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Organisationseinheit der BAM
Für die Sicherheit und Gebrauchstauglichkeit von geschweißten Behältern mit Aufdachungen unter Innendruck müssen die Biegezusatzspannungen berechnet oder wirklichkeitsnah abgeschätzt werden. Dazu können verschiedene Verfahren herangezogen werden, die sich in Aufwand, Genauigkeit und zeitlicher Verfügbarkeit des Ergebnisses unterscheiden. Beim Entwurf von Behältern, im Betrieb oder im Schadensfall kommen sie zum Einsatz.
Calculation of ultrasonic reflection and transmission in anisotropic austenitic layered structures
(1999)
Characterization of the microstructure of high-chromium cast irons using Mössbauer spectroscopy
(2001)
The finish grinding process for cement materials uses ball mills with differently sized grinding balls. Because the grinding takes place through the impact and friction of the balls, balls with a high wear resistance are desirable and the materials of choice are the high-chromium white cast irons. This article examines the behavior of these cast irons when subjected to various heat treatments. The emphasis is on the dependence of the microstructure properties on the chemical composition of the alloys and the heat treatment parameters. The content of retained austenite and that of carbon in the martensite phase were determined by the use of Mössbauer spectroscopy. The results verify that a higher proportion of retained austenite with low carbon content and a martensite with higher hardness produce a material with good fracture toughness and resistance to abrasive wear.
In lightweight car body shell mass production, due to requirements on vehicle weight reduction and carbon dioxide emissions, joining of advanced high strength steels (AHSS) with different joining procedures and especially hybrid bonding techniques is becoming more and more important. One of these hybrid bonding techniques is the combination of resistance spot welding and adhesive bonding called weldbonding. One of the important advantages of weldbonded joints in comparison to resistance spot welded joints are the enhanced mechanical properties. To guarantee sufficiently high quality conditions regarding the strength of the weldbonded joints, the influences of the applied adhesive systems and of different base metal combinations are studied. This is carried out for both non-corrosive and corrosive environments and for the choice of different joining parameters settings. In particular, the mechanical behaviour of the weldbonded joints is investigated under quasi-static, impact and fatigue loads. Furthermore, the energy absorption of the weldbonded joints for both non-corrosive and corrosive environments is studied. It is shown that the weldbonded joints possess higher mechanical strengths in all load cases (quasi-static, impact and fatigue). Corrosive attack affects weldbonded joints, and the quasi-static strength is reduced. Resistance spot welded joints are not affected by the corrosive attack, but even after several weeks of corrosive attack, the quasi-static strength of weldbonded joints remains higher than that of resistance spot welded joints.
For spot-welded joints, the resistance to
mechanical stress depends on the local strength properties
and gradients in the weld area. The commonly used
methods for investigating the stress–strain behaviour across
the weld area are connected with a high level of sample
preparation and with considerable limitations in local resolution.
A promising method for determining locally
resolved stress–strain curves is the instrumented indentation
test in connection with the method of representative
stress and strain (RS) and the method of artificial neural
networks (NNs). The stress–strain properties of the weld
nugget and the base metal determined by these two methods
are compared and discussed, additionally in relation to
the stress–strain curves obtained from the tensile test. The
measured Vickers hardness across the weld area is compared
with the evaluated local stress–strain properties.
Three steels used in automobile manufacturing are investigated:
mild steel DC04 and two advanced high-strength
steels (TRIP steel HCT690T and martensitic steel HDT
1200M). The results of the two methods (RS and NN) show
good correspondence for the base metal area but some
significant differences for the weld nugget. Comparing the
data across the weld area, no evidence of the presence of
residual stress (which would influence the results) was
found.
Methods to obtain weld discontinuities in spot-welded joints made of advanced high-strength steels
(2011)
Resistance spot welding is the major joining technique in mass car production. This applies in particular to high-strength steel and advanced high-strength steel (AHSS) joining of thin sheet steel components for lightweight body shell structures. Joining of AHSS in mass production might lead to weld discontinuities under certain circumstances. Those discontinuities in form of cracks might be an initial start of cracking in the spot-welded joints regarding fatigue loads. It is of great interest to figure out, if, in comparison to specimens without weld discontinuities, the crack initiating point changes and if the fatigue resistance might be reduced by the discontinuities. In this contribution, an overview of potential discontinuities is given. Their possible causes are discussed and means for their detection are highlighted. Among the possible causes of weld discontinuities, two major groups are distinguished: the welding parameters as primary influences in the welding process, and the production-specific influences as secondary ones. With emphasis on major cracks penetrating the weld nugget, these influences are analysed. Finally, a combination of extreme welding parameters with production-specific influences is chosen in order to establish a method which enables the preparation of fatigue test specimens with reproducible major cracks in different locations of the spot-welded joints. This method is than applied in order to prepare spot weld specimens for fatigue tests.
