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Im Rahmen des Teilprojektes 1 "Analyse und Erweiterung der Einsatzgrenzen der elastisch- plastischen Bruchmechanik zu tiefen Temperaturen hin mit der Option der systematischen Nutzung von Zähigkeitspotentialen im Übergangsbereich" wurden an drei Versuchswerkstoffen bei jeweils mehreren Prüftemperaturen Serien von Risswiderstandskurven aufgenommen. Die Arbeiten dienten der quantitativen Erfassung des Übergangs vom Spaltbruch zum Gleitbruch im Bereich nahe Ta mit dem Ziel, Sicherheitsreserven des Werkstoffs in diesem Bereich ausnutzen zu können. Im Rahmen des Teilprojektes 2 "Methoden zur Extrapolation von JR-Kurven für die Vorhersage der Rissöffnungsgeometrie unter postulierten Belastungen" wurden experimentelle Untersuchungen an Rohren aus dem Werkstoff 15NiCuMoNb5 (WB36) durchgeführt. Für die Rohrbiegeversuche wurde ein Prüfstand aufgebaut, auf dem bei Raumtemperatur Vierpunkt- Biegeversuche an Rohren mit unterschiedlichen Außenumfangsfehlergeometrien durchgeführt wurden. Mit Hilfe der zerstörungsfreien Verfahren Ultraschallprüfung, Schallemissionsprüfung, Gleichstrompotentialsondenverfahren und optische Analyse wurde das Risswachstums- und Leckageverhalten unter den komplexen Bedingungen der Rohrversuche quantitativ untersucht und detailliert vergleichend ausgewertet.
Pipelines and industrial piping systems are particularly relevant regarding technical safety, availability and maintenance. Large flow rates of hazardous substances imply that even smallest leakages can lead to high environmental impacts. Therefore, and to ensure the availability of infrastructure, an early detection and localization of potentially hazardous degradations to the walls (e.g. cracks, pittings, sedimentation, etc.) of the containments is necessary. However, in many cases it is not feasible to equip pipelines with a large number of point sensors at reasonable expense.
The principle of distributed fibre optic sensing relies on one single optical fibre, which simultaneously acts as a spatially continuous sensor as well as the signal transducer. Therefore, extensive structures can be provided with this type of sensor with comparatively low efforts.
As a consequence, monitoring oil and gas pipelines using distributed fibre optic sensors is on the upswing. Besides the established methods to measure temperature and strain, distributed acoustic sensing (DAS) has lately received considerable attention as a means to detect and localize third party threats to pipelines (approach of vehicles, digging, mechanical manipulation).
The so far not utilized potential of DAS as a means for continuous condition monitoring of pipes by detecting and localizing acoustic signals that point to certain damage scenarios, is currently under investigation in an interdisciplinary research project at BAM (AGIFAMOR, Ageing Infrastructures – Fibre Optic Monitoring of Pipes).
In order to qualify distributed acoustic fibre optic sensors for this application area, we especially focus on detecting and identifying the relevant acoustic emissions of interesting degradations as well as on the optimal way of application of the optical fibres to the specimen to achieve an optimal signal transmission of acoustic signals.
Four-point bending tests were carried out to analyze the acoustic characteristics of damage development in pipe segments made of steel, grade S355J2H, being 2.5 m long with an outer diameter of 168 mm and 16 mm wall thickness. To induce stable crack growth, the pipe segments were pre-damaged by a 90°circumferential notch in the middle of the pipe length. While the pipe was quasi-statically loaded, microscopic damage and plastic deformation accumulated to form a macroscopic crack that grew through the pipe wall until leakage. For acoustic emission (AE) monitoring, four broadband sensors of type VS 900 M were mounted close to the notch. Continuous AE signal detection was performed by the non-threshold method. Advantages and disadvantages of the non-threshold AE monitoring compared to a commonly employed method analyzing only signals exceeding a predefined threshold are discussed. The results of AE analysis are compared to additional information on the crack growth detected by the direct current potential drop (DCPD) technique. These studies were carried out in the course of the interdisciplinary research project AGIFAMOR, Ageing infrastructures - distributed acoustic monitoring of pipes at BAM.
The roll-on-roll-off passenger ferry MV ESTONIA sank during the night of 28 September 1994 in the Baltic Sea. In October 2000, divers recovered two palm-sized test pieces from the front bulkhead of the wreck. The investigators analysed these specimens to determine whether there were any indications of deliberate blasting. Since the wreck had been submerged for almost six years, it was clear that chemical traces would not be present on the surfaces of the test pieces. Therefore, the investigators performed comparative tests on shipbuilding steel to find a microstructural criterion that exclusively characterises a blast. The shipyard Jos. L. Meyer, Germany, had built the ESTONIA and supplied shipbuilding steel plates similar to that used for building the vessel in 1979/1980. The comparative tests comprised mechanical tests, shot peening tests and blasting tests using different explosives. Testing demonstrated that blasting always formed twinned ferrite grains in the microstructure over the whole cross-section of each of the 8 mm thick comparative plates. Although one of the original test pieces of the ESTONIA showed deformation twins, this was only confined up to 0.4 mm underneath the surfaces and not spread over the whole cross-section. Comparative shot peening tests produced the very same pattern of subsurface deformation twins. Therefore, the twins detected in the microsection of the test pieces of the ESTONIA wreck traced back to the shot peening process performed by the shipyard in 1979/1980 and not to a deliberate blast.
