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Elastomer seals are widely used as barrier seals in containers for low and intermediate level radioactive waste and for spent fuel transportation casks. In addition, they are also used for spent fuel storage and transportation casks (dual purpose casks (DPC)) as auxiliary seals to allow leakage rate measurements of metal barrier seals for demonstration of their proper assembling conditions. Depending on the area of use, the rubber materials have to demonstrate proper sealing performance with regard to mechanical, thermal, and environmental conditions as well as irradiation during the entire operation period. Concerning DPC, degradation effects should be limited in a way that, for example, effects from potentially released decomposition elements may not harm e.g. metal barrier seals. Leakage rate measurements should be possible also after long interim storage periods prior to subsequent transportation.
Because of the complex requirements resulting from the various applications of containers for radioactive waste and spent nuclear fuel, BAM has initiated several test programmes for investigating the behaviour of elastomer seals. In this contribution the current status is described and first results are discussed.
In the approval procedure of transport packages for radioactive materials, the mechanical and thermal safety assessment is carried out in Germany by competent authority BAM. In recent years BAM was involved in several licensing procedures of new spent fuel and HLW package designs, where the cask body was made of Ductile Cast Iron (DCI). According to IAEA regulations package designs have to fulfill requirements for specific conditions of transport. Type B(U) packages must withstand the defined accident conditions of transport. The temperature range from -40°C up to the operational temperature has to be considered. For the cask material DCI, it is necessary to determine the brittle fracture behavior. The German guideline BAM-GGR 007 defines requirements for the fracture mechanics of DCI. Due to complex structure of the cask body and the dynamic loading a fracture mechanical assessment in an analytical kind is not always possible. Experience of recent design approval procedures show that the application of numerical calculations are applicable to determine the fracture mechanical load in the cask body. At the first step a numerical analysis has to be done to identify the loading state at the whole cask body. Secondly an analysis of a detail of the cask body is made considering the displacement boundary conditions of the global model. An artificial flaw is considered in this detailed model to calculate the fracture mechanical loading state. The finite element mesh was strongly refined in the area of flaw. The size of the artificial flaw is characterized by the ultrasonic inspection used for the quality assurance of the package. The applicant developed additional analysis tools for calculation of stress intensity factor and/or J-Integral. The assessment approach by BAM led to the decision to develop own tools to the possibility for independent check of the results.
The paper describes the authority assessment approach for the DCI fracture mechanics analysis. The validation procedure incl. the development of own tools is explained. BAM developed a post-processor called JINFEM to determine the fracture mechanical loads. The regulatory 1 m puncture bar drop test is used to give an example of the assessment procedure.
In the design approval of transport packages for radioactive materials, the mechanical and thermal safety assessment is carried out in Germany by competent authority BAM. In recent years BAM was involved in several licensing procedures of new spent fuel and HLW package designs, where the cask body is of Ductile Cast Iron (DCI). According to IAEA regulations package designs have to fulfill requirements for specific conditions of transport. Type B(U) packages must withstand the defined accident conditions of transport. The temperature range from -40°C up to the operational temperature has to be considered. For the cask material DCI, it is necessary to determine safety against brittle fracture. The German guideline BAM-GGR 007 defines requirements for fracture mechanics of packagings made of DCI. Due to complex cask body structure and the dynamic loading a fracture mechanical assessment by analytical approaches is not always possible. Experience of recent design approval procedures show that the application of numerical calculations are applicable to determine the stresses and stress intensity factors in the cask body. At the first step a numerical analysis has to be done to identify
the loading state at the whole cask body. Secondly an analysis of a detail of the cask body is made considering the displacement boundary conditions of the global model. An artificial flaw is considered in this detailed model to calculate the fracture mechanical loading state. The finite element mesh was strongly refined in the area of the flaw. The size of the artificial flaw is based on the ultrasonic inspection acceptance criteria applied for cask body manufacture. The
applicant (GNS) developed additional analysis tools for calculation of stress intensity factor and/or J-Integral. The assessment approach by BAM led to the decision to develop own tools to the possibility for independent proof of the results.
The paper describes the authority assessment approach for DCI fracture mechanics analysis. The validation procedure incl. the development of own tools is explained. BAM developed a postprocessor to determine the fracture mechanical loads. A horizontal 1 m puncture bar drop test is used to give a detailed description of the assessment procedure.