Study of fatigue behavior for spot welded tensile shear specimens of advanced high strength steels
(2012)
For automotive body-in-white applications the influence of manufacture-related gaps between the steel sheets and also of manufacture-related surface cracks on the fatigue behavior of tensile shear specimens for spot welded TRIP steel was analyzed. It was shown that gaps between the steel sheets reduce the fatigue strength, whereas the fatigue behavior is neither influenced by cracks in the electrode indentation area nor in the heat effected zone.
In this study, the influence of production-related gaps on the shear tension strength and fatigue performance was investigated for resistance spot welded TRIP steel HCT690. Furthermore, the local strain distribution in shear tension test was calculated by the digital image correlation technique (DIC). The static shear tension strength was found to be almost independent of gaps up to 3 mm. The maximum local strain in the spot weld region however decreases depending on which sample side (deformed or undeformed) is considered. In addition, it has been ascertained that gaps of 3 mm lead to a significant drop in fatigue life compared to gap-free shear tension samples. This fact could be attributed to decreased stiffness, higher transverse vibration and higher rotation (θ) between the sheets as well as increased local stress calculated by 2 dimensional FE simulation.
For the designing of safety-relevant components particularly by means of finite element calculations, great significance is attached to the determination of local material parameters in the welding region. Conventional test methods can merely provide global parameters which, however, are frequently not sufficient precisely for the calculation of resistance-spot-welded components since these are characterised by the existence of joining zones with tight local limitations. In contrast, modern test methods such as optical strain field measurement permit the determination of the characteristic material data for concrete locations and times. In order to establish the potential of optical strain field measurements for the characterisation of the local material behaviour of spotwelded joints, tensile shear tests as well as tensile tests were carried out on resistance-spot-welded high-strength steels. The results show the high potential of this procedure not only for the quantification of the local strain behaviour in the joining region but also for the determination of local characteristic material data.
In the lightweight body shell mass production of automobiles, the application of hybrid bonding techniques becomes more and more important. Especially the combination of adhesive bonding and resistance spot welding called weldbonding is of great importance. The target of this contribution is to show the influence of medium-viscosity and low-viscosity structural adhesives on the process reliability of the weldbonding process and the mechanical properties of the hybrid bonded joints. The given results are based on the application of an epoxy PUR-based, an epoxy resin-based and a rubber-based adhesive system for joining a mild and some different advanced high strength steels (AHSS). It will be shown that both the process reliability of the weldbonding process and the mechanical behaviour of the weldbonded joints are influenced by the combinations of the base metals, the applied adhesive systems and the choice of the joining parameters. The behaviour of the weldbonded joints will be studied under quasi-static and impact loads. The discussion of the metallurgical structure of the weldbonded joints depending on the joining parameters will be given, too. Furthermore, the fatigue behaviour of the weldbonded joints will be studied.
Numerical simulation of component and assembly behaviour under different loading conditions is a main tool for safety design in automobile body shell mass production. Knowledge of local material behaviour is fundamental to such simulation tests. As a contribution to the verification of simulation results, the local deformation properties of spot-welded similar and dissimilar material joints in shear tension tests were investigated in this study for a TRIP steel (HCT690T) and a micro-alloyed steel (HX340LAD). For this reason, the local strain distribution was calculated by the digital image correlation technique (DIC). On the basis of the hardness values and microstructure of the spot welds, the differences in local strain between the selected material combinations are discussed. Additionally, the retained austenite content in the TRIP steel was analysed to explain the local strain values. Results obtained in this study regarding similar material welds suggest significant lower local strain values of the TRIP steel HCT690T compared to HX340LAD. One reason could be the decrease of retained austenite in the welded area. Furthermore, it has been ascertained that the local strain in dissimilar material welds decreases for each component compared with the corresponding similar material weld.
Joining of ultra high strength steels for lightweight body shell design in automobile manufacturing
(2010)
A method is reported with which heat affected zone (HAZ) cracks in a specific region of spot welded joints, made of advanced high strength steels, could be realised. The influence of HAZ cracks on the fatigue behaviour, which is the focus of the contribution, was studied by evaluating the stiffness characteristics as a function of the number of cycles N in comparison with crack-free specimens, i.e. by analysing HAZ and fatigue cracks on the specimen surface and the surface of fatigue fractures containing beach marks. It was found that the fatigue cracks are not initiated at the HAZ cracks. The number of cycles to failure Nf is not significantly reduced for specimens with HAZ cracks. Overall, the examinations did not reveal any influence of HAZ cracks on the fatigue strength of resistance spot welded joints.
