Filtern
Erscheinungsjahr
Dokumenttyp
- Zeitschriftenartikel (23) (entfernen)
Schlagworte
- Fatigue (3)
- Fire stability (3)
- Fully developed fire (3)
- Composite (2)
- Curing kinetics (2)
- Fracture (2)
- High-temperature properties (2)
- Self-healing (2)
- Buckling (1)
- CFRP (1)
Organisationseinheit der BAM
Paper des Monats
- ja (1)
A new approach is discussed for characterizing the damage state of FRP with the appearance of micro cracking and its influence on the residual strength. For the quantitative analysis of micro cracking, X-ray refraction topography was used. Fatigue treatment of carbon fibre reinforced plastics (CFRP) laminates were performed to create defined damage states. With regard to real loading conditions of CFRP, studies on tube samples were performed to investigate two dimensional (tensiontorsion) loads. A rheological material model was presented which described the increase of micro cracking in ±45° CFRP laminates with a continuum mechanical approach. The correlation between the results of the X-ray refraction topography, the damage parameter of the rheological model and the decrease of residual strength were shown. The inter fibre fracture surface of the investigated CFRP materials was determined with tensiontorsion loaded tube specimens of 90°-laminate and a layer-wise strength analysis was done. Micro cracking occurs even at 50% inter-fibre fracture loading and can lead to a distinct strength reduction. The intralaminar fatigue effect itself seems to be an indication for the damage accumulation and the load history.
Moderne Leichtbaustrukturen (Luftfahrt, Eisenbahn, Automotive) aus Faserverbundwerkstoffen (FVW) sind hohen mechanischen und klimatischen Beanspruchungen ausgesetzt. Aussagen über die Lebensdauer und Funktionssicherheit der FVW-Bauteile können eher aus Untersuchungen der mikromechanischen Eigenschaften gewonnen werden als aus der globalen Festigkeit. Die Röntgenrefraktionstopografie ist ein Verfahren zur zerstörungsfreien Bestimmung von inneren Oberflächen in Werkstoffen. Angewendet auf FVW lassen sich Aussagen über die Faserorientierungen, die Fertigungsqualität sowie über Faser-Matrix-Ablösungen und Matrixrisse infolge mechanischer Beanspruchung gewinnen. Nachfolgend wird ein neues Verfahren zur Bestimmung des Zwischenfaserbruchversagens am komplexen Laminat vorgestellt. Hierbei wird das Röntgenrefraktionsverfahren "online bei Zug-Belastung der Probe angewendet.
In a research project fatigue tests on two identical wing sections that are used as representative substitute components were performed to estimate lifetime enhancement of light-weight aircraft such as general aviation gliders. Single step fatigue tests at limit load on one component were compared with spectrum loading on the other. A characteristic damage behaviour was observed. Local buckling due to high shear loading of the sandwich core of the wing shell causes the main damage. Even though an intentionally high load level was chosen no increase of micro-cracking could be detected. Additionally no delamination effects in laminates or bondings were observed except the skin-core delamination which causes the buckling effect in the wing shell due to fatigue loading. Finally the concept of using representative substructures and accompanying specimen tests is an effective approach for in-service loading investigations and could also be applied to research on wind turbine blades.
Near-infrared spectroscopy (NIR) turned out to be well suited for analyzing the degree of cure for epoxy systems. In contrast to dynamic scanning calorimetry (DSC), where the released heat of reaction determines the degree of epoxy conversion indirectly, NIR spectroscopy is able to determine the conversion directly by analyzing structural changes. Therefore, a new heatable NIR cell was equipped with an integrated thermocouple, which enables the real sample temperature to be controlled and monitored in situ during epoxy curing. Dynamic scans at different heating rates were used for kinetic modelling, to define kinetic parameters and to predict real curing processes. The kinetic models and their parameters were validated with an isothermal and a more complex multi-step curing scenario. Two available commercial epoxy systems based on DGEBA were used with an anhydride and with an amine hardener. NIR results were compared with DSC data. The simulated conversion predicted with a model fitted on the basis of NIR and DSC dynamic scans showed good agreement with the conversion measured in the isothermal curing validation test. Due to the proven reliability of NIR in measuring the reaction progress of curing, it can be considered a versatile measurement system for in situ monitoring of component production in the automotive, aerospace and wind energy sectors.
