8 Zerstörungsfreie Prüfung
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Related work
Laboratory Study:
Combining Signal Features of Ground-Penetrating Radar to Classify Moisture Damage in Layered Building Floors
https://doi.org/10.3390/app11198820
On-Site Study:
TBA
Doctoral Thesis:
Non-destructive classification of moisture deterioration in layered building floors using ground penetrating radar
https://doi.org/10.14279/depositonce-19306
Measurement Parameters
The GPR measurements were carried out with the SIR 20 from GSSI and a 2 GHz antenna pair (bandwidth 1 GHz to 3 GHz) in common-offset configuration. Each B-Scan consists of N A-Scans, each including 512 samples of a 11 ns time window. Survey lines were recorded with 250 A-Scans/ meter, which equals a 4 mm spacing between each A-Scan No Gains were applied.
Folder Description:
Lab_dry, Lab_insulDamage, Lab_screedDamage
- each contain 168 Measurements (B-Scans) in .csv on 84 dry floors, floors with insulation damage and screed damage.
- each floor setup was measured twice on two orthogonal survey lines, indicated by _Line1_ and _Line2_ in the file name.
- the file names encode the building floor setup e.g. CT50XP100 describes a 50 mm cement screed with 100 mm extruded polystyrene below
- the material codes are
CT: cement screed, CA: anhydrite screed, EP: expanded polystyrene, XP: extruded polystyrene, GW: glass wool, PS: perlites
further information can be found in the publication https://doi.org/10.3390/app11198820
OnSite_
- 5 folders containing B-Scans on 5 different practical moisture damages
- the building floor setup is encoded according to the lab with an additional measurement point numbering at the start and a damage case annotation at the end of the file name with _dry, _insulationDamage and_screedDamage
File Description:
B-Scans, Measurement files - no header
- dimension: 512 x N data point with N beeing the number of A-Scans including 512 samples of a 11 ns time window.
- survey lines were recorded with 250 A-Scans/ meter, which equals a 4 mm spacing between each A-Scan
Moisture References
- Moist_Reference of On-Site Locations include the columns MeasPoint: Measurement point, wt%Screed: moisture content of screed layer in mass percent; wt%Insul: moisture content of insulation layer in mass percent. References were obtained by drilling cores with 68 mm diameter in the center of each survey line.
- Moist_Reference_Screed of Lab data include the columns Screed: Screed material and thickness in mm, wt%Screed moisture content of screed layer in mass percent
- Moist Reference_Insul of Lab data include the columns Insulation: Insulation material and thickness in mm, water addition in l: water added to the insulation layer in liters, V%Insulation: water added to the insulation layer in volume percent, RH%: resulting relative humidy in the insulation layer during measurement. These References are only avaible for Lab measurements on insulation damages.
To evaluate the durability of new alternative cement compositions, it is important to examine the internal transport of moisture through these materials. For this purpose, mortars were prepared from different types of cement and capillary suction experiments were carried out. The moisture transport was studied with an NMR tomograph and compared with weight measurements. With the tomograph, the total moisture input could be determined, as well as the moisture content within the samples non-destructively and spatially resolved. This allows precise observation of the moisture fronts. The tomograph was also used to determine the capillary transport coefficient.
LIBS‐ConSort: Development of a sensor‐based sorting method for construction and demolition waste
(2023)
AbstractA joint project of partners from industry and research institutions approaches the challenge of construction and demolition waste (CDW) sorting by investigating and testing the combination of laser‐induced breakdown spectroscopy (LIBS) with near‐infrared (NIR) spectroscopy and visual imaging. Joint processing of information (data fusion) is expected to significantly improve the sorting quality of various materials like concrete, main masonry building materials, organic components, etc., and may enable the detection and separation of impurities such as SO3‐cotaining building materials (gypsum, aerated concrete, etc.)Focusing on Berlin as an example, the entire value chain will be analyzed to minimize economic / technological barriers and obstacles at the cluster level and to sustainably increase recovery and recycling rates.The objective of this paper is to present current progress and results of the test stand development combining LIBS with NIR spectroscopy and visual imaging. In the future, this laboratory prototype will serve as a fully automated measurement setup to allow real‐time classification of CDW on a conveyor belt.