Extended weldability lobes in resistance spot welding of advanced high strength steels (AHSS)
(2009)
Resistance spot welded joints made of two advanced high strength steels (AHSS) and one high strength steel (HSS) were examined. In the high cycle fatigue regime tests were realised for one loading condition, and the load and the displacement were measured. From the load and displacement range, the stiffness was calculated and in situ normalised to its value after 1000 cycles. It was thus possible to use the normalised stiffness evaluated during the experiment as failure criterion for the fatigue test of resistance spot welded joints. In order to evaluate this failure criterion, fatigue cracks were produced in the three different steel grades mentioned above according to user-specified levels of the normalised stiffness. It was found that the fatigue crack area increases linearly and the through-sheet-thickness crack length exponentially with decreasing stiffness. The comparison of the fatigue crack propagation during the fatigue test of the three different tested base metals showed very similar values. The comparability of fatigue tests performed on spot welded joints might thus be improved by the in situ evaluated stiffness as a failure criterion. This can be also used in further work to verify results of computer simulations of the stress intensity factor at spot welds with the help of experimental results.
Die Ermittlung lokaler Werkstoffkennwerte im Schweißbereich ist für die Auslegung sicherheitsrelevanter Bauteile insbesondere durch Finite-Elemente-Berechnungen von großer Bedeutung. Konventionelle Prüfmethoden können lediglich globale Kennwerte bereitstellen, die jedoch gerade für die Berechnung widerstandspunktgeschweißter Bauteile häufig nicht ausreichen, da diese durch das Vorliegen örtlich eng begrenzter Fügezonen gekennzeichnet sind. Moderne Prüfmethoden wie die optische Dehnungsfeldmessung ermöglichen hingegen eine orts- und zeitkonkrete Bestimmung der Werkstoffkenndaten. Um das Potenzial optischer Dehnungsfeldmessungen für das Charakterisieren des lokalen Werkstoffverhaltens von Punktschweißverbindungen zu ermitteln, wurden Scherzugversuche sowie Zugversuche an widerstandspunktgeschweißten hochfesten Stählen durchgeführt. Die Ergebnisse zeigen das hohe Potenzial dieses Verfahrens sowohl für die Quantifizierung des lokalen Dehnungsverhaltens im Fügebereich als auch für die Ermittlung lokaler Werkstoffkenndaten.
In einem Forschungsvorhaben wurde der Einfluss von fertigungsbedingten Spalten von bis zu 3 mm auf das Tragverhalten der Widerstandspunktschweißverbindungen aus Stählen am Beispiel von HX340LAD+Z (Werkstoffnummer 1.0933), HCT780X+Z (1.0943), HCT980C (1.0955) und 22MnB5+AS140 untersucht. Neben spaltabhängigen Schweißbereichen wurden auch statische Festigkeit, dynamische Festigkeit sowie Schwingfestigkeit betrachtet. Schließlich wurden ein Prozesssicherheitskoeffizient sowie eine Prozess-Festigkeits-Kenngröße abgeleitet, mit deren Hilfe der Anwender das Verhalten der Punktschweißverbindungen unter Spalteinfluss beurteilen kann.
The recommendation is based on the co-authors’ work organized by the RILEM TC 256-SPF “Spalling of concrete due to fire: testing and modelling”. It aims to provide useful information, guidance and best practices in fire spalling assessment to laboratories that perform large-scale tests based on fire resistance test standards. It provides guidance on the spalling observation techniques during testing, as well as post-test spalling quantification/assessment methods. This document is intended to be used in conjunction with the fire resistance test standards, e.g. EN 1363-1 and ISO 834-1.
Flexible automation with compact NMR spectroscopy for continuous production of pharmaceuticals
(2019)
Modular plants using intensified continuous processes represent an appealing concept for the production of pharmaceuticals. It can improve quality, safety, sustainability, and profitability compared to batch processes; besides, it enables plug-and-produce reconfiguration for fast product changes. To facilitate this flexibility by real-time quality control, we developed a solution that can be adapted quickly to new processes and is based on a compact nuclear magnetic resonance (NMR) spectrometer. The NMR sensor is a benchtop device enhanced to the requirements of automated chemical production including robust evaluation of sensor data. Beyond monitoring the product quality, online NMR data was used in a new iterative optimization approach to maximize the plant profit and served as a reliable reference for the calibration of a near-infrared (NIR) spectrometer. The overall approach
was demonstrated on a commercial-scale pilot plant using a metal-organic reaction with pharmaceutical relevance.