Fire stability of glass-fibre sandwich panels: The influence of core materials and flame retardants
(2017)
Fire resistance has become a key property for structural lightweight sandwich components in aviation, shipping, railway vehicles, and construction. The development of future composite materials and components demands adequate test procedures for simultaneous application of compression and fully developed fire. Therefore an intermediate-scale approach (specimen size = 500 mm x 500 mm) is applied with compressive loads (up to 1 MN) and direct application of a burner to one side of the specimens, as established in aviation for severe burn-through tests. The influence of different core structures (polyvinylchloride foam, polyisocyanorate foam reinforced by stitched glass bridges, and balsa wood) was investigated for glass-fibre-reinforced sandwich specimens with and without flame retardants applied on the fabrics, in the matrix, and on surface for each specimen at the same time. Times to failure were increased up to a factor of 4. The intumescent coating prolongs the time to failure significantly.
What is more, using the intrinsic potential of the front skin together with the core to protect a load bearing back skin in sandwich panels, the design of the core – here using the wood core – is the most promising approach.
Non-isothermal heating rate kinetics was applied to two epoxy resin systems. In situ near-infrared (NIR) measurements were taken with a heatable NIR cell which allowed the cure to be monitored by characteristic absorption bands. An autocatalyzed reaction of the nth order was shown to describe the epoxy conversion curves. Differential Scanning Calorimetry (DSC) was used as a complementary method. The kinetic models developed by both NIR and DSC are in good accordance with experimental epoxy conversion in the in situ NIR setup for single and multiple cure temperature ramps.
A linear calibration curve of the characteristic absorption bands of epoxy normalized to aromatic vibrations was introduced. The curing degree of structural epoxies that were cured according to an industrial temperature cure profile was determined by NIR using the calibration curve. The epoxy conversions of the structural components showed good agreement with the experimental in situ NIR. Several degrees of cure for structural specimens were evaluated by NIR and residual reaction enthalpy by DSC. We present the non-destructive NIR spectroscopy as an alternative to determine fast and non-destructive epoxy conversion, particularly suitable for high degrees of cure on structural components.
A test set-up in intermediate scale was conceived to investigate the structural integrity of materials under fire. The task was to develop a realistic test scenario targeting component-like behaviour. Carbon-fibre-reinforced sandwich specimens (500 X 500 X 20 mm) were used to examine failure mechanisms, times to failure and critical failure loads under compression. Fire tests were performed with fully developed fire applied to one side of the specimen by an oil burner. In a first test series, the applied load was varied, but the fully developed fire remained unchanged. In general, times to failure were short. Decreased load levels resulted in prolonged times to failure and led to a different failure mechanism. Results obtained in the test series were compared with a bench-scale study (150 X 150 X 20 mm) investigating identical material. The comparison clearly revealed the influence of size on the time to failure and the load-bearing capacity.
Assessing the structural integrity of carbon-fibre sandwich panels in fire: Bench-scale approach
(2019)
The fire resistance of lightweight sandwich panels (SW) with carbon fibre/epoxy skins and a poly(methacryl imide) (PMI) foam core is investigated in compression under direct application of a severe flame (heat flux=200 kW m−2). A bench-scale test procedure was used, with the sample held vertically. The epoxy decomposition temperature was quickly exceeded, with rapid flash-over and progressive core softening and decomposition.
There is a change in failure mode depending on whether the load is greater or less than 50% of the unexposed failure load, or in other words if one or two skins carry the load. At high loads, failure involved both skins with a single clear linear separation across each face. There is an inflection in the failure time relationship in the ∼50% load region, corresponding to the time taken for heat to be transmitted to the rear face, along with a change in the rear skin failure mode from separation to the formation of a plastic hinge. The integrity of the carbon front face, even with the resin burnt out, and the low thermal diffusivity of the core, both play key roles in prolonging rear face integrity, something to be borne in mind for future panel design. Intumescent coatings prolong the period before failure occurs. The ratio of times to failure with and without protection is proposed as a measure of their effectiveness. Apart from insulation properties, their adhesion and stability under severe fire impact play a key role.