In recent decades, the number of components in concrete has grown, particularly in formulations aimed at reducing carbon footprints. Innovations include diverse binders, supplementary cementitious materials, activators, concrete admixtures, and recycled aggregates. These developments target not only the enhancement of material properties but also the mitigation of the ecological and economic impacts of concrete — the most extensively used material by humankind. However, these advancements also introduce a greater variability in the composition of raw materials. The material’s behavior is significantly influenced by its nanoscale properties, which can pose challenges in accurate characterization. Consequently, there’s an increasing need for experimental tuning of formulations. This is accompanied by a more inconsistent composition of raw materials, which makes an experimental tuning of formulations more and more necessary. However, the increased complexity in composition presents a challenge in finding the ideal formulation through trial and error. Inverse design (ID) techniques offer a solution to this challenge by allowing for a comprehensive search of the entire design space to create new and improved concrete formulations. In this publication, we introduce the concept of ID and demonstrate how our open-source app “SLAMD” provides all necessary steps of the workflow to adapt it in the laboratory, lowering the application barriers. The intelligent screening process, guided by a predictive model, leads to a more efficient and effective data-driven material design process resulting in reduced carbon footprint and improved material quality while considering socio-economic factors in the materials design.
Large-language models (LLMs) such as GPT-4 caught the interest of many scientists. Recent studies suggested that these models could be useful in chemistry and materials science. To explore these possibilities, we organized a hackathon. This article chronicles the projects built as part of this hackathon. Participants employed LLMs for various applications, including predicting properties of molecules and materials, designing novel interfaces for tools, extracting knowledge from unstructured data, and developing new educational applications. The diverse topics and the fact that working prototypes could be generated in less than two days highlight that LLMs will profoundly impact the future of our fields. The rich collection of ideas and projects also indicates that the applications of LLMs are not limited to materials science and chemistry but offer potential benefits to a wide range of scientific disciplines.
In this paper, we demonstrate the value of 1H NMR relaxometry for studying the hydration of clinker-reduced, more climate-friendly cementitious binders. The results were obtained on typical CEM I cements and sister samples containing two different reactive agricultural ashes as well as non-reactive biochars as supplementary cementitious materials. The findings prove that time-resolved NMR measurements provide valuable additional information when combined with classical heat flow calorimetry.
In this paper, we demonstrate the value of 1H NMR
relaxometry for studying the hydration of clinker-reduced, more
climate-friendly cementitious binders. The results were obtained
on typical CEM I cements and samples containing two different
reactive agricultural ashes as well as non-reactive biochars as
supplementary cementitious materials. The findings prove that
time-resolved NMR measurements provide valuable additional
information when combined with classical heat flow calorimetry.
This paper presents a novel approach for developing sustainable building materials through Sequential Learning. Data sets with a total of 1367 formulations of different types of alkali-activated building materials, including fly ash and blast furnace slag-based concrete and their respective compressive strength and CO2-footprint, were compiled from the literature to develop and evaluate this approach. Utilizing this data, a comprehensive computational study was undertaken to evaluate the efficacy of the proposed material design methodologies, simulating laboratory conditions reflective of real-world scenarios. The results indicate a significant reduction in development time and lower research costs enabled through predictions with machine learning. This work challenges common practices in data-driven materials development for building materials. Our results show, training data required for data-driven design may be much less than commonly suggested. Further, it is more important to establish a practical design framework than to choose more accurate models. This approach can be immediately implemented into practical applications and can be translated into significant advances in sustainable building materials development.
Capillary active interior insulation materials are an important approach to minimize energy losses of historical buildings. A key factor for their performance is a high liquid conductivity, which enables redistribution of liquid moisture within the material. We set up an experiment to investigate the development of moisture profiles within two different interior insulation materials, calcium-silicate (CaSi) and expanded perlite (EP), under constant boundary conditions. The moisture profiles were determined by two different methods: simple destructive sample slicing with subsequent thermogravimetric drying as well as non-destructive NMR measurements with high spatial resolution. The moisture profiles obtained from both methods show good agreement, when compared at the low spatial resolution of sample slicing, which demonstrates the reliability of this method. Moreover, the measured T2-relaxation-time distributions across the sample depth were measured, which may give further insight into the saturation degree of the different pore sizes. In order to explain differences in the moisture profiles between CaSi and EP, we determined their pore-size distribution with different methods: conversion of the NMR T2 relaxationtime distribution at full saturation, mercury intrusion porosimetry and indirect determination from pressure plate measurements. CaSi shows a unimodal distribution at small pore diameters, while in EP, a bi-modal or wider distribution was found. We assume that the smaller pore diameters of CaSi lead to a higher capillary conductivity, which causes a more distributed moisture profile in comparison with that of EP.
Der Vortrag gibt eine Übersicht über aktuelle zerstörungsfreie Prüfmethoden, die verwendet werden können, um eine Zustandsbewertung von Bauteilen im Bestand vorzunehmen und mögliche Wiederverwendungsstrategien zu entwickeln. Ebenfalls zeigt der Vortrag, welche Möglichkeiten es gibt, künstliche Intelligenzmethoden zu verwenden, um aus recykelten Materialien wieder hochwertige, neue Baustoffe zu entwickeln.