Dynamic fracture mechanics characteristics are required for design and safety proof of advanced
ductile cast iron (DCI) components. In this paper, the analytical compliance ratio
(CR) and numerical finite element (FE) key curve methods were investigated for dynamic Rcurve
testing. Two DCI materials, a purely ferritic and a ferritic one with 18 % of pearlite,
were tested at room temperature (RT) and -40 °C. The special focus is on the impact of the
materials damage and fracture behaviour on performance and limitations of the investigated
methods.
Systematic metallographic and fractographic microstructural analyses were performed accompanying
the test program. Summarizing systematics of the specific damage behaviour
and fracture mechanisms were developed taking microstructure, loading rate, specimen geometry
and test temperature into account.
There has been a change from ductile to brittle fracture mechanism observed at -40 °C with
ferritic DCI and even at RT with ferritic-pearlitic DCI. The ferritic-pearlitic DCI did not show Rcurve
behaviour at -40 °C and only single Juc values could be determined. Furthermore, with
ferritic-pearlitic DCI, random pearlite shares in the ligament caused the relation between
loading rate, force-deflection record and crack extension not to remain uniquely defined.
Therefore, the FE key curve method proofed not to be applicable since the FE model was
based on homogeneous isotropic material and ductile failure mode only. The analytical CR
key curve method worked well only with selected combinations of microstructure, specimen
geometry and temperature.
In summary it has to be concluded that a robust, accurate and sufficiently simple dynamic
key curve method that was suited for application in quality control of industrial relevant DCI
qualities cannot be provided currently.
A steel pipeline segment of 2.5 m length was subjected to quasi-static four-point bending load in three steps for studying the initial cracking and damage accumulation based on the Acoustic Emission (AE) technique and by the direct current potential drop (DCPD) technique. For the latter, a new post-test analysis method was established.
AE is found more sensitive to crack initiation than DCPD. Formation of mesoscopic and macroscopic cracks as well as their closure and the resulting friction generate weighted peak frequencies below 400 kHz, whereas microscopic cracking produces AE with broad band spectra identifiable by weighted peak frequencies above 400 kHz. Critical states alike the maximum load level and the leak opening were accompanied by peak amplitudes above 85 dBAE. This rather fundamental study provides a data base for possibly developing advanced strategies of detection and alarm systems based on acoustic monitoring of pipelines, or at least, steel structures.
Um ein tieferes Verständnis über die Schallemission bei der Entstehung und Ausbreitung von Rissen in Stahlrohrleitungen zu erlangen, wurde ein Stahlrohr der Güte S355J2H im Vierpunkt-Biegeversuch quasistatisch bis hin zum Wanddurchbruch (Leckage) belastet und mittels Schallemissionsmessung und Gleichstrompotentialmessung überwacht. Das Rohrsegment wurde durch einen 90°- Außenumfangskerb in der Mitte der Rohrlänge definiert vorgeschädigt, um davon ausgehend ein stabiles Risswachstum zu induzieren und die Analyse von Schallemission aus Rissereignissen, die am Kerb eintraten, sicherzustellen. Für die Schallemissionsmessung wurden vier Breitbandsensoren max. 105 mm vom Kerb entfernt montiert. Die Signalaufzeichnung erfolgte kontinuierlich und schwellwertunabhängig. Für die Gleichstrompotentialmessung wurde ein Gleichstrom von 300 A eingeleitet und der Potentialabfall über dem Kerb mit fünf Sonden entlang des Kerbs gemessen. Beide Messverfahren identifizieren die Rissinitiierung sowie Veränderungen im Risswachstum. Die detektierten Schallemissionsereignisse werden, unter Berücksichtigung spektraler Eigenschaften, mit fortschreitender Belastung und Rissentwicklung analysiert. Diese Studien wurden im Rahmen des interdisziplinären Forschungsprojekts AGIFAMOR, Aging infrastructure - Faseroptisches Monitoring von Rohrleitungen, an der BAM durchgeführt.
Ferritic spheroidal graphite cast iron (SGI) materials have a remarkable technical poten-tial and economic impact in modern industry. These features are closely related to the question of how the cast materials can be produced without structural defects and graphite degenerations such as for example chunky graphite. Although the chunky graphite degeneration superficially seems to be well known, its metallurgical background is still controversially discussed, appropriate field-tested non-destructive tools for its quantification in castings are lacking and the knowledge on its impact on material properties is fairly limited. Addressing this status, the article is providing a current overview on the subject. Existing theories on formation and growth mechanisms of chunky graphite are briefly reviewed. Furthermore, from a metallurgical point of view, causes for the appearance of chunky graphite as well as preventive measures are concisely summarized. Particular attention is paid to the morphology of chunky graphite and how it can be characterized by destructive and non-destructive techniques. Special emphasis was laid on providing a comprehensive overview on the impact of chunky graphite on strength, ductility, fatigue limit, fatigue crack growth rate as well as fracture tough-ness of ferritic SGI materials based on experimental data. Moreover, conclusions for the assessment of castings affected by chunky graphite are drawn.