance of failure.
Die additive Fertigung mittels Schweißverfahren bietet große ökonomische Vorteile für eine ressourceneffiziente Bauteilherstellung. Offene Fragen bezüglich Homogenität, Anisotropie der Schweißgefüge und den damit verbundenen Bauteileigenschaften stehen einer wirtschaftlichen Verarbeitung oftmals im Wege. Finale Bauteilgeometrie und Oberflächengüte erfordern meist komplementäre subtraktive Fertigungsschritte. Werkstoffe für hochbelastbare Komponenten sind oftmals schwer spanbar. In einem Vorhaben der BAM und des ISAF wurde untersucht, wie die Modifikation der AM-Schweißzusätze und das ultraschallunterstützte Fräsen (US) die Zerspanungssituation verbessern. Der vorliegende Artikel stellt wesentliche Zusammenhänge zwischen Legierung, Gefüge und Zerspanung zweier schwer spanbarer Hochleistungslegierungen (FeNi und CoCr) dar. Großes Potenzial zeigte neben dem US die Modifikation mit Zr und Hf bei Zulegierung in das Schweißgut mittels Beschichtung von Massivdrähten bzw. Herstellung von Fülldrähten.
The present Ph.D. thesis provides a comprehensive experimental and theoretical study of the bulging-cracking relationship in laser beam welding of thick unalloyed steel sheets. It focuses on experimentally proving the existence of the bulging region and on developing a coupled multiphysics mathematical framework to analyze its influence on the three critical factors controlling the susceptibility to solidification cracking, namely the thermal, metallurgical, and mechanical factors.
The research employs a novel experimental setup, utilizing a combination of transparent quartz glass and thick unalloyed steel sheet, enabling real-time visualization of the weld pool geometry and confirming the existence of a distinctive bulging region. To deepen the understanding of these experimental insights, an extensive multiphysics mathematical framework was developed and rigorously verified and validated. This framework introduces an innovative approach using Lamé curves for accurately describing complex three-dimensional weld pool geometries, including the bulging region's characteristics. Through analytical solutions and numerical procedures, it facilitates the computation of solidification parameters, which are crucial for understanding the metallurgical aspects of crack formation. The framework also incorporates a mechanical model to assess and evaluate the local stress distribution within the bulging region.
The findings indicate that an elongated, sharply shaped bulging region significantly increases the susceptibility to solidification cracking. This is attributed to its adverse impact on the distribution and local dwell time of liquid metal residing at grain boundaries during solidification, combined with the localized tensile stresses identified in the bulging region.
In essence, this research contributes to the broader understanding of solidification cracking in laser beam welding of thick unalloyed steel sheets, with a particular focus on the bulging region. The insights and methodologies developed in this thesis are valuable for future research and advancements in the application of the laser beam welding technology for joining high-thickness unalloyed steel components.
This study investigates the room‐ and high‐temperature (650 °C) tensile and low‐cycle‐fatigue behavior of Inconel 718 produced by laser powder bed fusion (PBF‐LB/M) with a four‐step heat treatment and compares the results to the conventional wrought material. The microstructure after heat treatment is characterized on different length scales. Compared to the wrought variant, the elastic and yield properties are comparable at both test temperatures while tensile strength, ductility, and strain hardening capacity are lower. The fatigue life of the PBF‐LB/M variant at room temperature is slightly lower than that of the wrought material, while at 650 °C, it is vice versa. The cyclic stress response for both material variants is characterized by cyclic softening, which is more pronounced at the higher test temperature. High strain amplitudes (≥0.7%) at room temperature and especially a high testing temperature result in the formation of multiple secondary cracks at the transitions of regions comprising predominantly elongated grain morphology and columns of stacked grains with ripple patterns in the PBF‐LB/M material. This observation and pronounced crack branching and deflection indicate that the cracks are controlled by sharp micromechanical gradients and local crystallite clusters.
The presentation gives an overview of BAM's activities on processing influences and application properties of MPEAs in the form of joined and machined high and medium entropy alloys (CoCrFeMnNi and CoCrNi). In the case of welding, the focus is on defect-free welded joints with sufficient mechanical properties. In the case of machining, the focus is on the possible influence on the surface quality of the materials through adequate milling parameters. In addition, the hydrogen absorption and diffusion properties as well as the electrochemical corrosion behavior are fundamentally examined.
Despite the advances in hardware and software techniques, standard numerical methods fail in providing real-time simulations, especially for complex processes such as additive manufacturing applications. A real-time simulation enables process control through the combination of process monitoring and automated feedback, which increases the flexibility and quality of a process. Typically, before producing a whole additive manufacturing structure, a simplified experiment in the form of a beadon-plate experiment is performed to get a first insight into the process and to set parameters suitably. In this work, a reduced order model for the transient thermal problem of the bead-on-plate weld simulation is developed, allowing an efficient model calibration and control of the process. The proposed approach applies the proper generalized decomposition (PGD) method, a popular model order reduction technique, to decrease the computational effort of each model evaluation required multiple times in parameter estimation, control, and optimization. The welding torch is modeled by a moving heat source, which leads to difficulties separating space and time, a key ingredient in PGD simulations. A novel approach for separating space and time is applied and extended to 3D problems allowing the derivation of an efficient separated representation of the temperature.
The results are verified against a standard finite element model showing excellent agreement. The reduced order model is also leveraged in a Bayesian model parameter estimation setup, speeding up calibrations and ultimately leading to an optimized real-time simulation approach for welding experiment using synthetic as well as real measurement data.
Stresses in repair welding of high-strength steels—part 2: heat control and stress optimization
(2024)
In welding of high-strength steels, e.g. for foundations and erection structures of wind energy plants, unacceptable defects can occasionally be found in the weld area, which should be removed by thermal gouging and subsequent re-welding. High shrinkage restraint of repair welds may lead to crack formation and component failure, predominantly in interaction with degraded microstructures and mechanical properties due to repair cycles. This study aims for elaboration of recommendations for repair concepts appropriate to the stresses and materials involved to avoid cold cracking, damage and expensive reworking. In part 1 [1] of this study, systematic investigations of influences of shrinkage restraint on residual stresses and cold cracking risk during repair welding of two high-strength steels S500MLO for offshore application and S960QL for mobile crane structures were focussed. In this part 2, the microstructure, particularly hardness, and residual stresses due to gouging and influences of heat control parameters in repair welding are analysed. A clear reduction in residual stress after gouging can be observed, especially for the specimens with restrained transverse shrinkage. Gouging to a depth of approx. 2/3 of the seam height does not lead to a complete relaxation of the observed reaction forces. Particularly for the higher strength steel S960QL, there are pronounced areas influenced by the gouging process in which a degradation of the microstructure and properties should be assumed. Overall, the repair welds show a significant increase in the width of the weld and HAZ compared to the original weld, especially in the case of S960QL/G89. The repair welds show higher welding-induced stresses than the original welds, especially in the areas of the HAZ and the base metal close to the weld seam. This behaviour can be attributed overall to increased restraint conditions due to the remaining root weld or shorter gouge grooves. In good agreement with earlier investigations, the residual stresses transverse to the weld can be significantly reduced by upwardly limited working or interpass temperatures, and the reaction stresses resulting from high restraint conditions can be effectively counteracted. The influence of the heat input on the stress formation is low compared to the interpass temperature for both test materials.
Dieser Beitrag befasst sich mit der Entwicklung eines wirtschaftlichen und robusten Verfahrens zum Schweißen dicker Stahlbleche. Es werden Ergebnisse für das Fügen von Blechen im Dickenbereich von 25 mm bis 80 mm vorgestellt. Die 30 mm dicken Schweißnähte konnten im Stumpfstoß in zwei Durchgängen unter Verwendung des Laserhybridschweißens und des Unterpulverschweißens (UP) geschweißt werden. Das Laserhybridschweißen wird als Einschweißung mit einer Tiefe von ca. 25 mm ausgeführt. Die UP-Lagen werden auf der gegenüberliegenden Seite des Blechs aufgebracht. Bei richtiger Wahl der Schweißparameter wird der
Nahtquerschnitt durch eine sichere Überlappung beider Lagen geschlossen. Bei Blechdicken über 30 mm ist eine Kantenvorbereitung erforderlich, die eine Ausführung der UP-Fülllagen in Engspalttechnik ermöglicht. Die Vorteile der vorgeschlagenen Prozesskombination liegen darin, dass die Nahtwurzel der Laserhybridnaht nicht geformt werden muss. Defekte in der Wurzel der Laserhybrideinschweißung können durch die UP-Lagen effektiv beseitigt werden. Das Verfahren bietet eine hohe Stabilität des Schweißprozesses in Bezug auf die
Qualität der Blechkanten. Plasmageschnittene Kanten konnten ohne Bindefehler geschweißt werden. Die erreichte Nahtqualität wurde durch zerstörende und zerstörungsfreie Prüfungen bestätigt.
In this presentation, the results of the determination of the diffraction and single-crystal elastic constants of laser powder bed fused Inconel 718 are presented. The analysis is based on high-energy synchrotron diffraction experiments performed at the Deutsches Elektronen-Synchrotron. It is shown that the characteristic microstructure of laser powder bed fused Inconel 718 impacts the elastic anisotropy and therefore the diffraction and single-crystal elastic constants. Finally, the consequences on the diffraction-based residual stress determination of laser powder bed fused Inconel 718 are discussed.
Based on the state-of-the-art research and regulations, the application of the fracture mechanics master curve (MC) concept to ferritic ductile cast iron (DCI) is being investigated in a joint research project between MPA Stuttgart and BAM Berlin. This paper outlines the research approach, the planned investigations and first results of the experimental program.
Der Bau von Gründungs- und Turmstrukturen für Windkraftanlagen erfordert den Einsatz moderner, nachhaltiger und ressourcenschonender hochfester Feinkornbaustähle. Durch den Schweißprozess verursachte Schweißnahtfehler sind nicht akzeptabel. Um diese zu beheben, ist das lokale thermische Fugenhobeln mit anschließendem Reparaturschweißen ein gängiges und wirtschaftliches Verfahren. Die hohe Schrumpfbehinderung um die ausgefugte Nut durch das umgebende Gefüge kann zu Rissbildung führen, wenn sich konstruktiv bedingte Spannungen und Eigenspannungen aus der Reparaturschweißung überlagern. Diese Gefahr wird durch die Verschlechterung der Mikrostruktur und der mechanischen Eigenschaften hochfester Stähle während des Schweißreparaturprozesses noch verstärkt.
For the hydrogen-based energy economy of tomorrow, the construction of the necessary infrastructure will play a central role. Most materials used to date, such as welded steels, can be prone to hydrogen embrittlement under certain conditions. This includes the classic delayed cold cracking during welding as well as degradation phenomena during service of components in hydrogen-containing environment. For the evaluation of any hydrogen effect, for example, on the mechanical properties of a welded metallic material, the hydrogen content must be precisely determined. In the case of weld seams, the carrier gas hot extraction (CGHE) according to ISO 3690 is meanwhile state-of-the-art. CGHE is based on accelerated hydrogen degassing due to the thermal activation of hydrogen at elevated temperatures. In addition to the quantification of hydrogen, thermal desorption analysis (TDA) with varying heating rates can be used to determine and evaluate the hydrogen trapping at microstructural defects in the material. For both techniques, experimental and metrological influences must be considered, which have a major effect on the result. For example, ISO 3690 suggests different sample geometries and minimum extraction times for CGHE. This study summarizes the results and experiences of numerous investigations at the Federal Institute for Materials Research and Testing (BAM) with different sample temperatures and geometries (ISO 3690 type B and cylindrical TDA samples) regarding the influence of the sample surface (polished/welded), measurement accuracy depending on the sample volume and the insufficient monitoring of the effect of PI control on the extraction temperature. A deviating extraction temperature from the target temperature can significantly falsify the measurement results. Based on the results, methods are shown which allow the desired extraction temperature to be reached quickly without physically interfering with the measuring equipment. This serves to significantly improve the reliability of the hydrogen measurement through increased signal stability and accelerated hydrogen desorption. In general, an independent temperature measurement with dummy samples is recommended for the heating procedure of choice to exclude possible undesired temperature influences before the measurement. The methods described can be transferred directly to industrial applications
In this contribution, we present a physically motivated heat source model for the numerical modeling of laser beam welding processes. Since the calibration of existing heat source models, such as the conic or Goldak model, is difficult, the representation of the heat source using so-called Lamé curves has been established, relying on prior Computational Fluid Dynamics (CFD) simulations.
