5 Werkstofftechnik
Filtern
Dokumenttyp
- Vortrag (432)
Sprache
- Englisch (333)
- Deutsch (96)
- Mehrsprachig (3)
Referierte Publikation
- nein (432) (entfernen)
Schlagworte
- Additive Manufacturing (38)
- Additive manufacturing (24)
- Microstructure (21)
- Corrosion (20)
- Glass (18)
- Ontology (17)
- Fatigue (13)
- Ceramics (12)
- LCF (11)
- 316L (10)
Organisationseinheit der BAM
- 5 Werkstofftechnik (432)
- 5.2 Metallische Hochtemperaturwerkstoffe (116)
- 5.1 Mikrostruktur Design und Degradation (112)
- 5.4 Multimateriale Fertigungsprozesse (101)
- 5.3 Polymere Verbundwerkstoffe (52)
- 5.6 Glas (51)
- 8 Zerstörungsfreie Prüfung (46)
- 5.5 Materialmodellierung (45)
- 9 Komponentensicherheit (44)
- 8.5 Röntgenbildgebung (35)
- 7 Bauwerkssicherheit (33)
- 5.0 Abteilungsleitung und andere (23)
- 9.4 Integrität von Schweißverbindungen (19)
- 7.6 Korrosion und Korrosionsschutz (18)
- 6 Materialchemie (15)
- 9.6 Additive Fertigung metallischer Komponenten (13)
- 7.5 Technische Eigenschaften von Polymerwerkstoffen (10)
- 9.0 Abteilungsleitung und andere (9)
- 9.3 Schweißtechnische Fertigungsverfahren (9)
- 6.3 Strukturanalytik (8)
- 1 Analytische Chemie; Referenzmaterialien (7)
- 4 Material und Umwelt (7)
- 8.0 Abteilungsleitung und andere (7)
- 8.4 Akustische und elektromagnetische Verfahren (7)
- 3 Gefahrgutumschließungen; Energiespeicher (6)
- 6.1 Oberflächen- und Dünnschichtanalyse (5)
- 4.2 Material-Mikrobiom Wechselwirkungen (4)
- 8.6 Faseroptische Sensorik (4)
- 1.2 Biophotonik (3)
- 3.0 Abteilungsleitung und andere (3)
- 8.1 Sensorik, mess- und prüftechnische Verfahren (3)
- 9.2 Versuchsanlagen und Prüftechnik (3)
- VP Vizepräsident (3)
- VP.1 eScience (3)
- 1.9 Chemische und optische Sensorik (2)
- 3.1 Sicherheit von Gefahrgutverpackungen und Batterien (2)
- 4.1 Biologische Materialschädigung und Referenzorganismen (2)
- 6.6 Physik und chemische Analytik der Polymere (2)
- 7.0 Abteilungsleitung und andere (2)
- 7.4 Baustofftechnologie (2)
- 7.7 Modellierung und Simulation (2)
- 1.4 Prozessanalytik (1)
- 1.6 Anorganische Referenzmaterialien (1)
- 2 Prozess- und Anlagensicherheit (1)
- 2.1 Sicherheit von Energieträgern (1)
- 3.5 Sicherheit von Gasspeichern (1)
- 4.4 Thermochemische Reststoffbehandlung und Wertstoffrückgewinnung (1)
- 6.0 Abteilungsleitung und andere (1)
- 6.2 Material- und Oberflächentechnologien (1)
- 6.4 Materialinformatik (1)
- 6.5 Synthese und Streuverfahren nanostrukturierter Materialien (1)
- 7.2 Ingenieurbau (1)
- P Präsident (1)
- P.0 Präsident und andere (1)
Eingeladener Vortrag
- nein (432) (entfernen)
Iron aluminides depict a sustainable and light-weight material class which could be employed in many applications requiring high strength at intermediate to high temperatures. According to first results, the alloy Fe-26Al-4Mo-0.5Ti-1B surpasses conventional materials in wet corrosion resistance and creep resistance up to 650 °C. For these reasons, the AiF research project “WAFEAL – Materials applications for iron aluminides” was initiated to transfer these findings into a standardised materials dataset and to derive best practices for processing. In the first place, a set of different microstructures adjusted by varying casting methods, wall thicknesses and heat treatments was investigated and correlated with hardness on macro and micro scale. Correlations were drawn between solidification rates and resulting grain sizes and hardness. The effect of vacancy hardening was only verified for wall thickness as low as 2.5 mm. Moreover, a common decrease of macrohardness after a heat treatment at 1000 °C for 100 h was observed irrespective of casting process or wall thickness. This effect was linked with an unexpected decrease of the complex boride phase fraction which acts as a hardening phase.