This paper demonstrates exemplarily how numerical and experimental approaches can be combined reasonably in mechanical assessment of package integrity according to the IAEA regulations. The paper also concentrates on the question about how static mechanical approaches can be applied, and what their problems are in relation to dynamic calculation approaches. Under defined impact tests, which represent accident transport conditions, the package has to withstand impact loading, e.g. resulting from a 9 m free drop onto an unyielding target in sequence with a 1 m puncture drop test. Owing to the local character of the interaction between the puncture bar and the cask body, it is possible to develop a dynamic numerical model for the 1 m puncture drop which allows an appropriate simulation of the interaction area. Results from existing experimental drop tests with prototype or small scale cask models can be used for verification and validation of applied analysis codes and models. The link between analysis and experimental drop testing is described exemplarily by considering a regulatory 1 m puncture bar drop test onto the cask body of a recently approved German high level waste transport package. For the 9 m drop test of the package, it is difficult to develop a dynamic numerical model of the package due to the complexity of the interaction between cask body, impact limiters and unyielding target. Dynamic calculations require an extensive verification with experimental results. The simulation of a 9 m drop of a package with impact limiters is thereby often more complex than the simulation of a 1 m puncture drop onto the cask body. A different approximation method can be applied for the consideration of dynamic effects on the impact loading of the package. In a first step, maximum impact force and rigid body deceleration of the cask body during the impact process can be calculated with simplified numerical tools. This rigid body deceleration can subsequently be applied on a verified static numerical model. Dynamic effects, which cannot be covered by the static numerical analysis, have therefore to be considered by using an additional dynamic factor. The paper describes this approach exemplarily for a 9 m horizontal drop of a typical spent fuel cask design.
A material testing program to characterize the concrete behavior under static and dynamic loads
(2010)
In this paper a comprehensive material testing program is described to characterize a German final repository concrete material (BERB1) subjected to static and dynamic loads. The BERB1 material was developed und specified by the German Bundesanstalt für Materialforschung und -prüfung (BAM) for targets used for drop tests according to the KONRAD requirements.
The testing consists of three concurrent laboratory experimental programs performed in the USA. An extensive preliminary testing program in Germany was performed to assure the required concrete specifications during fabrication and curing.
The first set of data is the static basic material test program consisting of structural tests to quantify macroscopic concrete properties under quasi-static loads. Cubic and cylindrical specimens are investigated under this effort. The second set of test data is from the static complete material test program, where cylindrical concrete specimens are subjected to a variety of quasi-static axial and radial stress and strain paths using a high-pressure hydraulic tri-axial chamber. The material is characterized for confining pressures up to 400 MPa. The third set of data is from the dynamic complete material test program, which uses a modified Split-Hopkinson Pressure Bar to induce dynamic compression and tension waves into cylindrical concrete specimens that generate strain-rates up to 400 s-1.
The ensemble of data generated in these experiments provides a complete set of data that effectively describes the behavior of this concrete and can be used to develop a constitutive calculation model. In addition, the results of the tests show a significant effect of moisture on the strength and rheology of this concrete for quasi-static pressures greater than 50 MPa. Numerical drop test simulations with the developed constitutive model in the Lagrangian finite element code, LS-DYNA, show good agreement with the experimental results from a BAM research project.
Polyurethane foam used as impact limiter material undergoes high plastic deformations, whereat the resulting stress-strain relations strongly depend on loading speed and temperature. This paper discusses the efforts necessary to develop a reliable numerical foam simulation model focussing on generation and implementation of temperature- dependent yield curves
Elastomer seals are mounted as barrier seals in lid systems of containers designed for transport and disposal of negligible heat generating radioactive waste and as auxiliary seals in spent fuel storage and transportation casks (dual purpose casks (DPC)). When the behavior of mounted seals under normal and hypothetical accident conditions of disposal and transport is to be simulated, a comprehensive knowledge of their complex mechanical properties at every state of aging is necessary. In previous works, BAM’s efforts in experimental investigations on specimen artificially aged at different temperatures and times and the implementation of the found results in finite element material models were presented. Additionally, our approaches to reproduce the aging process itself and to extrapolate the results of artificially accelerated aging to longer times were presented. Numerical simulations have shown that the behavior of the seal during mounting and one-sided pressurizing and the resulting performance values such as leakage rate strongly depend on the coefficient of friction (COF) between flange and seal. The friction coefficient, in turn, depends on the aging state of the elastomer material as several publications suggest (see below).
Dynamic COF between an exemplary ethylene propylene diene rubber (EPDM) material and a stainless steel ball were determined by using a self-designed linear oscillation tribometer. Unaged and artificially aged EPDM specimen stored for 30 days and 100 days at a temperature of 150 °C were tested. A stainless steel ball (d=10 mm) is brought in contact with the specimen’s surface und loaded by normal forces of 2.5 N, 5 N, 10 N and 20 N. During a reciprocating movement of the EPDM sheet, the horizontal force/friction force is continuously measured, and the COF can be derived.
It is well known that friction is a complex phenomenon especially in soft materials. It cannot be excluded that the measured friction force is influenced by additional force components, resulting from the ball’s grooving through the elastomer’s surface. This force depends on the penetration depth of the ball and on the resistance of the elastomer in its different states of aging. The latter results from microstructural changes i.e., chain scission and additional crosslinking that occur during aging which in turn influence the softening or hardening of the material.
A finite element (FE) ABAQUS® model was developed to reproduce the measurement process. It should help to better understand the physical mechanisms and to quantify the percentage of measured forces resulting from real friction on the one hand and forces resulting from unintended side effects that could falsify the result on the other hand. The behavior of the elastomer in its different states of aging is reproduced by a FE material model already presented in previous works of BAM.