Lamé curves, which describe the melting isotherm, are used in a subsequent finite-element (FE) simulation to define a moving Dirichlet boundary condition, which prescribes a constant temperature in the melt pool. As an alternative to this approach, we developed a physically motivated heat source model, which prescribes the heat input as a body load directly. The new model also relies on prior CFD simulations to identify the melting isotherm. We demonstrate numerical results of the new heat source model on boundary-value problems from the field of laser beam welding and compare it with the prior CFD simulation and the results of the Lamé curve model and experimental data.
Electromagnetic stirring is known to promote material flow, reduce porosity, uniform elements distribution, and refine grain in laser beam welding (LBW), which enhances the applicability of LBW in various industries. In this study, a phase-field model of dendrite growth in AA5754 Al alloy electromagnetic stirring laser beam welding was established. The model considered the thermal electromagnetic Lorentz force resulting from the interaction between the electric field generated by the Seebeck effect and the magnetic field, as well as the temperature gradient and solidification rate of the solidification interface obtained from the computational fluid dynamics electromagnetic stirring LBW model. The variation rules of dendrite growth with different magnetic parameters and effects are analyzed. Comprehensively, the magnetic field promotes the solidification rate, thus promoting interfacial instability and a large magnetic flux density leads to a faster interface instability. The solidification rate as well as the temperature gradient affect the growth rate, and the accelerated growth caused by the so lidification rate with a high frequency and a large magnetic flux density effectively inhibits the slow growth caused by the temperature gradient. The thermal electromagnetic Lorentz force is the main factor for the branch increment at low frequencies, while both thermal electromagnetic Lorentz force and temperature gradient in crease the number of branches at high frequencies. The calculated average branch numbers considering various factors in the stable stage under different magnetic parameters were consistent with the results of the scanning electron microscope tests.
Next to chemical composition, metallurgy and welding parameters, the intensity of restraint is one of the variables influencing solidification cracking. Tests like the Houldcroft Test, rate the hot cracking susceptibility indirectly on the amount of restraint the welding can endure without cracking. Modern lightweight steel construction welds can be subject to a larger amount of restraint due to their high-strength nature compared to classical use cases. By varying the plate thickness of Controlled Thermal Severity (CTS) tests produced out of S1100 QL, it was possible to vary the intensity of restraint on fillet welds at a high level. Testing was conducted with four different filler wires for Metal Active Gas (MAG) welding, including three solid and one metal-cored wire. In addition, two sets of welding parameters were tested. The first set with high heat input and high welding speed was shown to be more prone to solidification cracking compared to the second set with lower heat input and welding speed. The results show an increase in solidification cracking with increasing restraint severity.
This article focuses on the selective placement of additional LTT layers to generate compressive residual stresses in fatigue-critical areas of conventional weld joints. This enables an economical solution without effecting the integrity of welded joints. For this, longitudinal stiffeners made of high-strength steel were gas metal arc welded using conventional welding consumable in the first layer. Afterwards, a chromium-nickel alloyed LTT welding consumable was deposit on front sides of the stiffeners. By varying the welding parameters, different weld geometries of the LTT filler metal could be analyzed. The effects of additional LTT layers were investigated with regards to residual stresses, microstructure and strength. X-ray residual stresses measurements show that the residual stresses at the failure critical weld toe are significantly reduced by using additional LTT layers. While the conventional weld is characterized by tensile residual stresses, compressive residual stresses can be detected at the LTT weld. The level of residual stresses is influenced by the geometry of the LTT layer. Additional LTT layers with a high offset to the conventional weld generate more compressive residual stress in the HAZ than with a low offset. Therefore, the weld geometry has a considerable impact on the residual stress profile.
Influence of machining on residual stresses in additive manufactured high-strength steel components
(2024)
This study focuses on the effect of machining on the residual stresses and distortion of WAAM specimens. Defined specimens were welded fully automatically with a special WAAM solid wire (yield strength >820 MPa) with different geometric designs. The residual stresses state before and after cutting of the AM structure from the substrate plate were analyzed by means of X-ray diffraction on the specimen surface and complementary by 3d deformation analyses using photogrammetry. The results reveal significant influences of the geometry on the relaxation and redistribution of residual stresses.
MVT testing was conducted in Transvarestraint mode in multiple welding conditions and under a range of bending speeds. The materials observed were high strength filler metals used in GTAW namely DIN EN ISO 16834-A G 69 4 M21 Mn3Ni1CrMo (G69), 16834-A G 89 6 M21 Mn4Ni2CrMo (G89 6), 16834-A G 89 5 M21 Mn4Ni2,5CrMo (G89 5) and a filler wire 18276-A T 89 4 ZMn2NiCrMo M M21 1 H5 (T89). For evaluation light optical microscope pictures were used. Pixels containing cracks were manually segmented using a self-written program. Out of the segmented images data including crack length, position and area can be calculated for every crack. The results show dependencies of solidification cracking on the test parameters.
This presentation describes the usability of the hollow tensile specimen technique for in-situ material testing in a hydrogen atmosphere.
In addition, the presentation provides an outlook on the methodology for investigating the suitability of pipeline steels and their weld seams for hydrogen operation.
Diese Studie konzentriert sich auf den Einfluss der Bearbeitung auf die Eigenspannungen und den Verzug von WAAM-Proben. Definierte Proben wurden vollautomatisch mit einem speziellen WAAM-Massivdraht (Streckgrenze >820 MPa) mit unterschiedlichen geometrischen Designs geschweißt. Der Eigenspannungszustand vor und nach dem Abtrennen der AM-Struktur von der Substratplatte wurde mittels Röntgenbeugung an der Probenoberfläche analysiert und durch 3D-Verformungsanalysen mittels Photogrammetrie ergänzt. Die Ergebnisse zeigen einen signifikanten Einfluss der Geometrie auf die Relaxation und Umverteilung der Eigenspannungen.
Der Vortrag befasst sich mit der gezielten Einbringung zusätzlicher LTT-Lagen zur Erzeugung von Druckeigenspannungen in ermüdungskritischen Bereichen von konventionellen Schweißverbindungen. Dies ermöglicht eine wirtschaftliche Lösung, ohne die Integrität der Schweißverbindungen zu beeinträchtigen. Dazu wurden Längssteifen aus hochfestem Stahl in der ersten Lage mit konventionellem Schweißzusatzwerkstoff mittels Metall-Lichtbogenschweißen geschweißt. Anschließend wurde ein Chrom-Nickel-legierter LTT-Schweißzusatz auf die Stirnseiten der Steifen aufgebracht. Durch Variation der Schweißparameter konnten verschiedene Schweißnahtgeometrien des LTT-Zusatzwerkstoffs analysiert werden.
The weldability of stainless steels is largely controlled by the chemical composition, and alloys with ferritic or ferritic-austenitic solidification show the highest resistance to hot cracking. As the resulting phase balance also
affects the final properties, it may be beneficial to both foresee and measure the weld metal ferrite content. The WRC ’92 constitution diagram is currently the most accurate prediction tool available, but it does not take the cooling rate into consideration and the precision may be less accurate for stainless steels with high ferrite numbers (FN). This study aims to validate the reliability of the WRC ’92 diagram for weld metals with FN > 50. The chemical composition was altered through gas tungsten arc welding (GTAW) of UNS S32205 with ER347 filler wire that had been PVD-coated with either niobium (Nb), copper (Cu), nickel (Ni), manganese (Mn), carbon (C), or silicon (Si). The actual ferrite content was assessed using image analysis, FERITSCOPE® and X-ray diffraction (XRD). While the WRC ’92 diagram predictions were deemed accurate to acceptable for Ni, Si, and Mn, notable deviations were observed for Nb, Cu, and C. The FeriteScope exhibited a consistent trend with image analysis, though the values were higher, and scatter was wider, and the conversion factor is open for discussion. The lowest accuracy and largest spread were obtained using non-contact XRD, rendering it unsuitable for ferrite measurements of welds.
Effect of high-pressure hydrogen environment on the physical and mechanical properties of elastomers
(2024)
This study presents the influence of high-pressure hydrogen environment on the physical and mechanical properties of two types of cross-linked hydrogenated acrylonitrile butadiene rubbers. Based on the CSA/ANSI standard, static exposures in hydrogen experiments were performed up to 100 MPa at 120 °C. Characterization before and after exposure was conducted by means of density and hardness measurements, dynamic mechanical analysis (DMA), tensile tests, compression set, FT-IR and AFM analyses to assess effects after decompression. While the effect of high-pressure exposure is significant immediately after exposure, most of the physical and mechanical properties recover after 48 hours. FT-IR, AFM, SEM and compression set results indicate, however, permanent effects.
Controlled Thermal Severity (CTS) tests are known for applicatying high restraint intensity to fillet welds. Due to two different variations of the test it was possible to apply different amounts of restraint intensity to high-strength GMAW fillet welds at a high level of restraint. The results show the effect of heat input, filler material and restraint intensity on solidification cracking susceptibility.
Im Rahmen eines Kooperationsprojekts mit der Schottel GmbH wurde eine bauteilnahe Probengeometrie entwickelt, mit der sich unter Verwendung einer einachsigen Prüfmaschine das Spannungstiefenprofil in dem unter überlagerter Biege- und Zugspannung beanspruchtem Querschnitt im Schweißnahtübergang des Bauteils reproduzieren ließ.
Proben dieser Geometrie wurden vom Kooperationspartner im geschweißten bzw. geschweißten und spannungsarmgeglühten Zustand bereitgestellt. An der BAM wurden je Wärmebehandlungszustand mittels Senkerodieren zwei verschiedene künstliche Defektgeometrien im Schweißnahtübergang eingebracht.
Anhand der Proben wurden experimentell für alle vier Probenzustände Wöhlerlinien für ein Spannungsverhältnis von R = 0,1 ermittelt.
Zusätzlich wurde das u.a. an der BAM entwickelte IBESS-Verfahren angewandt, um die Wöhlerlinien analytisch zu bestimmen. Hierbei wurde eine sehr gute Übereinstimmung von Berechnung und Experiment erreicht, wobei die Berechnung zu einer leicht konservativen Lebensdauervorhersage führte.
Die Erzeugung rissschließfreier Anrisse in gekerbten bruchmechanischen Proben für anschließende Ermüdungsversuche kann durch eine zyklische Druckbelastung an der Kerbe erfolgen: Bei der Erstbelastung wird eine plastische Verformung an der Kerbspitze erzeugt, welche Zugeigenspannungen und damit eine risstreibende Kraft bei der folgenden zyklischen Druckbelastung hervorruft. Durch das Risswachstum kommt es zu einer Entspannung, bis der Riss schließlich arretiert, weil die effektive risstreibende Kraft auf den Schwellenwert abgesunken ist. Um Kurzrisswachstum in additiv, mittels pulverbettbasiertem Laserstrahlschmelzen (Laser Powder Bed Fusion - LPBF) gefertigtem AISI 316L Stahl und seinem konventionell erzeugten, warmgewalzten Pendant zu untersuchen, wurde dieses Verfahren im Rahmen der vorliegenden Arbeit genutzt. Im Falle des additiv gefertigten Materials kam es zu unerwartet langem Ermüdungsrisswachstum, bevor der Riss arretierte. Zur Ermittlung der Ursache erfolgte eine Messung der Eigenspannungsverteilungen mittels Neutronendiffraktion in der Kerbebene der additiv gefertigten Proben. Anschließend wurde ein Finite-Elemente-Modell zur Simulation des Ermüdungsrisswachstums in konventionellem und additiv gefertigtem Material implementiert. Im Rahmen dieses Vortrages wird insbesondere auf das Vorgehen bei der Simulation und auf die getroffenen Annahmen und Vereinfachungen eingegangen. Die Resultate werden mit den experimentellen Ergebnissen verglichen und das für die Simulation von Risswachstum genutzte Knoten-Freigabe-Verfahren (Node-Release), das Einbringen von Eigenspannungen als initiale Spannungen in der Simulation, und die Rechengrößen zur Quantifizierung der risstreibenden Kraft kritisch diskutiert.
The Varestraint test and its variant Transvarestraint are one of the most widely used techniques for evaluating a material solidification cracking sensitivity during welding. The result of such tests is a crack length which is proportional to the material’s cracking susceptibility. Nevertheless, the welding and load parameters can unintentionally influence the crack length, which in some cases can distort the material evaluation. An approach is described as to how these effects can be assessed with the aid of a digital crack analysis. The crack lengths are compared position-dependently with their possible propagation due to the weld pool movement during continuous loading. The index derived from this can be used by the operator to evaluate his test parameters. In addition, a comparison of the results of different Varestraint setups is made possible. Alongside experimental results, a numerical sensitivity analysis is presented on how individual welding and loading parameters can affect the crack lengths.