Due to the advantages of Laser Powder Bed Fusion (PBF-LB), i.e., design freedom and the possibility to manufacture parts with filigree structures, and the considerable amount of knowledge available for 316L in its conventional variant, the mechanical behavior, and related microstructure-property relationships of PBF-LB/316L are increasingly subject of research. However, many aspects regarding the - application-relevant - mechanical behavior at high temperatures are not yet fully understood. Here, we present the results of an experimental study on the LCF behavior of PBF-LB/316L featuring a low defect population, which makes this study more microstructure-focused than most of the studies in the literature. The LCF tests were performed between room temperature (RT) and 600 °C. The mechanical response is characterized by strain-life curves, and hysteresis and cyclic deformation curves. The damage and deformation mechanisms are studied with X-ray computed tomography, and optical and electron microscopy. The PBF-LB/M/316L was heat treated at 450 °C for 4 h, and a hot‑rolled (HR) 316L variant with a fully recrystallized equiaxed microstructure was tested as a reference. Besides, selected investigations were performed after a subsequent heat treatment at 900 °C for 1 h. The PBF-LB/316L exhibits higher cyclic stresses than HR/316L for most of the fatigue life, especially at room temperature. At the smallest strain amplitudes, the fatigue lives of PBF-LB/M/316L are markedly shorter than in HR/316L. The main damage mechanisms are multiple cracking at slip bands (RT) and intergranular cracking (600 °C). Neither the melt pool boundaries nor the gas porosity have a significant influence on the LCF damage mechanism. The cyclic stress-strain deformation behavior of PBF-LB/M/316L features an initial hardening followed by a continuous softening. The additional heat treatment at 900 °C for 1 h led to decreased cyclic stresses, and a longer fatigue life.
Additive manufacturing (AM) offers diverse advantages compared to conventional manufacturing. In this work the microstructure of austenitic steel 316L, manufactured with Selective Laser Melting (SLM), was analyzed and compared to microstructure of 316L hot rolled material. Methods used for analysis are microprobe, optical microscopy and electron backscatter diffraction.
Microstructure ageing of stainless steel AISI 316L manufactured by selective laser melting (SLM)
(2019)
Additive manufacturing (AM) processes, such as SLM, offer a variety of advantages compared to conventional manufacturing. Today AM parts are still comparatively less cost-effective if they are manufactured in large quantities. To make the AM parts more cost-efficient, the AM process has to be improved. It requires a good understanding of microstructure formation, microstructure-property-relations and ageing processes affected by different loads.
In this work the ageing behavior of SLM manufactured AISI 316L stainless steel is evaluated. The microstructure effected by mechanical, thermal and corrosive loads are investigated and compared to as-built microstructure. Tensile tests are used for mechanical ageing. For thermal and corrosive loads the typical application conditions of 316L apply. The methods of microstructure investigation include SEM, TEM, CT and EBSD. The main object of this work is the description of microstructure and ageing processes of AM parts.
Inconel 718 (IN718) is a traditional age-hardenable nickel-based alloy that has been increasingly processed by additive manufacturing (AM) in recent years. In the as-solidified condition, IN718 exhibits chemical segregation and the undesired Laves phase, requiring a solution annealing (SA) prior to aging. The material produced by AM does not respond to the established thermal routines in the same way as conventionally produced IN718, and there is still no consensus on which routine yields optimal results. This work aims to provide a fundamental understanding of the heat treatment (HT) response by continuously monitoring the microstructural evolution during SA via time-resolved synchrotron x-ray diffraction, complemented by ex-situ scanning electron microscopy (SEM). The samples were produced by laser powder bed fusion to a geometry of 10x20x90 mm³, from which Ø1x5 mm³ cylindric specimens were extracted. Two different scanning strategies – incremental 67° rotations, Rot, and alternating 0°/67° tracks, Alt – were used, leading to two different as-built conditions. 1-hour SAs were carried out in the beamline ID22 of the ESRF at 50 KeV. Two SA temperatures, SA1 = 1020 °C, and SA2 = 1080 °C were tested for each scanning strategy. Data were processed using the software PDIndexer. In the as-built state, all samples showed typical subgrain columnar cell structures with predominant Nb/Mo segregation and Laves phase at the cell walls, as seen by SEM. The Alt scan induced higher intensity on the Laves peaks than the Rot scan, suggesting a greater content of Laves. Chemical homogenization in the SA was largely achieved during the heating ramp (Fig. 1). SA2 eliminated the Laves peaks just before reaching 1080 °C, and mitigated differences between Rot and Alt samples. On the other hand, SA1 induced the precipitation of the generally detrimental δ phase, also observed by SEM. Furthermore, the Rot scan showed higher δ peak intensities than the Alt scan, indicating a higher content of δ in the latter. No signs of recrystallization were observed in any of the investigated SAs.
With an increasing demand in more efficient fuel consumption to reduce CO2 emissions, weight reductions in high-temperature materials at affordable costs gain increasing attention. One potential candidate is the intermetallic material class of iron aluminides, combining the advantages in mass savings, high temperature performance and recyclability of resources. The alloy Fe-26Al-4Mo-0.5Ti-1B was selected to study the microstructural features evolving from two casting processes, five wall thicknesses and three final conditions. Conclusions are drawn upon the correlations of processing variables, grain sizes and hardness.
Microstructural characterization of the AlMo 0.5 NbTa 0.5 ZrTi refractory complex concentrated alloy
(2020)
A set of some unexpected and interesting microstructures has put the so-called complex concentrated alloys (CCAs) in the eye of the scientific community and the AlMo0.5NbTa0.5TiZr refractory (r)CCA, aimed at substituting Ni-base superalloys in gas turbine applications, belongs to this alloy family. The AlMo0.5NbTa0.5TiZr rCCA was studied by SEM, EDX, EBSD and TEM, showing the presence of a nanoscopic basket-wave structure inside the grains, with two BCC phases. Additionally, thermodynamic calculations on the AlMo0.5NbTa0.5TiZr alloy were done with two different proprietary databases that anticipate two BCC-disordered phases with distinct constitutions as well as an HCP phase.