Modular plants using intensified continuous processes represent an appealing concept to produce pharmaceuticals. It can improve quality, safety, sustainability, and profitability compared to batch processes, and it enables plug-and-produce reconfiguration for fast product changes. To facilitate this flexibility by real-time quality control, we developed a solution that can be adapted quickly to new processes and includes a compact Nuclear Magnetic Resonance (NMR) spectrometer for online quality monitoring as well as a new model-based control approach. The NMR sensor is a benchtop device enhanced to the requirements of automated chemical production including ro-bust evaluation of sensor data.
Here, we present alternatives for the quantitative determination of the analytes using modular, physically motivated models. These models can be adapted to new substances solely by the use of their corresponding pure component spectra, which can either be derived from experimental spectra as well as from quantum mechanical models or NMR predictors. Modular means that spec-tral models can simply be exchanged together with alternate reagents and products. Beyond that, we comprehensively calibrated an NIR spectrometer based on online NMR process data for the first time within an industrial plant. The integrated solution was developed for a metal organic reac-tion running on a commercial-scale modular pilot plant and it was tested under industrial conditions.
Die Technologie-Roadmap „Prozess-Sensoren 2027+“ ist eine Weiterentwicklung vorgängiger Technologie-Roadmaps. Im Zentrum dieser Roadmaps stehen Sensoren zur Erfassung von physikalischen und chemischen Messgrößen mittels spezifischer und unspezifischer Messverfahren, die zur Steuerung und dem besseren Verständnis von Prozessen dienen.
Die Roadmap fasst die gemeinsame Technologie- und Marktsicht von Anwendern, Herstellern und Forschungseinrichtungen im Bereich Prozess-Sensorik in der verfahrenstechnischen Industrie zusammen. Sie beschreibt die wesentlichen Trends im Bereich Prozess-Sensorik und künftige Handlungsbedarfe für Hersteller, Anwender sowie für Einrichtungen der Forschung und Lehre.
Für die aktuellen und zukünftigen Anforderungen an Prozess-Sensoren werden 19 Thesen formuliert. Die Thesen basieren auf den Thesen der vorangegangenen Roadmaps, wobei die aus heutiger Sicht erforderlichen Anpassungen, Ergänzungen und teilweise auch Streichungen vorgenommen wurden. Die Thesen sind in 5 Themencluster eingeordnet. Digitalisierung und Nachhaltigkeit sind übergreifende Kernthemen der künftigen Entwicklung.
In case study one of the CONSENS project, two aromatic substances were coupled by a lithiation reaction, which is a prominent example in pharmaceutical industry. The two aromatic reactants (Aniline and o-FNB) were mixed with Lithium-base (LiHMDS) in a continuous modular plant to produce the desired product (Li-NDPA) and a salt (LiF). The salt precipitates which leads to the formation of particles. The feed streams were subject to variation to drive the plant to its optimum.
The uploaded data comprises the results from four days during continuous plant operation time. Each day is denoted from day 1-4 and represents the dates 2017-09-26, 2017-09-28, 2017-10-10, 2017-10-17.
In the following the contents of the files are explained.
Air pollution and climate change are potential drivers for the increasing burden of allergic diseases. The molecular mechanisms by which air pollutants and climate parameters may influence allergic diseases, however, are complex and elusive. This article provides an overview of physical, chemical and biological interactions between air pollution, climate change, allergens, adjuvants and the immune system, addressing how these interactions may promote the development of allergies. We reviewed and synthesized key findings from atmospheric, climate, and biomedical research. The current state of knowledge, open questions, and future research perspectives are outlined and discussed. The Anthropocene, as the present era of globally pervasive anthropogenic influence on planet Earth and, thus, on the human environment, is characterized by a strong increase of carbon dioxide, ozone, nitrogen oxides, and combustion- or traffic-related particulate matter in the atmosphere. These environmental factors can enhance the abundance and induce chemical modifications of allergens, increase oxidative stress in the human body, and skew the immune system toward allergic reactions. In particular, air pollutants can act as adjuvants and alter the immunogenicity of allergenic proteins, while climate change affects the atmospheric abundance and human exposure to bioaerosols and aeroallergens. To fully understand and effectively mitigate the adverse effects of air pollution and climate change on allergic diseases, several challenges remain to be resolved. Among these are the identification and quantification of immunochemical reaction pathways involving allergens and adjuvants under relevant environmental and physiological conditions.