Multiple principal element alloys encompass the well-known high entropy alloys (HEA). The alloy system represents a new class of materials consisting of at least three alloying elements, each containing 5 to 35 at.%. Thus, this alloying concept differs fundamentally from conventional materials such as steel or nickel alloys. For this purpose, the alloying elements are specifically selected, the microstructures are adjusted in a single-phase and, in some cases, multi-phase manner. In particular, conflicting goals, such as the trade-off between strength and ductility in conventional steels, are overcome. However, in the last 20 years, the focus has been on material synthesis. With the increase in available material quantities, the focus is now on processing issues such as joining and welding processes. The weldability of HEAs has received very little attention so far. The experience with dissimilar metal welds is completely lacking but is essential for the application of these materials in combination with conventional materials. The present study presents comprehensive experimental results on the weldability of an equimolar CoCrFeMnNi-HEA in cold-rolled and heat-treated condition, which was joined by tungsten inert gas welding to an austenitic steel AISI 304. The mechanical properties of the dissimilar metal welds were characterized by cross-weld tensile samples, whereas the local deformation in the weld of the different welding zones was measured by digital image correlation. In accordance with the respective initial HEA condition (cold-rolled vs. heat-treated), the local strain behavior was divergent and influenced the global mechanical properties of both DMW types. Nonetheless, the experiments provided proof in principle of the weldability for dissimilar joints of the CoCrFeMnNi-HEA welded to conventional materials like austenitic stainless steels ensuring a corresponding capability for mechanical loading. This allows further considerations on the application of these innovative materials.
Numerical and experimental assessment of liquid metal embrittlement in externally loaded spot welds
(2024)
Zinc-based surface coatings are widely applied with high-strength steels in automotive industry. Some of these base materials show an increased brittle cracking risk during loading. It is necessary to examine electrogalvanized and uncoated samples of a high strength steel susceptible to liquid metal embrittlement during spot welding with applied external load. Therefore, a newly developed tensile test method with a simultaneously applied spot weld is conducted. A fully coupled 3D electrical, thermal, metallurgical and mechanical finite element model depicting the resistant spot welding process combined with the tensile test conducted is mandatory to correct geometric influences of the sample geometry and provides insights into the sample’s time dependent local loading. With increasing external loads, the morphology of the brittle cracks formed is affected more than the crack depth. The validated finite element model applies newly developed damage indicators to predict and explain the liquid metal embrittlement cracking onset and development as well as even ductile failure.
Hydrogen has great potential on the path towards decarbonization of the energy and transport sectors and can mitigate the urgent issue of global warming. It can be sustainably produced through water electrolysis with potentially zero emissions, and efficiently used (e.g., in fuel cell systems). Despite its environmental advantages, hydrogen-metal interactions could result in the degradation of the mechanical properties of several structural materials. In order to determine the magnitude of the material degradation in relation to hydrogen exposure, extensive material testing is required. The standardized procedure for in-situ testing for the quantification of the impact of compressed gaseous hydrogen (CGH2) relies on the utilization of an autoclave around the tested specimen. Such test set-up is complex, expensive, time-consuming and requires special equipment, trained personnel, and strict safety procedures. A relatively recent method to circumvent these issues and provide affordable results consists of using hollow specimens, thus applying the hydrogen pressure inside rather than outside the specimen. It allows to reduce the volume of hydrogen by several orders of magnitude and to perform the tests more efficiently and in a safer manner. This study focuses on evaluating the tensile properties of X65 vintage pipeline steel tested in a high-pressure hydrogen environment using hollow specimens. Tests are performed in 6 MPa H2 and Ar at the nominal strain rate of 10−6 s−1 to evaluate the reduced area at fracture and the elongation loss. The effect of surface finishing on crack initiation and propagation is investigated by comparing two different manufacturing techniques. In this way, this study provides insights into the applicability of a novel, reliable, and safe testing method which can be used to assess the hydrogen-assisted ductility loss in metallic materials.
The hydrogen economy is one of the main solutions for achieving climate neutrality in Europe. Metallic materials, predominantly steels, are the most common structural materials in the various components along the hydrogen supply chain. Ensuring their sustainable and safe use in hydrogen technologies is a key factor in the ramp-up of the hydrogen economy. This requires extensive materials qualification, however, most of the accepted, and standardised test methods for determining the influence of gaseous hydrogen on metallic materials describe complex and costly procedures that are only available to a very limited extent worldwide (e.g., autoclave technique).
The hollow specimen technique is presented as an alternative method that can overcome the limitations of current techniques and complement them. To standardise the technique, a process has been initiated by ISO in 2021. Knowledge gaps for tests with the technique in hydrogen have been identified by DIN. The H2HohlZug project, which falls under the umbrella of TransHyDE, aims to address the identified knowledge gaps and provide a foundation for a comprehensive standardisation of the hollow specimen technique.
In einem laufenden Kooperationsprojekt zwischen der BAM Berlin und der MPA Stuttgart wird das probabilistische Master Curve (MC) Konzept nach ASTM E1921 hinsichtlich seiner Übertragbarkeit auf ferritisches Gusseisen mit Kugelgraphit (DCI) untersucht.
Zielsetzung ist die Bereitstellung einer Vorgehensweise zur Bestimmung und Bewertung der dynamischen Bruchzähigkeit von DCI im Übergangsbereich. In diesem Beitrag wird der Versuchswerkstoff der Festigkeitsklasse GJS-400 näher vorgestellt.
Ferner werden erste Ergebnisse von zwei bruchmechanischen Versuchsserien an SE(B)140-Großproben bei Belastungsraten von ca. 6∙104 MPa√ms-1 bei -40 °C und -60 °C präsentiert.
Im laufenden Verbundprojekt MCGUSS untersuchen dieProjektpartner MPA Stuttgart und BAM Berlin das probabilistische Master Curve (MC) Konzept nach ASTM E1921 hinsichtlich seiner Übertragbarkeit auf ferritisches Gusseisen mit Kugelgraphit (DCI).
Ziel des Projektes ist die Entwicklung einer Methode zur Bestimmung und Bewertung der dynamischen Bruchzähigkeit von DCI im Übergangsbereich. In diesem Beitrag werden die Eigenschaften des verwendeten Werkstoffs der Festigkeitsklasse GJS-400 vorgestellt und die sich daraus ergebenden Probenentnahmestellen näher erläutert.
Weiterhin werden erste Ergebnisse der C(T)25-Versuchsserien vorgestellt, die bei Belastungsraten von ca. 5∙103 MPa√ms-1, 5∙104 MPa√ms-1 und 5∙105 MPa√ms-1 und einer Temperatur von -40 °C durchgeführt wurden.
As energy carrier of the future, green hydrogen can make a decisive contribution to a sustainable energy supply. Particularly important is the decarbonization of heavy industry. Therefore, a reliable supply of hydrogen must be guaranteed. A hydrogen pipeline grid can achieve this purpose. In Europe concrete plans for a hydrogen pipeline grid already exist, as the so called “European Hydrogen backbone”. As building a completely new pipeline grid is economically not justifiable, a dual-way strategy of repurposing natural gas (NG) pipelines and newly built pipelines is intended. Long distance pipeline grids require regular maintenance and repairs. For natural gas (NG) pipelines in-service welding is state of the art. Concepts such as hot-tapping (drilling into pressurized pipelines) and “stoppling” (sealing off pipeline sections after installing bypasses or pressure relieves) allow the repair of damaged pipeline sections or the installation of new branches without shutting the pipeline down, which in most cases isn’t possible from an economic standpoint. The EIGA 121/14 guideline already pointed out in 2014 that “a hydrogen hot-tap shall not be considered a routine procedure”. This shows that the determination of the transferability of these repair concepts to hydrogen pipelines is of utmost importance. Due to the degrading effects of hydrogen on mechanical proper-ties, commonly referred to as “hydrogen embrittlement” it is necessary to understand and investigate the occurring effects. In the special case of repair welding on in-service hydrogen pipelines an increased hydro-gen uptake due to a large heat input and microstructural changes in the material needs to be considered. Therefore, material degradation must be investigated to determine whether modifications of repair procedures are necessary to ensure a reliable and safe hydrogen transportation via pipelines. For this reason, this paper gives an overview on existing weld repair concepts and its risks and limitations in terms of hydrogen absorption and possible embrittlement effects when transferred to hydrogen pipelines. The complexity lies in a large variety of materials (low alloyed steels), pipeline diameters and corresponding welded joints. The material compatibility of materials in used (repurposed NG-pipelines) and new condition must be investigated. Particularly for repurposed/used pipelines the effect of a pre-matured/corroded inner surface and sometimes insufficient documentation of the material “history” needs to be considered. An overview on ongoing and completed R&D-projects with respect to repair concepts for hydrogen pipelines and hydrogen effects on pipeline materials is given. The focus hereby lies on possible methods of material testing and modeling. Its current difficulties, limits and possible solution will be discussed.
Contemporary steels creep-resistant steels like the 13CrMoV9-10 are used as thick plates e.g., for applications in hydrocrackers. The large plate thickness requires high efficiency welding processes like submerged arc welding (SAW) and a mandatory post weld heat treatment (PWHT). The PWHT-parameters stem from a combination of empirical knowledge and traditional experiments on free shrinking (FS) welds. In that connection, the formation of so-called stress-relief cracking (SRC) must be anticipated. The SRC susceptibility of a welded component is a complex combination and interaction of com-ponent specific, thermal, and metallurgical factors. Many of which have to date not been conclusively researched. For example, it is well known that SRCs develop during PWHT due to formation and growth of carbides on prior austenite grain boundaries, resulting in a significant hardness increase (secondary hardening) and toughness decrease. This leads to a high SRC susceptibility of the coarse grain heat-affected zone (CGHAZ) of the last weld bead during PWHT. This is intensified in case of high residual stresses from the component-specific, structurally induced stiffness. In combination with multi-layer welding this leads to a multiaxial stress distribution. Nonetheless, the combined effect of PWHT and high-residual stresses on the SRC formation is merely unknown. For that reason, this study presents the effect of different heating rates in conjunction with a certain component stiffness. For that reason, SAW joints of 13CrMoV9-10 steel were investigated under FS and defined external restraint condition.
A fundamental study of physical mechanisms of wineglass-shaped fusion zone profile in laser melting
(2024)
The fusion zone geometry in laser melting processes e.g., laser welding and laser-based additive manufacturing, of metallic materials has commonly a wineglass-shaped profile which is critical to the grain orientation and stress distribution. Hereby, we adopt for the first time a decoupling work through a combination of multi-physics modelling and experiments to reveal the fundamental mechanisms of this special morphology. Two physicsbased easy-to-use metal vapour models are proposed to consider the vapour’s momentum and thermal effects separately. It is found that the direct laser energy absorption and Marangoni shear stress which are widely hypothesised to dominate the wineglass-shape formation show only a minor influence. The additional heating from the metallic vapour plume rather than its momentum impact contributes predominantly to the enlarging of the molten pool top region, resulting directly in the formation of the wineglass-shaped fusion zone. The generality of the plume heating effect is also validated in two types of materials (steel and Al) in a wide range of parameters.
Microalloying elements such as Nb and Ti play a decisive function in achieving the desired mechanical strength of quenched and tempered, high-strength fine-grain structural steels with a nominal yield strength ≥ 690 MPa. The current specifications for the chemical composition only provide manufacturers with upper limits. However, even minor deviations in the alloy concept can have a significant impact on the mechanical properties. Consequently, accurate prediction of weldability and the integrity of welded joints becomes difficult or even impossible due to differences in composition and the resulting microstructures. Undesirable consequences include a possible softening of the heat-affected zone (HAZ) or, conversely, hardening effects. In view of these challenges, various microalloying strategies with different Ti and Nb contents are being systematically investigated for the first time using specially developed laboratory casting alloys. Each alloying route is based on the common S690QL, maintaining both the chemical composition and the heat treatment parameters. To analyse the weldability, three-layer welds were performed using gas metal arc welding (GMAW) and critical microstructures, such as areas of the heat-affected zone (HAZ) that exhibit significant softening or hardening, were identified. The effect of the softened HAZ region on failure was evaluated using transverse tensile specimens. Digital image correlation (DIC) is used to image changes in local strains in different HAZ regions in situ. Using a specially developed mirror system, the local strains of the microstructure zones on the top and bottom of the weld are recorded simultaneously. This makes it possible to analyse how the weld seam geometry (e.g., V-seam) influences the strain gradients. In addition, the analysis of the local deformation helps to understand the effects of the softened HAZ on the global strain, the fracture constriction, the fracture position, and the overall fracture behavior.
Joining and welding technologies are of high importance for the manufacturing of components and parts used in sustainable energy generation, conversion, and transport. In that connection, offshore and on-shore installed wind turbines are of high interest for the generation of electrical energy as well as photo-voltaic systems (solar cells). The electricity can be either directly transported or conversed via power-to-gas e.g., to hydrogen. In that scope, electrolyzer up to MW-range are of interest as well as the conver-sion back to electricity via fuel cells. In addition, hydrogen is a key element of the decarburization of in-dustries as well as the mobility sector encompassing sea, air and land transportation driven by hydrogen or its derivates. Well-known examples cover the direct reduction of iron ore to replace the conventional blast furnace process up to gas turbines or fuel cells for home-end use. All mentioned technologies re-quire reliable components, which are to a high extend dependent on joining and especially welding pro-cessing of materials. Especially, the (petro-) chemical industry has many years of experience with both materials used in hydrogen applications. The challenge is e.g., the transition to mass production of sys-tem components of electrolyzers/fuel cells and for distribution grids. At this point, the scalability of cur-rently applied joining processes often limits the economic efficiency, whereas especially laser welding or additive manufacturing will be of high interest. In that connection, it is very important to provide answers by joint research of universities, institutes, and industrial companies. Very often, solutions are already available and “just” have to be investigated and adapted for the new application, like repair welding of NG pipelines. For that reason, we want to set up a series of comprehensive papers with the aforementioned title. The idea is to get an in-depth but manageable overview of the importance of joining technologies in sustaina-ble energy generation, conversion, and transport encompassing current processes, limitations, and fur-ther perspectives. In that connection, the additive manufacturing is gaining more and more attention. If applicable, current challenges in the adaption or creation of new standards/regulations shall be addressed.
Die additive Fertigung mittels Schweißverfahren bietet große ökonomische Vorteile für eine ressourceneffiziente Bauteilherstellung. Offene Fragen bezüglich Homogenität, Anisotropie der Schweißgefüge und den damit verbundenen Bauteileigenschaften stehen einer wirtschaftlichen Verarbeitung oftmals im Wege. Finale Bauteilgeometrie und Oberflächengüte erfordern meist komplementäre subtraktive Fertigungsschritte. Werkstoffe für hochbelastbare Komponenten sind oftmals schwer spanbar. In einem Vorhaben der BAM und des ISAF wurde untersucht, wie die Modifikation der AM-Schweißzusätze und das ultraschallunterstützte Fräsen (US) die Zerspanungssituation verbessern. Der vorliegende Artikel stellt wesentliche Zusammenhänge zwischen Legierung, Gefüge und Zerspanung zweier schwer spanbarer Hochleistungslegierungen (FeNi und CoCr) dar. Großes Potenzial zeigte neben dem US die Modifikation mit Zr und Hf bei Zulegierung in das Schweißgut mittels Beschichtung von Massivdrähten bzw. Herstellung von Fülldrähten.
Mikrolegierungselemente wie Nb und Ti sind entscheidend für die erwünschte mechanische Festigkeit von vergüteten Feinkornbaustählen mit einer Nennstreckgrenze von ≥ 690 MPa. Aktuelle Spezifikationen geben lediglich Obergrenzen für die chemische Zusammensetzung vor, allerdings können geringfügige Abweichungen erhebliche Auswirkungen auf die mechanischen Eigenschaften haben. Die Vorhersage der Schweißbarkeit und Integrität von Schweißverbindungen stellt aufgrund der variierenden Zusammensetzung und Mikrostrukturen Herausforderungen dar. Unerwünschte Effekte wie Erweichung der Wärmeeinflusszone (WEZ) oder Verfestigung können auftreten. Um dies zu untersuchen, wurden verschiedene Mikrolegierungsrouten mit variierenden Ti- und Nb-Gehalten an Laborschmelzen erforscht. Die Basis jeder Route entsprach der üblichen S690QL in Zusammensetzung und Wärmebehandlung. Dreilagenschweißungen wurden mittels Metallaktivgasschweißens (MAG) durchgeführt, um kritische Gefügebereiche zu identifizieren. Die Analyse konzentrierte sich auf Phasenumwandlungen während der Abkühlung und metallurgisches Ausscheidungsverhalten. Die mechanischen Eigenschaften der Schweißnähte wurden durch Zugversuche ermittelt. Die Ergebnisse zeigen einen bedeutenden Einfluss der Mikrolegierungsroute und Schweißwärmezufuhr auf die Ausscheidungskinetik, trotz insgesamt guter Schweißbarkeit der Werkstoffe.
Beim Unterpulverschweißen sind die Prozessgeräusche ein Indikator für eine gute Fügequalität. Diese Beurteilung kann i.d.R. nur von einer erfahrenen Fachkraft durchgeführt werden. Eine kürzlich entwickelte künstliche Intelligenz kann automatisch das akustische Prozesssignal anhand vortrainierter Merkmale klassifizieren und die Fügequalität anhand des Geräuschs beurteilen. Der Algorithmus, einmal richtig trainiert, kann den Prüfaufwand beim Unterpulverschweißen deutlich reduzieren.
The ISO 3690 standard “Determination of hydrogen content in arc weld metal” requires a thermal activation of the diffusible hydrogen in a piece of weld metal for the subsequent ex situ concentration measurement by carrier gas hot extraction CGHE or thermal desorption spectroscopy (TCD). Laser-induced breakdown spectroscopy (LIBS) offers a time and spatially resolved, almost non-destructive, in situ measurement of hydrogen at surfaces without sample preparation. We measured hydrogen in steels, which were charged either electrochemically or by high-pressure hydrogen gas, and compared the results. Further, the feasibility of quantitative hydrogen line scan measurements with LIBS was demonstrated by measuring hydrogen at water jet cut surfaces. The hydrogen concentrations measured with the help of LIBS were compared with CGHE measurements. It was observed that hydrogen can be reliably measured with LIBS for concentrations larger than 2 wt.-ppm. The maximum hydrogen concentration achieved using electrochemical charging was 85.1 ppm. The results show that LIBS is a promising technique for time- and spatially resolved measurements of hydrogen in steels.
Within fracture mechanics safety assessment for steels in nuclear technology, the probabilistic master curve (MC) concept according to ASTM E1921 is currently used for quasi-static loading conditions as a supplement to the established deterministic ASME reference curve concept. However, for ductile cast iron (DCI), a systematic review of potential modifications to the assumptions and the procedure according to ASTM E1921 and an associated validation are still lacking. For this reason, the application of the fracture mechanics MC concept to ferritic ductile cast iron is being investigated in a joint research project between MPA Stuttgart and BAM Berlin. According to Hojo et al. (2008) the MC concept is already in use for the brittle fracture safety assessment of ferritic forged steel containers, which would suggest an extension to ductile cast iron containers. In compliance with IAEA SSG-26, the safety assessment of DCI containers for transport as well as storage of radioactive materials is based on the fracture mechanics criterion of general exclusion of crack initiation. Within this context, the focus of the current research project is on the further development of brittle fracture safety assessment methods. Therefore, a methodology shall be established to determine and assess dynamic fracture toughness values of DCI in the ductile-to-brittle transition regime, using only a low number of small fracture mechanics test specimens extracted from a component. For the experimental program, a DCI material of grade GJS-400 (GGG-40) has been produced as it is generally used for transport and storage containers for nuclear material. A basic mechanical-technological material characterization consisting of tensile, Charpy, and Pellini tests has been planned and a comprehensive fracture mechanics test program was compiled covering dynamic testing of DC(T)9, C(T)25, C(T)50, SE(B)10, SE(B)25, and SE(B)140 specimens at various loading rates and temperatures. The specimen testing is divided between the project partners based on specimen geometry. MPA Stuttgart has been tasked with the testing of the C(T), DC(T) and Pellini specimens, while BAM Berlin was assigned the SE(B), Charpy and tensile tests. These tests allow for the determination of the loading rate relevant for brittle fracture via C(T)25 specimens and an assessment of size effects by transferring the relevant loading rate to other specimen geometries and sizes. Numerical analyses of different specimen geometries and test setups are planned to investigate the influence of stress triaxiality and loading rate. Furthermore, the time-dependent course of the Weibull stress is assessed via these numerical analyses. Throughout the experimental program, the microstructure-property relationship will also be investigated based on quantitative metallographic and fractographic analyses like scanning electron microscope images and metallographic sections. With the acquired experimental database fundamental assumptions of the MC concept, like the weakest link model and the Weibull distribution, will be assessed for the application to DCI. In the end, the applicability of the MC concept will be evaluated and if necessary, modifications to the MC concept for DCI will be proposed. This paper will present the preliminary results of the GJS400 material characterization and the related selection of test specimen extraction points. First results of the C(T)25 and SE(B)140 specimen testing will also be discussed supported by first metallographic analyses.
High-strength steels offer potential for weight optimization due to reduced wall thicknesses in modern constructions. Additive manufacturing processes such as Wire Arc Additive Manufacturing (WAAM) enable the resource-efficient production of structures. In the case of defects occurring in weld seams orWAAM components due to unstable process conditions, the economical solution is local gouging or machining and repair welding. It is important to understand the effects of machining steps on the multiaxial stress state in conjunction with the design-related shrinkage restraints. Research into how welding and slot milling of welds andWAAM structures affects residual stresses is still lacking. For this reason, component-related investigations with high-strength steels with yield strengths ≥790 MPa are carried out in our research. In-situ digital image correlation (DIC) and ex-situ X-ray diffraction (XRD) were used to analyze the stresses and strains induced on specimens during and after milling. The systematic analyses revealed a significant interaction of the stiffness and microstructure of the specimens with the initial residual stresses induced by welding. Subsequent repair welds can result in significantly higher residual stresses.
Zur Umsetzung der wasserstoffbasierten Energiewende ist eine zuverlässige Transportinfrastruktur unverzichtbar. Hierfür ist die Nutzung großer Teile des vorhandenen Erdgasnetzes vorgesehen. Im Rahmen von Reparatur- und Wartungsarbeiten ist das Schweißen im Betrieb an Erdgaspipelines Stand der Technik. In Verbindung mit Wasserstoff wirft diese Technik jedoch Fragen der Materialverträglichkeit auf. Das im Vortrag vorgestellte Projekt H2SuD leistet Beiträge zur Aufklärung des Einflusses von Reparaturschweißprozessen auf die Wasserstoffaufnahme und Degradation im Betrieb befindlicher H2 Gasleitungen. Ein Schwerpunkt des Vortrages liegt auf der im Projekt erarbeiteten Prüfmethode für Modellversuche, mit denen der Einfluss von Schweißen im Betrieb an Pipelines auf die Wasserstoffaufnahme getestet wird. Die Durchführung erster Versuche und dabei erzielte Ergebnisse werden präsentiert.
Die Umstellung der Wirtschaft auf wasserstoffbasierte Energieversorgung soll in Deutschland vor allem auf Basis der Umstellung des bestehenden Erdgasnetzes erfolgen. Dabei sollen ca. 90 % dieser Fernleitungsnetze auf dem bestehenden Erdgasnetz basieren. Die Beimischung von Wasserstoff zum Erdgas als auch der reine Wasserstofftransport werfen jedoch die Frage auf, ob und wie kompatibel die eingesetzten Materialien sind. Die Reparatur- und Erweiterungsfähigkeit von Erdgas-Bestandspipelines ist zu klären, wenn diese auf Wasserstoff umgestellt werden. Denn gerade Gashochdruckleitungen müssen regelmäßig gewartet und erweitert werden, um einen ordnungsgemäßen Betrieb sicherzustellen. Insbesondere das Schweißen unter Betriebsdruck bzw. an in Betrieb befindlichen Gasleitungen ist eine der wichtigsten Instandhaltungstechnologien, unabhängig von der Zusammensetzung des geförderten Mediums. Es ist daher dringend notwendig, eine geeignete Teststrategie zu erarbeiten, welche die nötigen Vorrausetzungen für sicheres Schweißen an in Betrieb befindlichen Druckwasserstoffleitungen schafft und entsprechende Kriterien für die Praxis liefert. Im Projekt H2-SuD - Einfluss des Schweißens auf die Wasserstoffaufnahme und Degradation im Betrieb befindlicher H2-Ferngasleitungen - soll geklärt werden, ob und wie stark mit einer Eigenschaftsdegradation geschweißter Rohrstähle in Gasnetzen in Folge einer Wasserstoffaufnahme zu rechnen ist. Die Präsentation gibt dazu einen kurzen Überblick über den aktuellen Status des Projektes. Die Förderung erfolgt im Rahmen der DVGW-Innovationsprogammes Wasserstoff (Nr. G 202131).
Within fracture mechanics safety assessment for steels in nuclear technology, the probabilistic master curve (MC) concept according to ASTM E1921 is currently used for quasi-static loading conditions as a supplement to the established deterministic ASME reference curve concept. However, for ferritic ductile cast iron (DCI), a systematic review of potential modifications to the assumptions and the procedure according to ASTM E1921 and an associated validation are still lacking. For this reason, the application of the fracture mechanics MC concept to ferritic ductile cast iron is being investigated in a joint research project between MPA Stuttgart and BAM Berlin. According to IAEA SSG-26, the safety assessment of DCI containers for transport as well as storage of radioactive materials is based on the fracture mechanics criterion of general crack initiation exclusion. Within this context, the focus of the research project is on brittle fracture. The goal is the establishment of a methodology to determine and assess dynamic fracture toughness values of DCI in the ductile-to-brittle transition regime, using samples extracted from a component.
The experimental program uses a DCI material of grade GJS-400, which is generally used for transport and storage containers of radioactive materials. Firstly, a basic mechanical-technological material characterization will be performed consisting of tensile, Charpy and Pellini tests. Following the material characterization, the loading rate relevant for brittle fracture will be determined using instrumented C(T)25-fracture tests at a temperature of -40°C. To be able to transfer the relevant loading rate to other specimen geometries or sizes, the time-dependent course of the Weibull stress is assessed via numerical analyses. With this information an extensive experimental program consisting of DC(T)9, C(T)25, C(T)50, SE(B)10, SE(B)25 and SE(B)140 specimens is performed. These experimental results will be further supported by numerical and fractographic analyses. The empirical experimental database developed for DCI materials will be used to assess the applicability of the MC concept for DCI materials under dynamic loading.
At the current time manufacturing and precracking of test specimens is ongoing. The authors provide first results concerning the mechanical-technological material characterization, the relevant loading rate for brittle fracture determined via C(T)25 tests, and some early results of other specimen types. These experimental results are also supported by preliminary numerical and statistical analyses.
In einem laufenden Kooperationsprojekt zwischen der BAM Berlin und der MPA Stuttgart wird das probabilistische Master Curve (MC) Konzept nach ASTM E1921 hinsichtlich seiner Übertragbarkeit auf ferritisches Gusseisen mit Kugelgraphit (DCI) untersucht. Zielsetzung ist die Bereitstellung einer Vorgehensweise zur Bestim-mung und Bewertung der dynamischen Bruchzähigkeit von DCI im Übergangsbe-reich. In diesem Beitrag wird der Versuchswerkstoff der Festigkeitsklasse GJS-400 näher vorgestellt. Ferner werden erste Ergebnisse von zwei bruchmechanischen Versuchsserien an SE(B)140-Großproben bei Belastungsraten von ca. 6∙104 MPa√ms-1 bei -40 °C und 60 °C präsentiert.
Erstarrungsrisse bilden sich beim Schweißen hinter dem Schmelzbad. Im verwendeten MAG-Schweißverfahren wurden stark eingespannte Schweißungen mit verschiedenen hochfesten Schweißzusätzen durchgeführt. Alle verwendeten Zusätze weisen unter gewöhnlicher Einspannung keine Tendenz zur Erstarrungsrissbildung auf. In Abhängigkeit der verwendeten Schweißparameter und des Einspanngrades konnten Erstarrungsrisse in den Nähten festgestellt werden. Die Versuche zeigen, dass beim Schweißen hochfester und stark eingespannter Kehlnähte eine Kombination von hohen Wärmeeinträgen und Schweißgeschwindigkeiten zu erhöhter Bildung von Erstarrungsrissen führen kann.
Bruchmechanik-basierende Methoden können für die Ermüdungsbewertung von mechanischen Bauteilen angewendet werden, die Defekte oder Risse enthalten und zyklischen Belastungen ausgesetzt sind. Die Kenntnis des Risswachstumsverhaltens für kurze und lange Risse ermöglicht die Bestimmung sowohl endlicher als auch unendlicher Lebensdauer. Ein erstes Problem ergibt sich jedoch aus der empirischen Bestimmung von Ermüdungswerkstoffkennwerten, die je nach Prüfbedingungen, z. B. Prüfmethode, Frequenz und Spannungsverhältnis R, variieren. Dies ist auf die Rissschließeffekte und weitere Umgebungsphänomene zurückzuführen, die das Rissfortschrittsverhalten beeinflussen. Ein zweites Problem ist das Fehlen von Standardversuchsverfahren zur Bestimmung des Schwellenwerts gegen Ermüdungsrissausbreitung ΔKth in Abhängigkeit von der Rissausbreitung. Dies ist problematisch, da ΔKth mit der Zunahme der Rissschließeffekte im Kurzrissbereich zunimmt und seine ungenaue experimentelle Bestimmung zu großen Abweichungen bei der Bewertung und, was noch kritischer ist, zu nicht konservativen Vorhersagen führt. Mit dem Ziel, zuverlässigere und sicherere Bewertungsverfahren bereitzustellen, wird in dieser Arbeit eine Methode vorgeschlagen, die auf effektiven Risswachstumsdaten basiert, die bei hohen Spannungsverhältnissen (R ≈ 0,8) ermittelt wurden. Zur Beschreibung der Entwicklung der Rissschließeffekte wird ein Kurzrissmodell auf der Grundlage von zyklischen R-Kurven und CPLR-Daten verwendet. Die analytischen Vorhersagen werden mit experimentellen Daten verglichen, die zur Validierung des Verfahrens durchgeführt wurden, und die daraus entstandenen Unterschiede werden diskutiert.
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Low Transformation Temperature (LTT)-Schweißzusätze stellen einen innovativen Ansatz zur Erhöhung der Ermüdungsfestigkeit geschweißter Konstruktionen dar. LTT-Schweißzusätze zeichnen sich durch eine martensitische Phasenumwandlung nahe der Raumtemperatur aus, welche Druckeigenspannungen in der Schweißnaht und der Wärmeeinflusszone (WEZ) generieren.
Dieser Vortrag fokussiert sich auf die gezielte Einbringung zusätzlicher LTT-Lagen an ermüdungskritischen Stellen von konventionell geschweißten Verbindungen. Dies ermöglicht eine ökonomische Anwendung, ohne dass die Schweißnahtintegrität zu stark beeinflusst wird. Die Auswirkungen zusätzlicher LTT-Lagen wurden anhand geschweißter Längssteifen aus hochfestem Stahl hinsichtlich der chemischen Zusammensetzung und der Eigenspannungen untersucht. Unter Variation der Schweißgeschwindigkeit und Abstand zur konventionellen Naht konnten 3 unterschiedliche Nahtausführungen des Chrom-Nickellegierten LTT-Zusatzes bewertet werden.
Die chemische Zusammensetzung wurde mittels OES-Analysen untersucht. Dabei stellte heraus, dass die Aufmischung in allen Varianten sehr ähnlich war trotz teils unterschiedlicher LTT-Volumina. Härtebestimmungen ergaben in allen 3 Varianten eine ähnliche Härte. Daraus lässt sich annehmen, dass die Martensitstarttemperatur bei allen Nahtvarianten ähnlich ist.
Röntgenografische Eigenspannungsmessungen belegen, dass die Eigenspannungen am versa-genskritischen Nahtübergang bei Einsatz von LTT-Schweißzusätzen deutlich abgesenkt werden. Während die konventionelle Schweißnaht Zugeigenspannungen von ca. 350 MPa aufweist, können an den LTT-Nähten teilweise Druckeigenspannungen von bis zu -150 MPa nachgewiesen werden. Je höher der Abstand zur konventionellen Naht und je größer das eingebrachte LTT-Volumen ist, umso stärker sind die Eigenspannungsreduzierungen am Nahtübergang. Da in allen 3 Varianten eine ähnliche Martensitstarttemperatur angenommen werden kann, ist somit die Geometrische Komponente der LTT-Zusatzlage ein entscheidender Faktor für die Eigenspannungsreduzierung.
AbstractPowder Bed Fusion with Laser Beam of Metals (PBF-LB/M) has gained more industrial relevance and already demonstrated applications at a small series scale. However, its widespread adoption in various use cases faces challenges due to the absence of interfaces to established Manufacturing Execution Systems (MES) that support customers in the predominantly data-driven quality assurance. Current state-of-the-art PBF-LB/M machines utilize communication architectures, such as OPC Unified Architecture (OPC UA), Message Queuing Telemetry Transport (MQTT) and Representational State Transfer Application Programming Interface (REST API). In the context of the Reference Architecture Model Industry 4.0 (RAMI 4.0) and the Internet of Things (IoT), the assets, particularly the physical PBF-LB/M machines, already have an integration layer implemented to communicate data such as process states or sensor values. Missing is an MES component acting as a communication and information layer. To address this gap, the proposed Extract Transform Load (ETL) pipeline aims to extract relevant data from the fabrication of each build cycle down to the level of scan vectors and additionally to register process signals. The suggested data schema for archiving each build cycle adheres to all terms defined by ISO/TC 261—Additive Manufacturing (AM). In relation to the measurement frequency, all data are reorganized into entities, such as the AM machine, build cycle, part, layer, and scan vector. These scan vectors are stored in a runtime-independent format, including all metadata, to be valid and traceable. The resulting machine log represents a comprehensive documentation of each build cycle, enabling data-driven quality assurance at process level.
Residual stress formation during repeated gouging and repair welding cycles of high-strength steels
(2024)
The construction of foundation and erection structures for wind power plants requires the use of modern, sustainable and resource-efficient high-strength fine-grained structural steels. Weld defects due to the welding process are unacceptable. To overcome this issue, local thermal gouging followed by re-welding is a common and cost-effective method. The high shrinkage restraint of the gouge by the surrounding structure can cause crack initiation when design and re-weld induced residual stresses are superimposed. This risk is intensified by the progressive degradation of the microstructure and mechanical properties of high-strength steels during the weld repair process.
This investigation focuses on high-strength steels S500MLO for offshore applications and S960QL for mobile crane applications. The reduction and development of residual stresses caused by local thermal gouging and re-welding was investigated. Digital Image Correlated (DIC) stress-strain analysis was performed during preheating, welding and cooling. The results of the global DIC analysis and local longitudinal and transverse residual stresses of the weld determined by X-ray diffraction were found to be in good agreement. Furthermore, different stress levels were identified during gouging and welding. Repeated repair cycles led to an increase of longitudinal and transverse residual stresses in the weld metal as well as a hardness increase in the heat affected zone.
A steel pipeline segment of 2.5 m length was subjected to quasi-static four-point bending load in three steps for studying the initial cracking and damage accumulation based on the Acoustic Emission (AE) technique and by the direct current potential drop (DCPD) technique. For the latter, a new post-test analysis method was established.
AE is found more sensitive to crack initiation than DCPD. Formation of mesoscopic and macroscopic cracks as well as their closure and the resulting friction generate weighted peak frequencies below 400 kHz, whereas microscopic cracking produces AE with broad band spectra identifiable by weighted peak frequencies above 400 kHz. Critical states alike the maximum load level and the leak opening were accompanied by peak amplitudes above 85 dBAE. This rather fundamental study provides a data base for possibly developing advanced strategies of detection and alarm systems based on acoustic monitoring of pipelines, or at least, steel structures.
This work explores the feasibility of producing bead-on-plate welds of a CrCoNi medium entropy alloy and a CrMnFeCoNi high entropy alloy using electron beam welding. The alloys were welded in two states: one in an as-cold-rolled condition and the other in an annealed condition. In addition, the materials are welded with two different parameters. The FCC microstructure of the welds is investigated using scanning electron microscopy assisted by energy-dispersive X-ray spectroscopy and electron-backscattered diffraction. The impact of the weld on the microstructure is discussed. The heat-affected zone is negligible for the annealed condition of both medium and high entropy alloys since there is no driving force for recrystallisation and the exposure time to high temperature is insufficient for grain coarsening. The texture formed in the fusion zone is also discussed and compared to the texture in the base metal and the heat-affected zone. Although the grain growth along the (100) crystallographic direction is preferential in all cases, the crystallographic texture type differs from each weld. Higher hardness values are measured in the medium entropy alloy’s base metal and fusion zone than in the high entropy alloy.
Wasserstoff erfüllt die zentrale Rolle für die Umwandlung der bisherigen fossil-basierten Energieerzeugung und -nutzung auf eine dekarbonisierte, nachhaltige Form. Dazu muss der Wasserstoff erzeugt, gespeichert, transportiert werden, bevor er wieder der Nutzung zugeführt wird. Hierzu sind entlang der gesamtem Prozesskette Wasserstofftechnologien notwendig, die einen sicheren Betrieb erfordern. Hierbei kommt dem schweißtechnischen Anlagen- und Behälterbau wesentliche Bedeutung zu, insbesondere (aber nicht ausschließlich) für Speicherung und Transport des Wasserstoffes. Der vorliegende Beitrag gibt einen kurzen Überblick, wo und wie die konventionelle Schweißtechnik hierzu wichtige Beiträge leistet. Die additive Fertigung, also das „Drucken“ von Bauteilen wird dabei zunehmend wichtiger, entlang der gesamtem Prozesskette der Wasserstofftechnologien. Gleichwohl darf nicht unterschätzt werden, dass auch wesentlicher Bedarf an der Erweiterung und teilweiser Neufassung von bestehenden Regel- und Normenwerken besteht.
Wasserstoff erfüllt die zentrale Rolle für die Umwandlung der bisherigen fossil-basierten Energieerzeugung und -nutzung auf eine dekarbonisierte, nachhaltige Form. Dazu muss der Wasserstoff erzeugt, gespeichert, transportiert werden, bevor er wieder der Nutzung zugeführt wird. Hierzu sind entlang der gesamtem Prozesskette Wasserstofftechnologien notwendig, die einen sicheren Betrieb erfordern. Hierbei kommt dem schweißtechnischen Anlagen- und Behälterbau wesentliche Bedeutung zu, insbesondere (aber nicht ausschließlich) für Speicherung und Transport des Wasserstoffes. Der vorliegende Beitrag gibt einen kurzen Überblick, wo und wie die konventionelle Schweißtechnik hierzu wichtige Beiträge leistet. Die additive Fertigung, also das „Drucken“ von Bauteilen wird dabei zunehmend wichtiger, entlang der gesamtem Prozesskette der Wasserstofftechnologien. Gleichwohl darf nicht unterschätzt werden, dass auch wesentlicher Bedarf an der Erweiterung und teilweiser Neufassung von bestehenden Regel- und Normenwerken besteht.
Die Kombination aus hoher Korrosionsbeständigkeit und guten mechanischen Eigenschaften von Duplexstählen (DSS) ist auf ihre chemische Zusammensetzung und das ausgewogene Phasenverhältnis von Ferrit (α) und Austenit (γ) zurückzuführen.
Viele industrielle Anwendungen erfordern eine stoffschlüssige Verbindung von DSS. Das Wolfram-Inertgas-Schweißen (WIG) ist relativ einfach zu handhaben, benötigt nur wenig Platz und ermöglicht ein automatisiertes Schweißen, mit sehr hoher Reproduzierbarkeit und ist daher hervorragend zum Schweißen von DSS.
Während der Erstarrung dieser Dualphasenstähle kann es zu kritischen Phasenverhältnissen von α und γ kommen, was zu Erstarrungsrissen, Korrosionsanfälligkeit, geringerer Duktilität und kritischen Festigkeitswerten führt. Um die gewünschten Werkstoffeigenschaften zu erhalten, muss daher die α/γ-Verteilung zuverlässig vorhergesagt werden. Dies geschieht in der Regel mit Hilfe des WRC1992-Diagramms. Die Vorhersagegenauigkeit des Ferritgehalts in diesem Diagramm ist jedoch meist nicht genau genug und muss daher optimiert werden. Daher ist es notwendig, selbst kleinste Veränderungen in der chemischen Zusammensetzung des Schweißguts idealerweise während des Schweißens zu überwachen. Dies wird in diesen Experimenten mit Hilfe der laser-induzierten Plasmaspektroskopie (LIBS) durchgeführt. Ein großer Vorteil dieser Technik ist die hochgenaue zeit- und ortsaufgelöste Messung der chemischen Zusammensetzung während des Schweißens. In vorherigen Arbeiten wurde bereits die chemische Zusammensetzung im Schweißgut und der WEZ quantifiziert. In der präsentierten Untersuchung wird der Einfluss einzelner Elemente, wie Nb und Cu, auf das resultierende Schweißmikrogefüge untersucht.
The combination of high corrosion resistance and good mechanical properties of duplex steels (DSS) is due to their chemical composition and the balanced phase ratio of ferrite (α) and austenite (γ).
Many industrial applications require a material joint of DSS. Tungsten inert gas (TIG) welding is relatively easy to use, requires little space and allows automated welding, with very high reproducibility and is therefore excellent for welding DSS.
During solidification of these steels, critical phase ratios of α and γ can occur, leading to solidification cracking, susceptibility to corrosion, lower ductility, and critical strength values. Therefore, to obtain the desired material properties, the α/γ distribution must be reliably predicted. This is usually done using the WRC1992 diagram. However, the prediction accuracy of the ferrite content in this diagram is usually not accurate enough and must therefore be optimized. It is therefore necessary to monitor even the smallest changes in the chemical composition of the weld metal, ideally during welding. This is done in these experiments using Laser-induced Breakdown Spectroscopy (LIBS). A major advantage of this technique is the highly accurate time- and spatially-resolved measurement of chemical composition during welding. Previous work has quantified the chemical composition in the weld metal and heat affected zone. In the presented study, the influence of individual elements, such as Nb and Cu, on the resulting weld microstructure is investigated.
Die Wasserstoffinfrastruktur ist eine zentraler Bestandteil der erfolgreichen Umsetzung der wasserstoffbasierten Energiewende. Dabei bilden Ferngasleitungen quasi das "Rückgrat" der Transportinfrastruktur großer Gasmengen. Dabei müssen unter Umständen Reparaturen an den Pipelines durchgeführt werden. Dabei ist in der Erdgasinfrastruktur das Schweißen an in Betrieb befindlichen (d.h. von Gas durchflossenen) Pipelines Stand der Technik. Es ist jedoch vollkommen offen, inwieweit diese Technik auf die reine Wasserstoffpipelines übertragbar sind. Hierzu leistet das Projekt H2SuD wichtige Beiträge zur Aufklärung des Einfluss eines Reparaturschweißprozesses auf die Wasserstoffaufnahme und Degradation im Betrieb befindlicher H2 Gasleitungen.
Large scale hydrogen assisted cracking test for thick walled SAW joints for offshore applications
(2023)
Offshore wind turbines continuously increase in size and weight and demand adequate offshore foundations concepts like monopiles, tripods or jackets. These components are typically submerged arc welded (SAW) high-strength thick steel plates like the S420ML. During welding, the occurrence of delayed hydrogen assisted cracking (HAC) must be anticipated. HAC is a critical combination of the local hydrogen concentration within a susceptible microstructure under certain mechanical load, i.e., the occurring (welding) residual stresses. The welding sequence of the thick-walled plates complicate the residual stress distribution due to the necessary repeated thermal cycling, i.e., welding seam / layer deposition to fill the joint. For that purpose, SAW with two-wire-technique was used to weld a specially designed and prototype-like mock-up of a real component with a thickness of 50 mm, filled more than 20 passes and a seam length of 1,000 mm. Additional welded stiffeners simulated the effect of a high restraint, to stimulate critical HAC conditions. The necessity of a minimum waiting time (MWT) before the NDT can be conducted (to exclude HAC) was critically verified by the application of ultrasonic testing of the welded joint at different time-steps of the NDT of 48 h after welding. The residual stresses were determined by a robot XRD goniometer. Tensile residual stresses up to the yield limit are found both in the weld metal and in the heat-affected zone. Numerical modelling allowed the qualitative estimation of the hydrogen diffusion in the weld. A remarkable HAC occurrence was not identified and proves both, a certain resistance of the weld joint to HAC and the (questionable) duration of the MWT.
This presentation summarizes the latest results on the microalloying influence on the preciptitation behavior on the mechanical properties of welded high-strength steel with a design yield strength of 690 MPa and above. For that reason, Charpy tests were performed for the pure weld metal and different heat-affected zones. Thermodynamic phase field modeling showed the usefulness of calculations in Thermocalc to predict the preciptiation behavior and (finally) to conclude the mechanistic behavior of the welded joint.
High entropy alloys (HEA) are a new class of materials that have been investigated since the early 2000s and offer great potential to replace conventional alloys. However, since they sometimes have significant contents of expensive alloying elements such as Co or Ni, their use is only conceivable in highly stressed areas of components. For this purpose, the weldability with conventional alloys such as high-alloy austenitic steels must be investigated. In addition to the resulting microstructure, the mechanical properties are also fundamental for the usability of HEAs in DMWs. For this purpose, TIG welds of CoCrFeMnNi HEA (cold rolled and recrystallized state) with AISI 304 austenitic steel are investigated. These mechanical properties are analyzed in this work by means of tensile tests and local hardness measurement. The local strain behavior of the welded joints is also characterized by means of Digital Image Correlation (DIC). The results of the local hardness measurement show a clear influence of the initial condition of the HEA on the HAZ. Thus, the HEA in the cold-rolled condition shows a clear softening because of recrystallization processes in the HAZ. On the other hand, there is no influence on the hardness of the weld metal, which is approx. 200 HV0.1 in both cases. The tensile tests show a consistent failure of the weld in the weld metal. However, regardless of the HEA condition, strengths in the range of the recrystallized HEA (RM ~ 550–600 MPa) are achieved, although with significantly reduced fracture elongations.
Die schädigende Wirkung von Wasserstoff auf die mechanischen Eigenschaften von Stählen ist zwar bekannt, aber noch immer nicht ausreichend erforscht. Die schnelle und sichere Markteinführung von Wasserstofftechnologien macht es erforderlich, dieses Thema genauer zu untersuchen. Im Allgemeinen wird dies oft als Wasserstoffversprödung bezeichnet. Daher ist es wünschenswert, eine Prüfmethode zu entwickeln, die auf einfache Weise die Materialeigenschaften unter Wasserstoffatmosphäre ermitteln kann. Derzeit werden mechanische Prüfungen unter Wasserstoffatmosphäre in Autoklaven durchgeführt. Für diese Technik ist eine aufwendige Hardware erforderlich, daher sind die Prüfungen teuer und die Prüfkapazitäten nur in geringem Umfang verfügbar. Die hier vorgestellte Prüfmethode verspricht einen zukunftsweisenden Ansatz zur Reduzierung von Kosten und Bearbeitungszeiten durch die Verwendung von Hohlkörpern, d.h. die Probe selbst stellt den Autoklav dar.
Die Wasserstoffinfrastruktur ist eine zentraler Bestandteil der erfolgreichen Umsetzung der wasserstoffbasierten Energiewende. Dabei bilden Ferngasleitungen quasi das "Rückgrat" der Transportinfrastruktur großer Gasmengen. Dabei müssen unter Umständen Reparaturen an den Pipelines durchgeführt werden. Dabei ist in der Erdgasinfrastruktur das Schweißen an in Betrieb befindlichen (d.h. von Gas durchflossenen) Pipelines Stand der Technik. Es ist jedoch vollkommen offen, inwieweit diese Technik auf die reine Wasserstoffpipelines übertragbar sind. Hierzu leistet das Projekt H2SuD wichtige Beiträge zur Aufklärung des Einfluss eines Reparaturschweißprozesses auf die Wasserstoffaufnahme und Degradation im Betrieb befindlicher H2 Gasleitungen.
Das DVS-Vorhaben 01.3211 „Herstellung beanspruchungsgerechter Oberflächen durch Kombination innovativer additiver und abtragender Fertigungsschritte an hochbelasteten Komponenten“ ist ein Kooperationsprojekt der Bundesanstalt für Materialforschung und -prüfung (BAM) und dem Institut für Schweißtechnik und Trennende Fertigungsverfahren (ISAF) der Technischen Universität Clausthal. Das Übergeordnete Projektziel ist das Erlangen von Erkenntnissen für eine sichere und wirtschaftliche, kombinierte additive und abtragende Fertigung aus kostenintensiven Werkstoffen hochbelasteter Komponenten insbesondere für KMU. Dabei stehe die beiden Werkstoffe CoCr26Ni9Mo5W (2.4681) und FeNi36 (1.3912) im Fokus. Mittels Modifikation der Schweißzusätze sind homogen und isotrop ausgeprägte Werkstoffeigenschaften und eine Erhöhung der Prozessstabilität und Fertigungsfreiheitsgrade bei der additiven Fertigung erzielbar. Darüber hinaus wird der Einfluss nachfolgender abtragender Bearbeitungsschritte des ultraschallunterstützen und des konventionellen Fräsprozesses untersucht. Die mit dem Forschungsvorhaben verbundenen Nutzen für KMU sind die Stärkung der Innovationsfähigkeit und der Wirtschaftlichkeit sowie die Erhöhung der Wettbewerbsfähigkeit. In AP-3 wurden die Mikrostruktur der MSG-Schweißung der CoCr-Referenzlegierung untersucht. In AP-4 wurden Zerspanversuche an der MSG-Schweißung der CoCr-Referenzlegierung durchgeführt.
Alloy 36 (1.3912), also known as “Invar,” is an alloy with 36% nickel. The alloy has a remarkably low thermal expansion coefficient in certain temperature ranges. This peculiarity is called the invar effect, which was discovered in 1896 by the Swiss physicist Charles Édouard Guillaume. Therefore, it is used in applications in which dimensional stability is critical, such as molding tools for composite materials in aerospace, automotive applications, or liquified natural gas (LNG) cargo tanks. Moreover, increasingly complex structures and the optimization of resource efficiency also require additive manufacturing steps for the production or repair of components. Additively manufactured components have a heterogeneous microstructure and anisotropic mechanical properties. In addition, the manufactured components require subsequent machining surface finishing, like finish milling, to achieve their final contour. Nickel iron alloys are difficult to machine. Additionally, inhomogeneous microstructure may lead to unstable cutting forces and conditions. In part I of this investigation, the initial alloy 36 is modified with the elements Ti, Zr, and Hf up to a maximum of 0.33 wt.-%. The influence of the modification elements on the microstructure as well as on the hardness of the AM components is examined. Furthermore, one modification is applied to metal arc welding process and investigated. Part II focuses on the effect of the alloy modifications on machinability as well as on the surface integrity of plasma-transferred-arc-welded (PTA) and finish milled invar components.
Einfluss der Schweiß- und Prüfparameter bei der Heißrissbewertung hochfester Schweißzusatzwerkstoffe
(2023)
Die Heißrissneigung beim Schweißen kann mittels einer ganzen Reihe von Prüfverfahren ermittelt werden. Eine etablierte Methode ist die sogenannte Varestraint-Prüfung, welche auch an der Bundesanstalt für Materialforschung und -prüfung (BAM) als modifizierter Varestraint/Transvarestraint-Test (MVT) zum Einsatz kommt. Die Ergebnisse von Varestraint-Prüfungen hängen jedoch stets in unterschiedlichem Maße von der individuellen Prüfmaschinenauslegung und den verwendeten Prüfparametern ab. Dies kann zu einer uneinheitlichen Bewertung des Rissverhaltens führen, wenn die Risslänge konventionell als Kriterium für die Rissneigung herangezogen wird. Scheinbare Abhängigkeiten von Prozessparametern erschweren dann die Interpretation der Ergebnisse. Eine neuartige Bewertungsmethodik entkoppelt den Maschineneinfluss vom Materialverhalten und verwendet die Dehnrate als Risskriterium in Analogie zu Prokhorovs Heißrissmodell. Die neue Auswertung wird anhand einer Studie hochfester Schweißzusatzwerkstoffe vorgestellt, deren Rissverhalten in Abhängigkeit der chemischen Zusammensetzung und der Schweißparameter bewertet wird.
Duplex stainless steels (DSS) are frequently used, especially in applications requiring high strength combined with high corrosion resistance in aggressive media. Examples include power plant components and maritime structures. During welding of these steels, local variations in chemical composition can occur. This results in ferritization of the material and negatively affects the mechanical properties of the components. In this work, tungsten inert gas (TIG) welding experiments were performed with DSS. Chemical composition analysis was realized in situ by using Laser Induced Breakdown Spectroscopy (LIBS). The aim of the work is to quantitatively measure the chemical composition in the weld seam of various DSS and to identify possible influences of welding parameters on the microstructure of the material. The chemical concentrations of the main alloying elements Cr, Ni, Mn on the surface of the sample during the welding process and the cooling process were measured. Mn and Ni are austenite stabilizers and their content increases during welding by using certain high alloyed filler material. Spectra were recorded every 1.3 s at a spacing of approximately 2 mm. During the cooling process the location of the measurement was not changed. The LIBS method is proofed to be suitable for the quantitative representation of the chemical compositions during the welding process.
It was found that there is a systematic dependence of the crack growth on the welding parameters as well as on the load. Decreasing welding speeds with simultaneously higher heat input promote crack formation with increasing strain rate.
Based on the results, a new crack criterion was finally selected which allows an extended assessment of the material behavior during the MVT-test. The threshold introduced can quantify the dependencies of the crack formation on the welding and testing parameters, which could not be comprehensively described with the conventional evaluation. In principle, the evaluation routine can also be transferred to other Varestraint or externally loaded hot cracking tests.
This presentation summarizes the latest research results of the influence of the post weld heat treatment (PWHT) rate and
the global mechanical stress conditions on the stress relief cracking (SRC) susceptibility of low-alloyed and creep-resistant CrMoV steel submerged arc weld joints. It was found that a certain effect of very low heating rates could be confirmed. In addition, the interlinking of SRC susceptibility increasing effects during the PWHT and the ex-post indentification in metallographic cross-section via microstructure characterization is very complex.
Since there is a continuously growing demand for complex, frequently heavy-sectioned spheroidal graphite cast iron (SGI) castings it is worth paying attention to the chunky graphite (CHG) degeneration which may occur under certain technological circumstances. Although a reference line for preventive actions in terms of general metallurgical and process measures could be drawn to avoid CHG in heavy-sectioned ferritic SGI castings, a broad majority of experts claim the avoidance of CHG in heavy sections cannot yet be rated a hundred percent process safe. A major reason may be seen in the fact that a universal, generally accepted explanation of CHG formation and growth has not yet been established, although several theories have been proposed. Nevertheless, metallurgical aspects are not in the focus of this paper.
This paper is about the current state of methods to detect CHG in SGI on the laboratory and component scales. Capabilities and limits of different metallographic, fractographic and non-destructive computer tomographic methods to recognize and quantify CHG are discussed. With respect to the characteristic fili-gree three-dimensional string-like, multi-branched CHG structure, which is non-isometric and non-dispersed, serious implications on the possibility to quantitatively characterize the amount of CHG must be considered.
In contrary to the metallurgical aspects, the knowledge about the impact of CHG on the materials and com-ponents properties is still surprisingly limited. Therefore, special emphasis of this paper is on the impact of CHG degeneration on the properties of ferritic SGI. Experimental results are reviewed to illustrate the effect of CHG on mechanical strength and ductility properties as well as fracture mechanics properties in terms of crack resistance and fracture toughness.
The present situation is characterized by discussions and uncertainty about the acceptance or rejection of SGI components containing CHG. Addressing this, conclusions from the materials engineering point of view are drawn for quality control, a safe operational strategy in the foundry and component safety.
Since there is a continuously growing demand for complex, frequently heavy-sectioned spheroidal graphite cast iron (SGI) castings it is worth paying attention to the chunky graphite (CHG) degeneration which may occur under certain technological circumstances. Although a reference line for preventive actions in terms of general metallurgical and process measures could be drawn to avoid CHG in heavy-sectioned ferritic SGI castings, a broad majority of experts claim the avoidance of CHG in heavy sections cannot yet be rated a hundred percent process safe. A major reason may be seen in the fact that a universal, generally accepted explanation of CHG formation and growth has not yet been established, although several theories have been proposed. Nevertheless, metallurgical aspects are not in the focus of this paper.
This paper is about the current state of methods to detect CHG in SGI on the laboratory and component scales. Capabilities and limits of different metallographic, fractographic and non-destructive computer tomographic methods to recognize and quantify CHG are discussed. With respect to the characteristic fili-gree three-dimensional string-like, multi-branched CHG structure, which is non-isometric and non-dispersed, serious implications on the possibility to quantitatively characterize the amount of CHG must be considered.
In contrary to the metallurgical aspects, the knowledge about the impact of CHG on the materials and com-ponents properties is still surprisingly limited. Therefore, special emphasis of this paper is on the impact of CHG degeneration on the properties of ferritic SGI. Experimental results are reviewed to illustrate the effect of CHG on mechanical strength and ductility properties as well as fracture mechanics properties in terms of crack resistance and fracture toughness.
The present situation is characterized by discussions and uncertainty about the acceptance or rejection of SGI components containing CHG. Addressing this, conclusions from the materials engineering point of view are drawn for quality control, a safe operational strategy in the foundry and component safety.
It is proposed to model the experimentally observed weld pool boundary with superellipses (Lamé curves) and to find the unknown parameters of the curves using optimization methods. It has been shown experimentally that during laser welding of austenitic stainless steel with a thickness of 2 mm at a speed of 20 mm/s, the rear weld pool part has a shape close to triangular which can be accurately approximated by a superellipse. Analytical dependences of the trajectory and growth rate of the crystal and its cross-sectional area on the geometry of the rear weld pool part are obtained.
Eight commercial austenitic stainless steels were tensile tested in reference atmosphere, in gaseous high-pressure hydrogen and in gaseous hydrogen precharged condition using conventional (CS) and tubular specimens (TS). For all configurations, 0.2 yield strength and ultimate tensile strength were comparable. In reference atmosphere, reduction of area of CS was higher compared to TS, whereas in gaseous high pressure hydrogen reduction of area of CS was lower compared to TS. In gaseous hydrogen precharged condition reduction of area of CS and TS were comparable for the severely affected grades. The differences in necking behavior between CS and TS are explained by different competitions between necking and hydrogen assisted crack initiation and growth especially for the tests in high pressure hydrogen gas.
Measurement of hydrogen concentration in steel using Laser-induced Breakdown spectroscopy (LIBS)
(2023)
Currently, the ISO 3690 standard requires a thermal activation of the diffusible hydrogen in weld metal for the subsequent ex situ concentration measurement by TDS. Laser-induced breakdown spectroscopy (LIBS) would offer a time and spatially resolved, almost non-destructive, measurement of hydrogen at surfaces. We could already show that this analysis technique allows for highly accurate in situ measurements of chemical compositions of e.g. Mn, Cr and Ni during welding e.g. in the melt pool, the weld metal or the heat affected zone. For quantitative LIBS measurements of hydrogen in steel, certified reference materials with different hydrogen concentrations were used for calibration.
There is a significant problem in welding steels: A critical combination of diffusible hydrogen, hardness microstructure and weld residual stresses can cause cold cracks to form in the weld microstructure. We investigated hydrogen in steels, which was loaded either electrochemically or with high-pressure hydrogen gas. Subsequently, various experiments were conducted to verify the feasibility of hydrogen measurements with LIBS. For example, depth profiles of hydrogen distribution could be obtained. Furthermore, samples were water jet cut and a line scan was made over the cross section to obtain a spatially resolved representation of the hydrogen. Total hydrogen concentrations were determined using carrier gas hot extraction. Our results show that LIBS is a promising technique for time and spatially resolved measurement of hydrogen in steels.
Duplexstähle besitzen ein zweiphasiges Gefüge und werden aufgrund ihrer verbesserten Schweißeignung gegenüber den Vollausteniten häufig im Anlagen- bzw. Apparatebau eingesetzt. Aufgrund der hohen Abkühlgeschwindigkeit und dem Abbrand von Legierungselementen kommt es zu einer Ferritisierung des Schweißguts und damit zu einer Degradation der mechanischen Eigenschaften. Zur Vorhersage des Phasenverhältnisses im Schweißgut wird das WRC1992-Diagramm genutzt. Dieses Diagramm zeigt einige Ungenauigkeiten und benötigt zur genaueren Vorhersage der Phasenverhältnisse eine Überarbeitung. Um den Einfluss einzelner Elemente auf das Schweißnahtmikrogefüge besser zu verstehen, wurden drahtförmige Schweißzusatzwerkstoffe mit dem Ferrit-Bildner Nb und dem Austenit-Bildner Cu beschichtet und für Schweißungen verwendet. Die Messmethode der Laser-induzierten Plasmaspektroskopie (LIBS) bietet hier eine gute Möglichkeit der in situ Überwachung der chemischen Konzentrationen, während des WIG-Schweißens von Duplexstählen. Die LIBS-Messergebnisse, konnten mit der Ferritnummer und der Schweißnahtmikrostruktur korreliert werden.
Einfluss der Schweiß- und Prüfparameter bei der Heißrissbewertung hochfester Schweißzusatzwerkstoffe
(2023)
Die Heißrissneigung beim Schweißen kann mittels einer ganzen Reihe von Prüfverfahren ermittelt werden. Eine etablierte Methode ist die sogenannte Varestraint-Prüfung, welche auch an der Bundesanstalt für Materialforschung und -prüfung (BAM) als modifizierter Varestraint/Transvarestraint-Test (MVT) zum Einsatz kommt. Die Ergebnisse von Varestraint-Prüfungen hängen jedoch stets in unter-schiedlichem Maße von der individuellen Prüfmaschinenauslegung und den verwendeten Prüfparametern ab. Dies kann zu einer uneinheitlichen Bewertung des Rissverhaltens führen, wenn die Risslänge konventionell als Kriterium für die Rissneigung herangezogen wird. Scheinbare Abhängigkeiten von Prozessparametern erschweren dann die Interpretation der Ergebnisse. Eine neuartige Bewertungsmethodik entkoppelt den Maschineneinfluss vom Materialverhalten und verwendet die Dehnrate als Risskriterium.
Das Schweißen von hochfesten Feinkornbaustählen erfordert aufgrund der Sicherstellung der Gütewerte des Grundwerkstoffes (Zähigkeit, Festigkeit) auch in der Schweißverbindung, die Einhaltung von engen Grenzen bei der Auswahl von Schweißparametern. Die Reproduzierbarkeit von beanspruchungsgerechten hochfesten Schweißverbindungen hängt vom Schweißverfahren und der damit einhergehenden komplexen Gefügeausbildung ab. Hierbei müssen hochfeste Schweißverbindungen mindestens die gleichen Festigkeitsanforderungen erfüllen wie der eingesetzte Grundwerkstoff. In diesem Vortrag werden speziell die Herausforderungen wie der Empfindlichkeit gegenüber der wasserstoffunterstützen Kaltrissbildung beim Schweißen von hochfesten Feinkornbaustählen und dem Mikrolegierungseinfluss auf die divergente Ausbildung der Wärmeeinflusszone thematisiert.
Mikrolegierungselemente, wie Nb und Ti, sind für die signifikante Festigkeitssteigerung von vergüteten, hochfesten Feinkornbaustählen mit einer Nominalstreckgrenze ≥ 690 MPa unerlässlich. Normvorgaben zur chemischen Zusam-mensetzung geben dabei nur obere Grenzwerte für die Hersteller vor. Weiterhin wirken sich bereits kleine Abwei-chungen in der Legierungsroute teilweise drastisch auf die mechanischen Eigenschaften aus. Somit wird eine adä-quate Vorhersage der Schweißeignung und der Integrität der Schweißverbindung aufgrund der variierenden Mikro-gefüge erschwert bis unmöglich. Unerwünschte Nebeneffekte sind die mögliche Erweichung der Wärmeeinflusszone (WEZ) als auch der gegenteilige Effekt der Aufhärtung.
Microalloying elements, such as Nb and Ti, are essential for significantly increasing the strength of quenched and tempered, high-strength structural steels with a nominal yield strength ≥ 690 MPa and their welded joints. The standard specifications (e.g., EN 10025-6) for the chemical composition are only tolerated limit contents within which the steel manufacturers operate. The standard composition, however, says nothing per se about the properties of the material. Even small deviations in the alloy route can have a drastic effect on the mechanical properties. This makes it difficult or even impossible to adequately predict the weldability and integrity of the welded joint. An undesirable side effect is the possible softening of the heat-affected zone (HAZ), as well as the opposite hardening.Mechanical-technological investigations of the notched impact strength confirm the results of the simulation regarding the development of different microalloy routes in the welded state. From this, the influence of the heat effect of welding on the microstructure formation in the HAZ and the corresponding mechanical properties can be described qualitatively.
For a significant increase in the strength of high-strength fine-grained structural steels with a nominal yield strength ≥690 MPa, the addition of microalloying elements such as Nb and Ti is required. The standard specifications for the chemical composition of these steels (e.g., in EN 10025-6) often only give the manufacturer limit contents to achieve the defined properties. The effect of the alloying elements in the heat affected zone (HAZ) is sometimes completely contrary.
This makes it difficult to adequately predict the batch dependency regarding weldability and the load-bearing behaviour of the welded joint. Three different micro-alloyed steels of the grade S690QL were produced on a laboratory scale, focusing on different Nb and Ti contents. To investigate the tempering effect, these were gas metal arc welded in three layers. In addition to metallographic investigations of individual HAZ areas, thermodynamic phase calculations were carried out using Thermo-Calc, following variations in the chemical composition. This provides an understanding of phase transformation, precipitation growth, and dissolution during welding as a function of temperature and cooling conditions. The results show
a divergent metallurgical behaviour in the HAZ of the three different micro-alloyed steels. Thereby, the Ti micro-alloyed grade showed a strong softening of the HAZ in contrast to the Nb micro-alloyed grade. This can be attributed to a contrary precipitation behaviour during welding.
In the course of tomorrow's hydrogen-based energy transition, the construction of the corresponding infrastructure will play a central role. In that context, large diameter long-distance transmission pipelines for hydrogen will be the backbone in the European Union with service pressures from 70 to 90 bar (e.g., de-pending on national regulations). It is a major goal to repurposing the existing natural gas (NG) infrastructure despite the necessity of new pipelines. From that point of view repair welding or further welding of branch pipe etc. can be necessary during in-service, i.e., permanent flow of pressurized hydrogen. The reason is that a shut-down of large diameter pipelines is not easy or sometimes merely impossible. At the moment, it is entirely open if current repair welding procedures for NG pipe-lines can be transferred to pure hydrogen pipelines. For that reason, a collaborative project between BAM, DVGW (German Association for Gas and Water Professions) and a large number of gas grid operators, pipeline manufacturers and construction companies was initiated in 2023 to answer questions on: (1) How many hydrogen is additionally absorbed during the preheating and maintaining at interpass temperature under remaining operational pressures? (2) Is the hydrogen concentration sufficient to reach a critical condition? (3)Which material and weld microstructure are the most susceptible? (4) Is there a difference in the repair welding behavior of NG pipelines with materials in “used” condition? (5) Which welding parameters and joint dimensions must be ensured for safe repair welding? The final aim of this project is the publication of a recommended practice for repair welding of in-service hydrogen pipelines. For that reason, the present study gives an overview on: (A) current practice in repair welding of in-service pipelines and (b) plans for hydrogen pipelines and first results of international research projects.
This contribution briefly summarizes the standardization activities in accordance with the "Nationale Roadmap Wasserstofftechnologien" and presents selected results on the activities in Germany with scope on hydrogen transport in pipelines. The talk was given during a panel discussion to set-up a steering committee for standardization for hydrogen pipelines and welding , coordinated by the International Institute of Welding.
The role of defects in the fatigue strength of Wire Arc Additively Manufactured (WAAMed) Ti-6Al-4V is analysed by means of the IBESS model, a fracture mechanics short crack growth approach based on the cyclic R-curve. Pores and crack-like defects are analysed. Estimations of the role of pore shape and size agree well with published fatigue data of WAAM Ti-6Al-4V with pores. The model is also used to explain the effect of fabrication defects on the scatter of experimental data. This demonstrates that short crack growth models represent a suitable engineering tool for the fatigue assessment of defective AM materials.
The application of anti-corrosion coated, high-strength steels in the automotive industry has increased in recent years. In combination with various zinc-based surface coatings, liquid metal embrittlement cracking can be observed in some of these materials. A high-quality, crack-free spot-welded joint is essential to realize the lightweight potential of the materials. In this work, the LME susceptibility of different coatings, which will be determined by the crack length and the occurrence rate, will be investigated using a welding under external load setup. The uncoated specimens did not show any LME. EG, GI and GA showed significantly less LME than ZM coatings. The latter coatings showed much larger crack lengths than the EG, GI and GA coatings. Furthermore, two mechanisms regarding the LME occurrence rate were observed: the occurrence of LME in zinc–magnesium coatings was theorized to be driven by the material properties of the coatings, whereas the occurrence of LME at EG, GI and GA samples was forced mainly by the application of the external tensile load.
In the experimental setup of this work, the materials were exposed to unusually high mechanical loads (up to 80% of their yield strength) to evoke LME cracks.
Mikrolegierungselementen, wie Nb und Ti sind für eine signifikante Festigkeitssteigerung von vergüteten, hochfesten Feinkornbaustählen mit einer Nominalstreckgren-ze ≥ 690 MPa unerlässlich. Normvorgaben zur chemischen Zusammensetzung dieser Stähle geben zur Erzielung der vorgeschriebenen Eigenschaften dabei oft nur Grenzgehalte für die Hersteller vor. Die Wirkung der Mikrolegierungselemente bzw. ihrer Karbide und/oder Nitride ist teilweise komplett konträr, insbesondere bei Auflösung und Wiederausscheidung in der WEZ bei identischem Schweißzusatz. Somit wird eine adäquate Vorhersage der Chargenabhängigkeit hinsichtlich der Schweißeignung und des Tragverhaltens der Schweißverbindung erschwert. Eine unerwünschte Eigenschaft ist dabei die Erweichung der WEZ, wie auch u.U. der gegenteilige Effekt der Aufhärtung.
Mikrolegierungselementen, wie Nb und Ti sind für eine signifikante Festigkeitssteigerung von vergüteten, hochfesten Feinkornbaustählen mit einer Nominalstreckgrenze ≥ 690 MPa unerlässlich. Normvorgaben zur chemischen Zusammensetzung dieser Stähle geben zur Erzielung der vorgeschriebenen Eigenschaften dabei oft nur Grenzgehalte für die Hersteller vor. Die Wirkung der Mikrolegierungselemente bzw. ihrer Karbide und/oder Nitride ist teilweise komplett konträr, insbesondere bei Auflösung und Wiederausscheidung in der WEZ bei identischem Schweißzusatz. Somit wird eine adäquate Vorhersage der Chargenabhängigkeit hinsichtlich der Schweißeignung und des Tragverhaltens der Schweißverbindung erschwert. Eine unerwünschte Eigenschaft ist dabei die Erweichung der WEZ, wie auch u.U. der gegenteilige Effekt der Aufhärtung.
Vor diesem Hintergrund werden im Rahmen eines DFG-Vorhabens systematisch Mikrolegierungs-routen mit variierenden Ti- und Nb-Gehalten des hochfesten und vergüteten Feinkornbaustahls S690QL untersucht. Dazu wird das MAG-Schweißen mit modifizierten Sprühlichtbogen verwendet, welches durch hohe Abschmelzleistung gekennzeichnet ist und schmalere Nahtöffnungswinkel (α = 30°) ermöglicht. An Dreilagen-Schweißungen wird der Effekt der metallurgischen Zusammensetzung in Kombination mit hoher Wärmeeinwirkung auf die Ausbildung einer kritischen WEZ-Gefügezone mit Erweichung und/oder exzessiver Aufhärtung untersucht. Ein besonderes Augenmerk wird auf die Phasenumwandlungen und das Ausscheidungsverhalten im Gefüge der Wärmeeinflusszone gelegt. Neben umfangreichen metallographischen Untersuchungen einzelner WEZ-Bereiche wurden, unter Variation der chemischen Zusammensetzung,
thermodynamische Phasenberechnungen mittels Thermo-Calc durchgeführt. Hierdurch wird ein Verständnis zur Phasentransformation und Ausscheidungswachstum und -auflösung während des Schweißens in Abhängigkeit von Temperatur und Abkühlbedingungen geschaffen. Das Ziel ist es, den Einfluss der Wärmeeinwirkung auf die Gefügeausbildung in der WEZ und dessen mechanischer Eigenschaften zu analysieren. Insbesondere wird hier auf die Auswirkung der unterschiedlichen Mikrolegierungskonzepte (Ti oder Nb) geachtet.
Mikrolegierungselemente, wie Nb und Ti, sind für die signifikante Festigkeitssteigerung von vergüteten, hochfesten Feinkornbaustählen mit einer Nominalstreckgrenze ≥ 690 MPa unerlässlich. Normvorgaben zur chemischen Zusammensetzung geben dabei nur obere Grenzwerte für die Hersteller vor. Weiterhin wirken sich bereits kleine Abweichungen in der Legierungsroute teilweise drastisch auf die mechanischen Eigenschaften aus. Mechanisch-technologische Untersuchungen zur Kerbschlagzähigkeit mittels Kerbschlagbiegeversuchen durchgeführt wurden, bestätigen dabei die Ergebnisse der thermodynamischen Simulation bezüglich des Ausscheidungsverhaltens während der Temperatur-Zeit Schweißzyklen. Daraus lässt sich der Einfluss der Wärmeeinwirkung beim Schweißen auf die Gefügeausbildung in der WEZ und der korrespondierenden mechanischen Eigenschaften qualitativ beschreiben.
The elastic properties (Young's modulus, shear modulus) of Ni-based alloy Inconel IN718 were investigated between room temperature and 800 °C in an additively manufactured variant (laser powder bed fusion, PBF‑LB/M) and from a conventional process route (hot rolled bar). The moduli were determined using the dynamic resonance method. The data set includes information on processing parameters, heat treatments, grain size, specimen dimensions and weight, Young’s and shear modulus as well as their measurement uncertainty.
The dataset was generated in an accredited testing lab using calibrated measuring equipment. The calibrations meet the requirements of the test procedure and are metrologically traceable. The dataset was audited as BAM reference data.